• Title/Summary/Keyword: N.D.C method

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Electronic and Optical Properties of amorphous and crystalline Tantalum Oxide Thin Films on Si (100)

  • Kim, K.R.;Tahir, D.;Seul, Son-Lee;Choi, E.H.;Oh, S.K.;Kang, H.J.;Yang, D.S.;Heo, S.;Park, J.C.;Chung, J.G.;Lee, J.C.
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.382-382
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    • 2010
  • $TaO_2$ thin films as gate dielectrics have been proposed to overcome the problems of tunneling current and degradation mobility in achieving a thin equivalent oxide thickness. An extremely thin $SiO_2$ layer is used in order to separate the carrier in MOSFETchannel from the dielectric field fluctuation caused by phonons in the dielectric which decreases the carrier mobility. The electronic and optical properties influenced the device performance to a great extent. The atomic structure of amorphous and crystalline Tantalum oxide ($TaO_2$) gate dielectrics thin film on Si (100) were grown by utilizing atomic layer deposition method was examined using Ta-K edge x-ray absorption spectroscopy. By using X-ray photoelectron spectroscopy and reflection electron energy loss spectroscopy (REELS) the electronic and optical properties was obtained. In this study, the band gap (3.400.1 eV) and the optical properties of $TaO_2$ thin films were obtained from the experimental inelastic scattering cross section of reflection electron energy loss spectroscopy (REELS) spectra. EXAFS spectra show that the ordered bonding of Ta-Ta for c-$TaO_2$ which is not for c-$TaO_2$ thin film. The optical properties' e.g., index refractive (n), extinction coefficient (k) and dielectric function ($\varepsilon$) were obtained from REELS spectra by using QUEELS-$\varepsilon$(k, $\omega$)-REELS software shows good agreement with other results. The energy-dependent behaviors of reflection, absorption or transparency in $TaO_2$ thin films also have been determined from the optical properties.

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Simultaneous analysis of β-lactam antibiotics and β-blockers by LC-MS/MS (LC-MS/MS를 이용한 베타락탐계 항생제와 베타차단제의 동시분석)

  • Son, Bo-young;Kim, Jun-il;An, Chi-hwa;Lee, Su-won;Kim, Bogsoon;Chung, Deukmo
    • Analytical Science and Technology
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    • v.29 no.4
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    • pp.179-185
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    • 2016
  • An effective analytical method has been developed for the determination of β-blockers(atenolol, metoprolol and propranolol) and 6 β-lactams(amoxicillin, penicillin G, cefaclor, cefadroxil, cephalexin and cephradine) in water samples using two different cartridges. The samples were extracted by solid-phase extraction (SPE) with the usage of polymeric hydrophile-lipophile balance(HLB cartridges) and strong cation-exchange mixed-mode polymeric sorbent (MCX cartridges). A XDB-C18 column(1.8 μm; 3.0 mm × 100 mm) was used for the sufficient chromatographic resolution. The calibration curves showed good linearity with high correlation coefficients (>0.995). The method detection limits (MDL) and the limits of quantification(LOQ) were from 1.1 to 3.9 ng/L and from 5 to 13 ng/L, respectively. The method was applied for the determination of the target compounds in tributaries and raw water of the Han River and these were found at N.D. to 0.209 μg/L.

Effect of Processing Gain on the Iterative Decoding for a Recursive Single Parity Check Product Code (재귀적 SPCPC에 반복적 복호법을 적용할 때 처리 이득이 성능에 미치는 영향)

  • Chon, Su-Won;Kim, Yong-Cheol
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.35 no.9C
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    • pp.721-728
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    • 2010
  • CAMC (constant amplitude multi-code) has a better performance of error correction in iterative decoding than SPCPC (single parity check product code). CAMC benefits from a processing gain since it belongs to a spread spectrum signal. We show that the processing gain enhances the performance of CAMC. Additional correction of bit errors is achieved in the de-spreading of iteratively decoded signal. If the number of errors which survived the iterative decoding is less than or equal to ($\sqrt{N}/2-1$), all of the bit errors are removed after the de-spreading. We also propose a stopping criterion in the iterative decoding, which is based on the histogram of EI (extrinsic information). The initial values of EI are randomly distributed, and then they converge to ($-E_{max}$) or ($+E_{max}$) over the iterations. The strength of the convergence reflects how successfully error correction process is performed. Experimental results show that the proposed method achieves a gain of 0.2 dB in Eb/No.

