• Title/Summary/Keyword: Nano Scale

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Study on the Microstructure of Trivalent Chrome Layers b AFM and SANS

  • Choi, Y.;Lee, J.J.;Lee, B.K.;Kim, M.;Kwon, S.C.;Seung, B.S.
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2003.05a
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    • pp.61-61
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    • 2003
  • It is important to know SIze distribution of defects In electroplated trivalent chrome layers because it significantly influences on performance of the layers. Most of the nano-scale defects are able to be introduced by hydrogen evolution during the plating. Little information is available on the nano-size defects. In this study, SANS was applied to determine the size distribution of nano-scale defects in the trivalent chrome layers prepared in a formate bath. The defect size and distribution was dependent upon plating conditions such as current density and applied voltage. SANS is one of useful techniques to determine the nano-scale defect in the electroplated layers.

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AC Breakdown Property of Nano-$TiO_2$ and Micro-Silica filler Mixture of Epoxy Based Composites

  • Heo, J.;Jung, E.H.;Lim, K.J.;Kang, S.H.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.11a
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    • pp.150-150
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    • 2009
  • In this paper, various kinds of epoxy based nanocomposites were made and AC breakdown properties of nano-$TiO_2$ and micro-silica filler mixture of epoxy based composites were studied by sphere to sphere electrode. Moreover, nano- and micro-filler combinations were adopted as an approach toward practical application of nanocomposite insulating materials. AC breakdown test was performed at room temperature $(25^{\circ}C)$, $80^{\circ}C$ and $100^{\circ}C$. The result shows breakdown strength about non-filled, nano-scale $TiO_2$, micro-scale silica and nano-$TiO_2$, micro-silica filled epoxy composites.

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Dynamic response of nano-scale plates based on nonlocal elasticity theory (비국소 탄성 이론을 이용한 나노-스케일 판의 강제진동응답)

  • Kim, Jin-Kyu;Han, Sung-Cheon;Park, Weon-Tae
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.14 no.1
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    • pp.436-444
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    • 2013
  • This article presents the dynamic response of nano-scale plates using the nonlocal continuum theory and higher-order shear deformation theory. The nonlocal elasticity of Eringen has ability to capture the small scale effects and the higher-order shear deformation theory has ability to capture the quadratic variation of shear strain and consequently shear stress through the plate thickness. The solutions of transient dynamic analysis of nano-scale plate are presented using these theories to illustrate the effect of nonlocal theory on dynamic response of the nano-scale plates. The relations between nonlocal and local theories are discussed by numerical results. Also, the effects of nonlocal parameters, aspect ratio, side-to-thickness ratio, size of nano-scale plate and time step on dynamic response are investigated and discussed. The amplitude and cycle increase when nonlocal parameter increase. In order to validate the present solutions, the reference solutions are used and discussed. The theoretical development as well as numerical solutions presented herein should serve as reference for nonlocal theories as applied to the transient dynamic analysis of nano-scale structures.

Microstructure Analysis of Rabbit and Chicken Femurs by Light Microscopy and Transmission Electron Microscopy (광학현미경과 투과전자현미경을 이용한 토끼와 닭 대퇴골의 미세구조 분석)

  • Kim, Chang-Yeon;Kim, Eun-Kyung;Jeon, Tae-Hoon;Nam, Seung-Won;Kim, Youn-Joong
    • Applied Microscopy
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    • v.40 no.3
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    • pp.155-162
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    • 2010
  • Bone is a hierarchically structured composite material which has been well studied by the materials engineering community because of its unique structure and mechanical properties. Bone is a laminated organic-inorganic composite composed of primarily hydroxyapatite, collagen and water. The main mineral that gives bone's hardness is calcium phosphate, which is also known as hydroxyapatite. Light microscopy (LM) and transmission electron microscopy (TEM) were used to study the structure of femurs from chicken and rabbit. The elemental analysis was used to search variation in the distribution of calcium, potassium and oxygen in the femur. Current investigation focused on two structural scales: micro scale (arrangement of compact bone) and nano scale (collagen fibril and apatite crystals). At micro scale, distinct difference was found in microstructures of chicken femur and rabbit femur. At nano scale, we analyzed the shape and size of apatite crystals and the arrangement of collagen fibril. Consequently, femurs of chicken and rabbit had very similar chemical property and structures at nano scale despite of their different species.

Fabrication of Ag doped Hydroxyapatite and its Antimicrobial Effects with the Particle Size

  • Oh, Kyung-Sik;Kim, Kyung-Ja;Jeong, Young-Keun
    • Journal of Powder Materials
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    • v.8 no.3
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    • pp.192-196
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    • 2001
  • Ag doped Hydroxyapatite powder in nano-scale was successfully synthesized either by co-precipitation or by ion exchange route. The fabricated powder was successfully dispersed through freeze drying due to the prevention of secondary particles. The antimicrobial effects of nano-HAp against E.coli was superior to micron ones not only in its strength but also in duration.

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A study of nano-scale electrical discharge characteristics for automotive sensor applications

  • Choi, Hae-Woon;Han, Man-Bae
    • Proceedings of the KWS Conference
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    • 2009.11a
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    • pp.235-238
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    • 2009
  • To study the relationship between spark ignition and the gap in the nano-scale region, the electric potential was applied to between a Pt-Ir tip and a gold substrate. The tip was sharpened by electro-chemical etching process in the solution of $CaCl_2;H_2O$ and acetone. The radius of tip was measured to be around 200nm and attached to the scanning probe microscope to control the gap between the tip and the substrate. The electric potential of 10V to 80V was applied to initialize the spark. The gaps and the current profile were measured to analyze the characteristics of spark ignition. A spark sustaining time was measured to be between 50ns and 200ns depending on the applied electric potential and the gap between the electrodes. The continuous electric discharge was successfully sustained up to 1 second of spark or arc time. The developed process can be applicable to the micro-scale fabrication of automotive sensors as a similar concept of GTAW.

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Improvement of Brightness for AlGaInP High-brightness LEDs with Nano-scale Roughness on Top-GaP Surface (Top-GaP 상부에 나노 크기의 Roughness 처리에 의한 AlGaInP 고휘도 LED의 휘도 향상)

  • So, Soon-Jin;Ha, Hun-Sung;Park, Choon-Bae
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.1
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    • pp.68-72
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    • 2008
  • AlGaInP high-brightness LEDs(HB-LEDs) have gained importance a variety of application operating in the red, orange, yellow and yellow-green wavelength. The light generated from inside LED chips should be emitted to the air through the surfaces of the chips. However, because of the differences between the semiconductor and air or epoxy's refractive index, some of the light was blocked so that caused lowering external quantum efficiency. In this study, nano-scale roughness on the top-GaP layer of AlGaInP epitaxial wafer was fabricated to improve' the brightness of AlGaInP LEDs. Nano-scale roughness was made by ICP dry etcher. Our AlGaInP LEDs with nano-scale roughness has higher brightness (about 28.5 %) than standard AlGaInP LEDs.