• 제목/요약/키워드: N.D.C method

검색결과 792건 처리시간 0.032초

Electronic and Optical Properties of amorphous and crystalline Tantalum Oxide Thin Films on Si (100)

  • Kim, K.R.;Tahir, D.;Seul, Son-Lee;Choi, E.H.;Oh, S.K.;Kang, H.J.;Yang, D.S.;Heo, S.;Park, J.C.;Chung, J.G.;Lee, J.C.
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2009년도 제38회 동계학술대회 초록집
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    • pp.382-382
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    • 2010
  • $TaO_2$ thin films as gate dielectrics have been proposed to overcome the problems of tunneling current and degradation mobility in achieving a thin equivalent oxide thickness. An extremely thin $SiO_2$ layer is used in order to separate the carrier in MOSFETchannel from the dielectric field fluctuation caused by phonons in the dielectric which decreases the carrier mobility. The electronic and optical properties influenced the device performance to a great extent. The atomic structure of amorphous and crystalline Tantalum oxide ($TaO_2$) gate dielectrics thin film on Si (100) were grown by utilizing atomic layer deposition method was examined using Ta-K edge x-ray absorption spectroscopy. By using X-ray photoelectron spectroscopy and reflection electron energy loss spectroscopy (REELS) the electronic and optical properties was obtained. In this study, the band gap (3.400.1 eV) and the optical properties of $TaO_2$ thin films were obtained from the experimental inelastic scattering cross section of reflection electron energy loss spectroscopy (REELS) spectra. EXAFS spectra show that the ordered bonding of Ta-Ta for c-$TaO_2$ which is not for c-$TaO_2$ thin film. The optical properties' e.g., index refractive (n), extinction coefficient (k) and dielectric function ($\varepsilon$) were obtained from REELS spectra by using QUEELS-$\varepsilon$(k, $\omega$)-REELS software shows good agreement with other results. The energy-dependent behaviors of reflection, absorption or transparency in $TaO_2$ thin films also have been determined from the optical properties.

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LC-MS/MS를 이용한 베타락탐계 항생제와 베타차단제의 동시분석 (Simultaneous analysis of β-lactam antibiotics and β-blockers by LC-MS/MS)

  • 손보영;김준일;안치화;이수원;김복순;정득모
    • 분석과학
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    • 제29권4호
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    • pp.179-185
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    • 2016
  • 물 시료 중에 잔류하는 β-차단제 3종(아테놀롤, 메토프롤롤, 프로프라놀롤)과 β-락탐계 항생제 6종(아목시실린, 페니실린G, 세파클러, 세파드록실, 세파렉신, 세프라딘)을 다른 두 종류의 카트리지를 사용하여 효과적인 분석방법을 정립하였다. 고분자 친수성-친유성 균형 카트리지(Hydrophile-lipophile balance, HLB)와 강한 양이온 교환 혼합 모드인 고분자 흡수 카트리지(Mixed mode cation exchange, MCX)를 사용하여 자동고체상 추출장치(Solid-phase extraction, SPE)로 전처리를 하였다. 충분한 크로마토그래피 분리를 위해 XDB-C18 (1.8 μm; 3.0 mm × 100 mm) 컬럼을 사용하였다. 정량을 위한 검정곡선의 상관계수(r²)가 0.995 이상으로 우수한 직선성을 나타내었다. 방법검출한계(Method detection limits, MDL)와 정량한계(Limit of quantitation, LOQ)는 각각 1.1~3.9 ng/L와 5~13 ng/L이었다. 이 분석방법으로 한강으로 유입되는 지천과 원수를 실태 조사 한 결과 N.D.~0.209 μg/L 농도로 검출되었다.

재귀적 SPCPC에 반복적 복호법을 적용할 때 처리 이득이 성능에 미치는 영향 (Effect of Processing Gain on the Iterative Decoding for a Recursive Single Parity Check Product Code)

  • 전수원;김용철
    • 한국통신학회논문지
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    • 제35권9C호
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    • pp.721-728
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    • 2010
  • 재귀적 구조의 SPCPC (single parity check product code)인 CAMC (constant amplitude multi-code) 는 반복적 복호를 행할 때 SPCPC에 비하여 오류 정정 성능이 우수하다. 본 논문에서는 대역확산 신호인 CAMC의 처리 이득이 성능 향상에 미치는 영향을 분석한다. 일반적인 곱 부호에서는 반복적 복호로 오류 정정 과정이 종료되지만, CAMC 는 반복적 복호 후의 역확산 과정에서 추가적으로 오류가 정정된다. 잔존하는 비트 오류의 수가 ($\sqrt{N}/2-1$)개 이하인 경우에는 (N은 코드워드의 길이), 역확산 과정에서 그 오류들은 모두 정정된다. 반복적 복호에서 EI (extrinsic information)의 분포 형태를 관찰한 결과, 초기의 EI 분포는 대체로 랜덤하나, 몇 회의 iteration 후에는 ($-E_{max}$) 혹은 ($+E_{max}$)의 이진 값으로 수렴한다. EI의 분포가 오류 정정의 진행 사항을 반영하는 점을 이용하는 iteration 제어 방법을 실험한 결과 Eb/No 에서 약 0.2 dB의 이득을 얻었다.