Accelerated inflammation in peripheral artery disease patients with periodontitis

  • Kure, Keitetsu;Sato, Hiroki;Aoyama, Norio;Izumi, Yuichi
    • Journal of Periodontal and Implant Science
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    • v.48 no.6
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    • pp.337-346
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    • 2018
  • Purpose: Peripheral artery disease (PAD) is a form of arteriosclerosis that occurs in the extremities and involves ischemia. Previous studies have reported that patients with periodontitis are at high risk for PAD. However, the relationship between these 2 diseases has not yet been fully elucidated. In this cross-sectional study, we investigated this relationship by comparing patients with PAD to those with arrhythmia (ARR) as a control group. Methods: A large-scale survey was conducted of patients with cardiovascular disease who visited Tokyo Medical and Dental University Hospital. We investigated their oral condition and dental clinical measurements, including probing pocket depth, bleeding on probing, clinical attachment level, and number of missing teeth; we also collected salivary and subgingival plaque samples and peripheral blood samples. All patients with PAD were extracted from the whole population (n=25), and a matching number of patients with ARR were extracted (n=25). Simultaneously, ARR patients were matched to PAD patients in terms of age, gender, prevalence of diabetes, hypertension, dyslipidemia, obesity, and the smoking rate (n=25 in both groups). Real-time polymerase chain reaction was performed to measure the bacterial counts, while the enzyme-linked immunosorbent assay method was used to measure anti-bacterial antibody titers and proinflammatory cytokine levels in serum. Results: PAD patients had more missing teeth ($18.4{\pm}2.0$) and higher serum levels of C-reactive protein ($1.57{\pm}0.85mg/dL$) and tumor necrosis factor-alpha ($70.3{\pm}5.7pg/mL$) than ARR patients ($12.0{\pm}1.7$, $0.38{\pm}0.21mg/dL$, and $39.3{\pm}4.5pg/mL$, respectively). Meanwhile, no statistically significant differences were found in other dental clinical measurements, bacterial antibody titers, or bacterial counts between the 2 groups. Conclusions: Our findings suggested that PAD patients had poorer oral and periodontal state with enhanced systemic inflammation.

Effect of Li2O-Bi2O3 Addition on the Piezoelectric Properties of Pb(Mg1/3Nb2/3)0.65Ti0.35O3 Ceramics (Li2O-Bi2O3 첨가가 Pb(Mg1/3Nb2/3)0.65Ti0.35O3 세라믹의 압전 특성에 미치는 영향)

  • Kim, Jae Hyuk;Kim, Shi Yeon;Choi, Jeoung Sik;Yeo, Dong-Hun;Shin, Hyo-Soon;Nahm, Sahn
    • Journal of Powder Materials
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    • v.26 no.5
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    • pp.405-409
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    • 2019
  • Piezoelectric ceramic specimens with the $Pb(Mg_{1/3}Nb_{2/3})_{0.65}Ti_{0.35}O_3$ (PMN-PT) composition are prepared by the solid state reaction method known as the "columbite precursor" method. Moreover, the effects of the $Li_2O-Bi_2O_3$ additive on the microstructure, crystal structure, and piezoelectric properties of sintered PMN-PT ceramic samples are investigated. The addition of $Li_2O-Bi_2O_3$ lowers the sintering temperature from $1,200^{\circ}C$ to $950^{\circ}C$. Moreover, with the addition of >5 wt.% additive, the crystal structure changes from tetragonal to rhombohedral. Notably, the sample with 3 wt.% additive exhibits excellent piezoelectric properties ($d_{33}=596pC/N$ and Kp = 57%) and a sintered density of $7.92g/cm^3$ after sintering at $950^{\circ}C$. In addition, the sample exhibits a curie temperature of $138.6^{\circ}C$ at 1 kHz. Finally, the compatibility of the sample with a Cu electrode is examined, because the energy-dispersive X-ray spectroscopy data indicate the absence of interdiffusion between Cu and the ceramic material.

A new line to line fault location algorithm in distribution power networks using 3 phase direct analysis (3상회로의 직접해석에 의한 배전계통 선간단락 사고 고장거리 계산 알고리즘)

  • Jin, B.G.;Choi, M.S.;Lee, S.J.;Yoon, N.S.;Jung, B.T.;Lee, D.S.
    • Proceedings of the KIEE Conference
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    • 2002.07a
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    • pp.108-110
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    • 2002
  • In this paper, a fault location algorithm is suggested for line to line faults in distribution networks. Conventional fault location algorithms use the symmetrical component transformation, a very useful tool for transmission network analysis. However, its application is restricted to balanced network only. Distribution networks are, in general, operated in unbalanced manners, therefore, conventional methods cannot be applied directly, which is the reason why there are few research results on fault location in distribution networks. Especially, the line to line fault is considered as a more difficult subject. The proposed algorithm uses direct 3-phase circuit analysis, which means it can be applied not only to balanced networks but also to unbalanced networks like distribution a network. The comparisons of simulation results between one of conventional methods and the suggested method are presented to show its effectiveness and accuracy.

