• Title/Summary/Keyword: NIOSH method

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Determination of Arylmethyl Halides by Gas Chromatograph (Gas Chromatograph에 의한 Arylmethy Halides의 정량)

  • Oh, Dos Suk;Choi, Ho Chun
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.4 no.1
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    • pp.25-32
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    • 1994
  • Arylmethyl halides(benzyl chloride, BZYC; benzal chloride, BZYA; benzotrichloride, BZTC) and related compounds(benzyl alcohol, BZYA; benzoyl chloride, BZOC) were determined by GC using capillary column. Detailed results are as follows. 1. Stability In methanol benzotrichloride slowly transferred to benzoyl chloride by hydrolysis(ca. 7.5% for 5 days), but the others were stable. Therefore, benzotrichloride solution should be prepared just before analysis. 2. GC analysis Tenax-GC was used to absorbent and desorption solvents were $CCl_4$ and MeOH. Arylmethyl halides were analyzed within 7.5min without interference with related compounds. The calibration curve(ca. 15-80 ppm in soln), repeatability(n=10) and the desorption efficiency were good. Limit of detection by NIOSH method was about 0.003 ppm for arylmethyl halide, respectively. To analyze arylmethyl halides and related compounds in working places GC using capillary column is anticipated to be used effectively.

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Worker Exposure to Asbestos Fibers in Asbestos Slate Manufacturing and Asbestos Textile Industries (석면슬레이트 제조 및 석면방직사업장 근로자의 석면분진폭로)

  • 박두용;백남원
    • Journal of Environmental Health Sciences
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    • v.14 no.2
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    • pp.13-27
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    • 1988
  • Two asbestos slate manufacturing and seven asbestos textile plants in Korea were surveyed from May 20 to July 2, 1987. The purposes of this study were to evaluate 1) worker exposure to asbestos, 2) compliance to the standards and 3) the efficiency of existing local exhaust systems. Sixty-two personal samples and eighty-three area samples were collected and analyzed using "NIOSH 7400" method. Results of this study were as follows. 1. The asbesots exposure concentrations in asbestos textile plants were 1.3 - 14.3 fibers/cc(geometric mean(GM), 4.4 fibers/cc). 2. Worker exposure level to asbestos fiber in asbestos slate manufacturing industry was 0.21 fibers/cc during wet processing, which is below the Korean Standard of 2 fibers/cc. 3. Most local exhaust systems installed in asbestos textile plants were inadequately designed. 4. Ninety-six percent of the 145 samples exceeded the U.S. Occupational Safety and Health Administration (OSHA) Permissible Exposure Limit (PEL) of 0.2 fibers/cc and forty-nine percent of the samples exceeded the Korean Standatd of 2 fibers/cc.

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Job Stress and Work-related Musculoskeletal Symptoms of General Hospital Nurses (일개 종합병원 간호사의 직무스트레스와 근골격계 증상)

  • Woo, Nam-Hee;Kim, Souk-Young
    • Korean Journal of Occupational Health Nursing
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    • v.18 no.2
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    • pp.270-280
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    • 2009
  • Purpose: This study was conducted to examine the relationship between job stress and work-related musculoskeletal symptoms of hospital nurses. Method: The questionnaires were administered to 290 nurses working in a general hospital located in S city from September 1 to 15, 2008. The data were analysed with descriptive statistics, and logistic regression test by SPSS WIN 14.0. Results: With the NIOSH criteria 1, the musculoskeletal symptoms were prevalent in 66.8% of the subjects. The musculoskeletal symptoms by body parts appeared mostly on leg/foot(40.6%) and followed by shoulder (38.7%), waist(30.3%), neck(23.6%), hand/wrist/finger(14.0%) and arm/elbow(4.4%). There were statistically significant differences in prevalence rate of musculoskeletal symptoms by age, work department, career and job stress. Conclusion: When developing a management program for musculoskeletal symptoms of hospital nurses, it is necessary to fully understand nurses' work considering each hospital's nursing administration system.

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A Simple Proposition for Improving Industrial Hygiene Air Sampling Methods

  • Paik, Samuel Y.;Zalk, David M.
    • Safety and Health at Work
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    • v.10 no.3
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    • pp.389-392
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    • 2019
  • When conducting an exposure assessment, the primary goal of the industrial hygienist is to fully characterize the worker's exposure during a work shift to compare it with an occupational exposure limit. This applies regardless of the duration of the work activity as an activity that is relatively short in duration can still present exposure in excess of the occupational exposure limit even when normalized over an 8-hr shift. This goal, however, is often impeded by the specification of a minimum sample volume in the published sampling method, which may prevent the sample from being collected or submitted for analysis. Removing the specification of minimum sample volume (or adjusting it from a requirement to a recommendation), in contrast, allows for a broader assessment of jobs that consist of short-duration and high-exposure activities and also eliminates the unnecessary practice of running sampling pumps in clean air to collect a specified, minimum volume.

