• Title/Summary/Keyword: NIST

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A Study on the Radioactive Products of Components in Proton Accelerator on Short Term Usage Using Computed Simulation (몬테칼로 시뮬레이션을 활용한 양성자가속기 단기사용 시 구성품의 방사화 평가)

  • Bae, Sang-Il;Kim, Jung-Hoon
    • Journal of radiological science and technology
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    • v.43 no.5
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    • pp.389-395
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    • 2020
  • The evaluation of radioactivated components of heavy-ion accelerator facilities affects the safety of radiation management and the exposure dose for workers. and this is an important issue when predicting the disposal cost of waste during maintenance and dismantling of accelerator facilities. In this study, the FLUKA code was used to simulate the proton treatment device nozzle and classify the radio-nuclides and total radioactivity generated by each component over a short period of time. The source term was evaluated using NIST reference beam data, and the neutron flux generated for each component was calculated using the evaluated beam data. Radioactive isotopes caused by generated neutrons were compared and evaluated using nuclide information from the International Radiation Protection Association and the Korea Radioisotope association. Most of the nuclides produced form of beta rays and electron capture, and short-lived nuclides dominated. However, In the case of 54Mn, which is a radioactive product of iron, the effect of gamma rays should be considered. In the case of tritium generated from a material with a low atomic number, it is considered that handling care should be taken due to its long half-life.

Data intercomparison and determination of toxic and trace elements in Algae using Instrumental Neutron Activation Analysis (중성자방사화분석에 의한 Algae중의 독성미량원소의 정량 및 실험실간 비교검증)

  • Chung, Yong-Sam;Moon, Jong-Hwa;Park, Kwang-Won;Lee, KiI-Yong;Yoon, Yoon-Yeol
    • Analytical Science and Technology
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    • v.12 no.4
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    • pp.346-353
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    • 1999
  • For the non-destructive multi-elemental analysis of environmental and biological materials, instrumental neutron activation analysis (INAA) was applied for the determination of toxic and trace elements in a set of three Algae samples provided by the International Atomic Energy Agency (IAEA). The analytical quality control was evaluated by comparing the analytical results of two standard reference materials of the National Institute of Standards and Technology (NIST); Oyster Tissue (SRM 1566a) and Citrus Leaves (SRM 1572). According to given analytical procedure, the concentration of 15-25 elements including spiked elements such as As, Cd, Cr and Hg in Algae samples were determined. To identify and validate these results, a data intercomparison program using more than 35 analytical methods in 150 laboratories was carried out and the estimated statistical data are summarized. Result of INAA is favorable, therefore, it is illustrated that can be applied for routine analysis of essential and toxic elements in algae samples as well as analytical quality assurance.

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Development of Analytical Techniques for Human Serum and Urine by Using Glow Discharge (글로우 방전을 이용한 혈청과 뇨의 분석기술 개발)

  • Lee, Sang Chun;Choi, Kyung-Soo;Son, Eun-Ho;Sim, Young-Jin
    • Analytical Science and Technology
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    • v.11 no.3
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    • pp.167-173
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    • 1998
  • An electrothermal vaporization-hollow cathode glow discharge-atomic emission spectrometer(ETV-HCGD-AES) has been developed for detecting heavy metals in human serum and urine samples. Fisrt of all, we designed a glow discharge cell for atomic emission spectrometry and its analytical performance was studied with the standard reference materials(SRMs) purchased from the NIST. Practically, the ETV-HCGD-AES demonstrated better instrumental sensitivity and selectivity for detecting Hg and Pb in the SRMs, serum and urine, than ICP-OES since the ETV-HCGD-AES was not required the complicate sample digestion procedure, which improved sample transportation efficiency.

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A Technique to Minimize Impurity Signal from Blank Rhenium Filaments for Highly Accurate TIMS Measurements of Uranium in Ultra-Trace Levels

  • Park, Jong-Ho;Choi, In-Hee;Song, Kyu-Seok
    • Mass Spectrometry Letters
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    • v.1 no.1
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    • pp.17-20
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    • 2010
  • As background significantly affects measurement accuracy and a detection limit in determination of the trace amounts of uranium, it is necessary to minimize the impurities in the filaments used for thermal ionization mass spectrometry (TIMS). We have varied the degassing condition such as the heating currents and duration times to reduce the backgrounds from the filaments prepared with zone-refined rhenium tape. The most efficient degassing condition of the heating current and the duration time was determined as 3.5 A and 60 min, respectively. The TIMS measurement combined with the isotope dilution mass spectrometry (IDMS) technique showed that the uranium backgrounds were determined to be in a few fg level from blank rhenium filaments. The background minimized filaments were utilized to measure the uranium isotope ratios of a U030 (NIST) standard sample. The excellent agreement of the measurement with the certified isotope ratios showed that the degassing procedure optimized in this study efficiently reduced the impurity signals of uranium from blank rhenium filaments to a negligible level.