Accelerated inflammation in peripheral artery disease patients with periodontitis

  • Kure, Keitetsu;Sato, Hiroki;Aoyama, Norio;Izumi, Yuichi
    • Journal of Periodontal and Implant Science
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    • 제48권6호
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    • pp.337-346
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    • 2018
  • Purpose: Peripheral artery disease (PAD) is a form of arteriosclerosis that occurs in the extremities and involves ischemia. Previous studies have reported that patients with periodontitis are at high risk for PAD. However, the relationship between these 2 diseases has not yet been fully elucidated. In this cross-sectional study, we investigated this relationship by comparing patients with PAD to those with arrhythmia (ARR) as a control group. Methods: A large-scale survey was conducted of patients with cardiovascular disease who visited Tokyo Medical and Dental University Hospital. We investigated their oral condition and dental clinical measurements, including probing pocket depth, bleeding on probing, clinical attachment level, and number of missing teeth; we also collected salivary and subgingival plaque samples and peripheral blood samples. All patients with PAD were extracted from the whole population (n=25), and a matching number of patients with ARR were extracted (n=25). Simultaneously, ARR patients were matched to PAD patients in terms of age, gender, prevalence of diabetes, hypertension, dyslipidemia, obesity, and the smoking rate (n=25 in both groups). Real-time polymerase chain reaction was performed to measure the bacterial counts, while the enzyme-linked immunosorbent assay method was used to measure anti-bacterial antibody titers and proinflammatory cytokine levels in serum. Results: PAD patients had more missing teeth ($18.4{\pm}2.0$) and higher serum levels of C-reactive protein ($1.57{\pm}0.85mg/dL$) and tumor necrosis factor-alpha ($70.3{\pm}5.7pg/mL$) than ARR patients ($12.0{\pm}1.7$, $0.38{\pm}0.21mg/dL$, and $39.3{\pm}4.5pg/mL$, respectively). Meanwhile, no statistically significant differences were found in other dental clinical measurements, bacterial antibody titers, or bacterial counts between the 2 groups. Conclusions: Our findings suggested that PAD patients had poorer oral and periodontal state with enhanced systemic inflammation.

Li2O-Bi2O3 첨가가 Pb(Mg1/3Nb2/3)0.65Ti0.35O3 세라믹의 압전 특성에 미치는 영향 (Effect of Li2O-Bi2O3 Addition on the Piezoelectric Properties of Pb(Mg1/3Nb2/3)0.65Ti0.35O3 Ceramics)

  • 김재혁;김시연;최정식;여동훈;신효순;남산
    • 한국분말재료학회지
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    • 제26권5호
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    • pp.405-409
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    • 2019
  • Piezoelectric ceramic specimens with the $Pb(Mg_{1/3}Nb_{2/3})_{0.65}Ti_{0.35}O_3$ (PMN-PT) composition are prepared by the solid state reaction method known as the "columbite precursor" method. Moreover, the effects of the $Li_2O-Bi_2O_3$ additive on the microstructure, crystal structure, and piezoelectric properties of sintered PMN-PT ceramic samples are investigated. The addition of $Li_2O-Bi_2O_3$ lowers the sintering temperature from $1,200^{\circ}C$ to $950^{\circ}C$. Moreover, with the addition of >5 wt.% additive, the crystal structure changes from tetragonal to rhombohedral. Notably, the sample with 3 wt.% additive exhibits excellent piezoelectric properties ($d_{33}=596pC/N$ and Kp = 57%) and a sintered density of $7.92g/cm^3$ after sintering at $950^{\circ}C$. In addition, the sample exhibits a curie temperature of $138.6^{\circ}C$ at 1 kHz. Finally, the compatibility of the sample with a Cu electrode is examined, because the energy-dispersive X-ray spectroscopy data indicate the absence of interdiffusion between Cu and the ceramic material.

3상회로의 직접해석에 의한 배전계통 선간단락 사고 고장거리 계산 알고리즘 (A new line to line fault location algorithm in distribution power networks using 3 phase direct analysis)

  • 진보건;최면송;이승재;윤남선;정병태;이덕수
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2002년도 하계학술대회 논문집 A
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    • pp.108-110
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    • 2002
  • In this paper, a fault location algorithm is suggested for line to line faults in distribution networks. Conventional fault location algorithms use the symmetrical component transformation, a very useful tool for transmission network analysis. However, its application is restricted to balanced network only. Distribution networks are, in general, operated in unbalanced manners, therefore, conventional methods cannot be applied directly, which is the reason why there are few research results on fault location in distribution networks. Especially, the line to line fault is considered as a more difficult subject. The proposed algorithm uses direct 3-phase circuit analysis, which means it can be applied not only to balanced networks but also to unbalanced networks like distribution a network. The comparisons of simulation results between one of conventional methods and the suggested method are presented to show its effectiveness and accuracy.