A Comparison of Collection Concentrations Based on Airborne Toluene Diisocyanates Measurement Methods (공기 중 Toluene diisocyanates 측정방법에 따른 포집농도 비교)

  • Park, Hyung-Sung;Won, Jong-Uk;Kim, Chi-Nyon;Roh, Jaehoon
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.23 no.4
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    • pp.341-347
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    • 2013
  • Objectives: The aim of this study is to investigate the differences in airborne TDI concentrations based on the filter collection method and liquid collection method and to compare airborne TDIs concentrations by sampling method change when using the filter collection method in the spray-painting process. Methods: For the sample measurement, the filter collection method(OSHA#42) and liquid collection method(NIOSH#5522) were used; for the sampling method, the full-period single sampling and full-period consecutive sampling methods were used. The samples were collected in spray-painting and drying process locations. Results: In all samples collected from the spray-painting and drying process locations through the filter collection and liquid collection methods, greater amounts of 2,6-TDI than 2,4-TDI were detected. When the TDI collection concentrations based on the sampling methods were compared, the concentrations of 2,4-TDI and 2,6-TDI collected by the consecutive sampling method were higher than the concentrations of 2,4-TDI and 2,6-TDI collected by the single sampling method for both the filter collection method and liquid collection method used in the spray-painting process. These differences were statistically significant. Conclusions: When TDI collection concentrations based on the sample measurement methods were compared, the concentration of 2,4-TDI and 2,6-TDI collected through the liquid collection method were higher than the concentrations of 2,4-TDI and 2,6-TDI collected by the filter collection method, and the differences were statistically significant. In the drying process, no difference was shown in the collection concentrations of 2,4-TDI and 2,6-TDI with the two measurement methods.

Behavior Evaluation of Aluminium oxide through Measurement of Mass Concentration under Laboratory Environment (연구실 환경에서의 질량농도 측정을 통한 Aluminium oxide의 거동 평가)

  • Park, Jeong-Hwa;Kim, Dong-Hyun;Kim, Jong-Kyu;Kim, Hyung-Sik;Kim, Jeong-Hun
    • Journal of Digital Convergence
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    • v.14 no.3
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    • pp.279-285
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    • 2016
  • With the development of nanotechnology, the amount of nanomaterials increases and the problems of environment and the toxic property associated with it have become a social problem. But regulations and laws of nanomaterials have not yet been established. The purpose of this study is to utilize as the database of safety guidelines for research activities' workers associated with nanomaterials to conduct a behavior evaluation of aluminium oxide, which is most widely used in thirteen kinds of WPMN manufactured nanomaterials in the country. The experiment proceeds in the chamber reduced to 1/6 size of the actual laboratory, the test method was performed in NIOSH 0500. As the results of the study, the mass concentration was in inverse proportion to the particle size of the nanomaterials. And the mass concentration during the operation of ventilation equipment was reduced to about 1/8 times. In the future, it can be utilized as the database of safety guidelines for research activities' workers associated with nanomaterials. However, in order to increase the reliability of the study, the experiment of the mass concentration by particle size and Condensation Particle Counters will be needed additionally.

A Study of the Effects of the Trunk Angles and the Upper Ann Angles on Workloads in the Lifting Work (들기작업 시 몸통각도와 상완각도가 작업부담에 미치는 영향에 관한 연구)

  • Chang, Seong-Rok;Park, Hyung-Gu
    • Journal of the Korean Society of Safety
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    • v.24 no.2
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    • pp.69-75
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    • 2009
  • It is well-known that lifting capacity of a worker is influenced by body posture during the task. When a task analyst make use of RULA and REBA Trunk and upper arm angles are recorded in a separate item. It means that the interaction between the angles of two body segments may be ignored in a final score. The NLE(NIOSH Lifting Equation) has been used to supplement this problem. However, there is no study to validate the result of RWL (Recommended Workload Limit) under the existence of interactions between trunk and upper arm angles. The goal of this study was to assess the effect of the interaction between trunk and upper arm angles. Three responses, including NMVC(normalized maximum voluntary contraction), RWL(Recommended Weight Limit) and subjective judgment in psychophysical method (Borg's scale), were recorded according to the combinations of three trunk angles and nine upper arm angles. The results showed that lifting capacity is highly influenced by interaction of two body segments(trunk and upper arm). It means that the task workload has to be analyzed along with the interaction of trunk angles and upper arm angles when the task analyst assesses potential risk factors on the postures. This study may be able to be a fundamental study to develop an assessment method for lifting task analyses according to body postures.