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Evalustion and Prediction for the Fatigue crack Initiation and Growth Life by Reliability Approach (I) -Statistical Consideration for Fatigue Crack Growth Life- (신뢰성 공학적 피로 균열의 발생, 진전 수명 평가 및 예측에 관한 연구 ( I ) -피로 균열 진전 수명의 통계학적 분포 특성-)

  • 권재도;최선호;황재석;곽상국;전경옥;장재영
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.14 no.6
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    • pp.1583-1591
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    • 1990
  • Life prediction and residual life prediction of structures of machines are one of the most strongly world wide needed problems as requirement in the stage of slowly developing economy which comes after rapidly and highly developing stage. For the purpose of statistical life prediction, fatigue test was conducted under the 4 stress levels, and for each stress level, about 20 specimens are used. The statistical properties of crack growth parameter m and C in the fatigue crack growth law of da/dN=C(.DELTA.K)sup m/, and the relationship between m and C, and the statistical distribution pattern of fatigue crack growth rate can be obtained by experimental results.

A Study on the Gas Sensing Characteristics of Pt/$SnO_2$ Gas Sensor (Pt/$SnO_2$ 가스 센서의 가스 감지 특성에 관한 연구)

  • Lee, J.H.;Kim, C.K.;Kim, J.G.;Kim, D.J.
    • Proceedings of the KIEE Conference
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    • 1997.07d
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    • pp.1304-1307
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    • 1997
  • A hydrogen gas sensor utilizing Pt/$SnO_2$ system was fabricated by the pressed pellet method. The crystal structure, direction of the crystal, crystal size and microstructure between the catalyst and the support ($SnO_2$) were characterized with Electron Diffraction Analysis, Transmission Electron Microscopy, Scanning Electron Microscopy. After the reactor with a Pt/$SnO_2$ sample was run with a flow rate of 30sccm (a mixture of $0.5%H_2$ in $N_2$) for a while, the resistance of $SnO_2$ was saturated, but the $SnO_2$ kept absorbing $H_2$ gas. $H_2$ gas sensing properties of Pt/$SnO_2$ were investigated at several temperatures. As a result, it was observed that Pt/$SnO_2$ has high sensitivity at $300^{\circ}C$ and $400^{\circ}C$.

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Synthesis of CM-Chitin from Crab Shells (게껍질로부터 CM-Chitin의 합성)

  • Ahn, C.I.;Kim, S.H.;Yoo, Y.J.;Park, C.H.;Lim, H.S.;Park, C.K.;Park, E.K.
    • Journal of the Korean Applied Science and Technology
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    • v.10 no.2
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    • pp.41-47
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    • 1993
  • Chitin was isolated from crab shells by modified Hackman's method, which was treated again with aqueous sodium hydroxide solution to give alkali chitin(sodium alkoxide of chitin). And after, the alkali chitin is allowed to react with monochloroacetic acid to synthesize 6-O-(carboxymethyl) chitin [CM-Chitin] under diminished pressure. In order to synthesize high performance CM-Chitin as hygroscopic agent, it was measured that the yield and degree of subsititution of each CM-Chitin according to molar ratio(monochloroacetic acid equivalent mol/N-acetyl-D-glucosamine residue) and their moisture-absorption and moisture-release properties were measured and compared with those of hyaluronic acid. The moisture-absorption and moisture-release properties of CM-Chitin, especially 0.8 in degree of substitution, were found quite similar to those of hyaluronic acid. The preliminary results show that CM-Chitin might be used as hygroscopic agent instead of hyaluronic acid in field of cosmetics.

Electrical Characteristics of Bi3.25Nd0.75Ti3O12 Ferroelectric Thin Films Prepared by MOD Process Depending on Annealing Temperatures (MOD법을 이용 제조한 Bi3.25Nd0.75Ti3O12 강유전 박막의 열처리 온도에 따른 전기적 특성)

  • 김기범;장건익
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.7
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    • pp.599-603
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    • 2003
  • Ferroelectric B $i_4$$_{-x}$N $d_{x}$ $Ti_3$ $O_{12}$ (BNdT) thin films with the composition(x=0.75) were prepared on Pt/Ti/ $SiO_2$(100) substrate by metal-organic deposition. The films were annealed by various temperatures from 550 to $650^{\circ}C$ and then the electrical and structural characteristics of BNdT films were investigated for the application of FRAM. Electrical properties such as dielectric constant, 2Pr and capacitance were quite dependent on the thermal heat treatment. The measured 2Pr value on the BNdT capacitor annealed at $650^{\circ}C$ was 56$\mu$C/$\textrm{cm}^2$ at an applied voltage of 5V. In fatigue characteristics value remained constant up to 8$\times$10$^{10}$ read/write switching cycles at a frequency of 1Mhz regardless of annealing temperatures.