Look-Up Table Based Implementations of SHA-3 Finalists: JH, Keccak and Skein

  • Latif, Kashif;Aziz, Arshad;Mahboob, Athar
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • v.6 no.9
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    • pp.2388-2404
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    • 2012
  • Cryptographic hash functions are widely used in many information security applications like digital signatures, message authentication codes (MACs), and other forms of authentication. In response to recent advances in cryptanalysis of commonly used hash algorithms, National Institute of Standards and Technology (NIST) announced a publicly open competition for selection of new standard Secure Hash Algorithm called SHA-3. One important aspect of this competition is evaluation of hardware performances of the candidates. In this work we present efficient hardware implementations of SHA-3 finalists: JH, Keccak and Skein. We propose high speed architectures using Look-Up Table (LUT) resources on FPGAs, to minimize chip area and to reduce critical path lengths. This approach allows us to design data paths of SHA-3 finalists with minimum resources and higher clock frequencies. We implemented and investigated the performance of these candidates on modern and latest FPGA devices from Xilinx. This work serves as performance investigation of leading SHA-3 finalists on most up-to-date FPGAs.

Elemental Analysis of Coal by Inductively Coupled Plasma Mass Spectrometry (誘導結合플라스마 質量分析法에 의한 石炭의 元素 分析)

  • 이용근;고인형;이동수
    • Journal of Korean Society for Atmospheric Environment
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    • v.8 no.3
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    • pp.155-161
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    • 1992
  • A simple, fast yet sensitive method is described for the determination of fifty elements in coal by inductively coupled plasma mass spectrometry. The method involves complete dissolution of coal with mixed acid $(HNO_3, HF, HClO_4)$ in hish pressure Teflon bomb and subsequent inductively coupled plasma mass spectrometric(ICP-MS) measurement. The accuracy of the method, being evaluated by the analysis of NIST SRMs (1632a, 1632b) is better than 20% RSD for most elements. The limits of detection defined by two times $\sigma$ (standard deviation of operational blank) are in order of sub-ppm to ppm, which are low enough to quantitate most elements. However, the determiantions for few elements such as V, As, Se are severely interfered by molecular ions such that their accurate determiantions are not possible. Analytical results for twentyon coals from eight countries including six ones world major coal producing, Korea, Japan, China, I.C.S., U.S.A., Canada, Australia, and South Africa are presented. While the results for major elements agree well with the existing ones, those for a few trace elements disagree considerably. The existing values are considerably higher. It is not possible to judge which are more accurate. However, the exisisting values are more likely to be errorous inasmuch as they are obtained without using high purity reagents and clean laboratory techniques.

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A Numerical Modeling of Smoke Behavior and Detection in a Pressurized Module(PM) of the International Space Station(ISS) (국제우주정거장의 가압모듈에서 연기거동 및 감지에 관한 수치 모델링)

  • Park, Seul-Hyun;Lee, Joo-Hee;Kim, Youn-Kyu;Hwang, Cheol-Hong
    • Proceedings of the Korea Institute of Fire Science and Engineering Conference
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    • 2011.11a
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    • pp.7-10
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    • 2011
  • 최근 국제우주정거장에서 화재안전에 관한 중요성의 인식으로 화재의 감지/소화의 메커니즘을 구체적으로 이해하기 위한 다양한 연구들이 시도되고 있다. 본 연구에서는 국제우주정거장에서 각종 실험과 연구를 진행하는 가압모듈을 대상으로 환기, 연기거동 및 감지에 관한 수치모델링을 수행하였다. 수치모델링은 NIST에서 개발된 FDS (Fire Dynamic Simulator)가 사용되었다. 국제우주정거장 내부는 마이크로중력환경으로 부력이 존재하지 않아 화재 발생 시 화염 및 연기거동은 지상에서의 현상들과 큰 차이를 보이게 된다. 따라서 현재 가압모듈에서 적용되고 있는 환기조건의 변화에 따른 연기거동 및 감지특성에 대한 연구는 향후 국내의 국제 우주정거장 실험 참여를 위한 기초적인 정보를 제공할 것으로 기대된다.