Examination of Formaldehyde Emissions from the Hot-Pressing of Particleboard (파티클보드의 열압으로부터 포름알데히드 배출량 조사)

  • Oh, Yong-Sung;Kwak, Jun-Hyuk
    • Journal of the Korean Wood Science and Technology
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    • v.29 no.4
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    • pp.33-39
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    • 2001
  • Laboratory particleboards (PBs) were made with urea-formaldehyde (UF) resins at four press times and two resin application rates. Enclosed caul system was used for collecting the exhaust gases materials generated during the hot-pressing of PB. Exhaust gases materials generated inside the enclosed caul during the hot-pressing of PB were collected in a controlled air stream. Formaldehyde from the exhaust gases collected was determined per a chromotropic method of the National Institute of Occupational Safety and Health Method 3500. The test results showed that formaldehyde emissions during the hot-pressing of PB increased with increasing press time, UF resin mole ratio, and resin application rate.

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Reduction of Hexavalent Chromium Collected on PVC Filters in Field Electroplating Process (현장 도금 공정에서 PVC 여과지에 채취된 6가 크롬의 환원)

  • Shin Yong Chul;Paik Nam Won;Yi Gwang Yong;Lee Byung Kyu;Lee Ji Tae
    • Journal of Environmental Health Sciences
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    • v.28 no.1
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    • pp.41-49
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    • 2002
  • Recently, pilot studies showed an evidence of reduction of airborne hexavalent chromium, Cr(VI), on PVC filter during air sampling and storage. However, the information on this in the field was limited. Thus, we studied the reduction behaviors of airborne Cr(VI) on PVC filters during sampling and storage at three field electroplating operations. Regression between sampling time and the reduction (ratio of Cr(VI) to total Cr concentrations) was not statistically significant (p>0.05). However, the reductions in samples collected for 240 ~ 340 minutes were significantly higher than those for 30 - 60 minutes. On the other hand, another experiment showed a good correlation (r=0.96) between sampling time and the reduction without an exceptional value. Storage temperature was not a factor affecting the reduction of Cr(VI) collected on PVC filter. The loss of Cr(VI) samples stored in alkali solution (2% NaOH/3% Na$_2$CO$_3$) was significantly lower than that stored in vial according to NIOSH method (p<0.05). Thus, dipping Cr(VI) samples into alkali solution was a storage method to minimize tile reduction.

Comparison between the Charcoal Tube Sampling Method and the Diffusive Sampler, and the Applicability of Diffusive Sampler in the Field (확산형포집기(3M OVM #3500)와 활성탄관의 유기용제 포집농도 비교 및 확산형포집기의 현장 적용 가능성)

  • Jang, Sung Ho;Kim, Hyoung-Ah
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.15 no.3
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    • pp.261-269
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    • 2005
  • To investigate the field applicability of a diffusive sampler (3M OVM #3500, passive sampling method) authors conducted a simultaneous measurement of personal organic solvents exposure in the air of the workplaces by charcoal tube with low volume sampler (active sampling method) and diffusive sampler. Samples were collected and analyzed by NIOSH method ($NMAM^{(R)}$) from thirty-eight workers in 12 factories who work in 6 different processes. Geometric mean (GM) and geometric standard deviation (GSD) were used to describe the result. To compare the results of the two methods, paired t-test was used. According to the manual of the exposure assessment of the mixed organic solvents (Ministry of Labor, Korea), Em was calculated. Simple linear regression was used to evaluate the relationship between the two methods. Results were as follows; 1. Eight different solvents (ethyl acetate, n-hexane, toluene, xylene, acetone, isopropyl alcohol, methyl ethyl ketone (MEK), and methyl isobutyl ketone) were detected simultaneously in the two methods and the concentrations of the personal exposure were lower than 0.5 TLV level. The concentration of the charcoal tube method was higher than that of a diffusive sampler in n-hexane and MEK (p<0.05). 2. Em of the charcoal tube method was higher than that of diffusive sampler method but not significantly different and was lower than the OEL (Occupational Exposure Limit) in all 6 processes. 3. There was a significant correlation between the two methods in low concentrations of the 8 organic solvents (p<0.05). In conclusion, there was no difference in charcoal tube method and diffusive sampler method in low concentrations of some organic solvents, diffusive sampler can be applied to assess the personal monitoring in low level exposure.