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신뢰성 공학적 피로 균열의 발생, 진전 수명 평가 및 예측에 관한 연구 ( I ) -피로 균열 진전 수명의 통계학적 분포 특성- (Evalustion and Prediction for the Fatigue crack Initiation and Growth Life by Reliability Approach (I) -Statistical Consideration for Fatigue Crack Growth Life-)

  • 권재도;최선호;황재석;곽상국;전경옥;장재영
    • 대한기계학회논문집
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    • 제14권6호
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    • pp.1583-1591
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    • 1990
  • 본 연구에서는 결함체의 정도 높은 수명 예측을 하기 위한 기초연구의 일환으 로서 다수의 피로 실험을 통한 다수의 실험 데이터로부터 확률 통계학적 방법을 적용 해서 피로 균열의 발생, 진전 및 파단 특성의 정략적인 파악을 수행하여, 수명예측 및 신뢰성 평가를 위한 시스템에 도입함으로써 실제 구조물의 수명예측에 적용하고자 한 다. 피로 균열의 발생 및 파단수명의 통계적 분포특성과 수명예측에 관해서는 제2보 등에서 보고할 예정이다.

Pt/$SnO_2$ 가스 센서의 가스 감지 특성에 관한 연구 (A Study on the Gas Sensing Characteristics of Pt/$SnO_2$ Gas Sensor)

  • 이재홍;김창교;김진걸;김덕준
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1997년도 하계학술대회 논문집 C
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    • pp.1304-1307
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    • 1997
  • A hydrogen gas sensor utilizing Pt/$SnO_2$ system was fabricated by the pressed pellet method. The crystal structure, direction of the crystal, crystal size and microstructure between the catalyst and the support ($SnO_2$) were characterized with Electron Diffraction Analysis, Transmission Electron Microscopy, Scanning Electron Microscopy. After the reactor with a Pt/$SnO_2$ sample was run with a flow rate of 30sccm (a mixture of $0.5%H_2$ in $N_2$) for a while, the resistance of $SnO_2$ was saturated, but the $SnO_2$ kept absorbing $H_2$ gas. $H_2$ gas sensing properties of Pt/$SnO_2$ were investigated at several temperatures. As a result, it was observed that Pt/$SnO_2$ has high sensitivity at $300^{\circ}C$ and $400^{\circ}C$.

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게껍질로부터 CM-Chitin의 합성 (Synthesis of CM-Chitin from Crab Shells)

  • 안종일;김승환;유영진;박창호;임헌선;박찬구;박은경
    • 한국응용과학기술학회지
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    • 제10권2호
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    • pp.41-47
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    • 1993
  • Chitin was isolated from crab shells by modified Hackman's method, which was treated again with aqueous sodium hydroxide solution to give alkali chitin(sodium alkoxide of chitin). And after, the alkali chitin is allowed to react with monochloroacetic acid to synthesize 6-O-(carboxymethyl) chitin [CM-Chitin] under diminished pressure. In order to synthesize high performance CM-Chitin as hygroscopic agent, it was measured that the yield and degree of subsititution of each CM-Chitin according to molar ratio(monochloroacetic acid equivalent mol/N-acetyl-D-glucosamine residue) and their moisture-absorption and moisture-release properties were measured and compared with those of hyaluronic acid. The moisture-absorption and moisture-release properties of CM-Chitin, especially 0.8 in degree of substitution, were found quite similar to those of hyaluronic acid. The preliminary results show that CM-Chitin might be used as hygroscopic agent instead of hyaluronic acid in field of cosmetics.

MOD법을 이용 제조한 Bi3.25Nd0.75Ti3O12 강유전 박막의 열처리 온도에 따른 전기적 특성 (Electrical Characteristics of Bi3.25Nd0.75Ti3O12 Ferroelectric Thin Films Prepared by MOD Process Depending on Annealing Temperatures)

  • 김기범;장건익
    • 한국전기전자재료학회논문지
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    • 제16권7호
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    • pp.599-603
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    • 2003
  • Ferroelectric B $i_4$$_{-x}$N $d_{x}$ $Ti_3$ $O_{12}$ (BNdT) thin films with the composition(x=0.75) were prepared on Pt/Ti/ $SiO_2$(100) substrate by metal-organic deposition. The films were annealed by various temperatures from 550 to $650^{\circ}C$ and then the electrical and structural characteristics of BNdT films were investigated for the application of FRAM. Electrical properties such as dielectric constant, 2Pr and capacitance were quite dependent on the thermal heat treatment. The measured 2Pr value on the BNdT capacitor annealed at $650^{\circ}C$ was 56$\mu$C/$\textrm{cm}^2$ at an applied voltage of 5V. In fatigue characteristics value remained constant up to 8$\times$10$^{10}$ read/write switching cycles at a frequency of 1Mhz regardless of annealing temperatures.