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Multi-dimensional Fire Behaviors in an Under-ventilated Compartment Fire (환기부족 구획화재에서 다차원 화재거동)

  • Hwang, Cheol-Hong;Park, Chung-Hwa;Ko, Gwon-Hyun;Lock, Andrew
    • Proceedings of the Korea Institute of Fire Science and Engineering Conference
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    • 2010.04a
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    • pp.37-42
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    • 2010
  • 실제 규모 ISO 9705 표준 화재실에서 과환기(over-ventilated) 및 환기부족(under-ventilated) 화재에 대한 열 및 화학적 특성에 관한 실험이 수행되었다. 또한 FDS(Fire Dynamic Simulator)를 이용하여 수치적 예측성능에 대한 평가와 환기부족화재에서 건물 내부의 다차원 화재현상에 대한 해석이 이루어졌다. 과환기 및 환기부족화재의 특성은 연소효율, 총괄 당량비 뿐만 아니라 고온 상층부의 온도분포, 연소 생성물의 농도에 의해 명확하게 구분되었다. 실험결과와의 비교를 통해 과환기 및 환기부족화재에서 FDS는 공간내부의 온도, 열유속 및 다양한 화학종의 분포를 정량적으로 잘 예측함을 확인하였다. 과환기화재와 비교할 때, 환기부족화재에서 내부유동은 반대방향의 다차원 재순환 유동구조를 갖고 있음을 발견하였다. 동시에 공간내부의 $O_2$ 및 CO의 분포 역시 다차원 구조를 갖기 때문에 기존화재연구에서 측정되는 고온 상층부의 열 및 화학적 특성은 환기부족화재를 이해하는데 많은 한계가 있음을 확인하였다.

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Application of Methane Mixed Plasma for the Determination of Ge, As, and Se in Serum and Urine by ICP/MS

  • Park, Kyung-Su;Kim, Sun-Tae;Kim, Young-Man;Kim, Yun-je;Lee, Won
    • Bulletin of the Korean Chemical Society
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    • v.24 no.3
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    • pp.285-290
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    • 2003
  • An analytical method for the simultaneous determination of trace Ge, As and Se in biological samples by inductively coupled plasma/mass spectrometry has been investigated. The effects of added organic gas into the coolant argon gas on the analyte signal were studied to improve the detection limit, accuracy and precision. The addition of a small amount of methane (10 mL/min.) into the coolant gas channel improved the ionization of Ge, As and Se. The analytical sensitivity of the proposed Ar/CH₄system was superior by at least two-fold to that of the conventional Ar method. In the present method, the detection limits obtained for Ge, As and Se were 0.014, 0.012 and 0.064 ㎍/L, respectively. The analytical reliability of the proposed method was evaluated by analyzing the certified standard reference materials (SRM). Recoveries of 99.9% for Ge, 103% for As, 96.5% for Se were obtained for NIST SRM of freeze dried urine sample. The proposed method was also applied to the biological samples.

Development of a New Refrigerant Mixture (RM-1) to improve the performance of Heat Pump System for Heating and Cooling of the Living Space (생활공간 냉난방용 열펌프의 성능개선을 위한 새로운 혼합냉매(RM-1) 개발)

  • Song, Heon;Ro, Jeong-Geun
    • Journal of the Korean Solar Energy Society
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    • v.31 no.5
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    • pp.67-76
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    • 2011
  • 생활공간 냉난방용 열펌프의 성능향상을 위해 R22의 대체 냉매로서 새로운 혼합냉매R22/R23/R152a(RM-1)을 개발하고 U. S. A.의 NIST사의 REFPRO Pprogram을 이용해 이 혼합냉매의 P-h diagram을 구성하여 실용화에 이용할 수 있도록 하였다. 본 연구는 실험을 통해 R22와 RM-1의 열펌프 성능효과를 분석하였다. 입 출구 물의 온도와 제2의 전열매체로서 물의 질량유량, 압축기의 소요 에너지 그리고 열펌프의 기타 열적 특성을 다양한 조건하에서 측정하였다. 이 실험 데이터를 통해 공기-물 열펌프 시스템에서의 RM-1과 R22의 성능계수(COP)를 비교하였다. 이를 통해, 혼합냉매 RM-1을 사용하는 열펌프 시스템은 외기온 $-17^{\circ}C$에서도 2.2의 성능계수로 작동하는 결과를 본 연구에서 보여주었다.