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High Temperature Stability of Nitride Ceramic Materials in LiF-NdF3-Nd2O3 Molten Salts System (LiF-NdF3-Nd2O3 용융염에서 질화물계 세라믹재료의 고온안정성)

  • Kwon, Sukcheol;Lee, Young-Jun;Ryu, Hong-Youl;Lee, Go Gi;Jo, Sung Koo;Lee, Jong-Hyeon
    • Korean Journal of Materials Research
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    • v.25 no.12
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    • pp.694-702
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    • 2015
  • Nd-Fe-B permanent magnets have been used in a wide variety of applications because of their high magnetic flux density. So, demand for neodymium has been increasing in worldwide. In this study, an electrowinning process was performed in $LiF-NdF_3-Nd_2O_3$ high temperature molten salts. However, a corrosion resistant material for use in the molten salt must be found for stable operation because of the harsh corrosion environment of the electrowinning process. Therefore, for this paper, boron nitride(BN), aluminum nitride(AlN), and silicon nitride($Si_3N_4$) were selected as protective and structural materials in the high temperature electrolyte. To investigate the characteristics of BN, AlN, and $Si_3N_4$, in molten salts, materials were immersed in the molten salts for 24, 72, 120, and 192 hours. Also, surface condition and stability were investigated by SEM and EDS and corrosion products were calculated by HSC chemistry. As a result, among BN, AlN, and $Si_3N_4$, AlN was found to show the best protective material properties.

A Study on the Synthesis and Its Biodistribution of C-11 and F-18 Labelled Choline (C-11 및 F-18 표지 콜린의 합성과 체내동태에 관한 연구)

  • Yang, Seung-Dae;Kim, Sang-Wook;Suh, Yong-Sup;Chun, Kwon-Soo;Ahn, Soon-Hyuk;Hur, Min-Goo;Lim, Sang-Moo;Hong, Sung-Woon;Yu, Kook-Hyun
    • The Korean Journal of Nuclear Medicine
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    • v.35 no.3
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    • pp.185-191
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    • 2001
  • Objectives: Recently, $[methyl-^{11}C]-({\beta}$-Hydroxyethyl)trimethylammonium ($[^{11}C]$choline) Has been discovered to be a very effective tracer in imaging various human tumors using positron omission tomography. Because of the short half-life of C-11, it is very difficult to use in a routine imaging procedure and needs a frequent synthesis of $[^{11}C]$choline. This can be supplemented by the substitution of $[^{11}C]$choline with $[methyl-^{18}F]$fluorocholine. Here, we would like to report ceil uptake and biodistribution of $[^{11}C]$choline and $[^{18}F]$fluorocholine as a basic study. Methods: $[^{11}C]$Choline was prepared by the treatment of $[^{11}C]CH_3I$ with N,N-dimethylaminoethanol and $[^{18}F]$fluorocholine was synthesized from reaction of $CH_2Br[^{18}F]F$ with N,N-dimethylaminoethanol. The radiochemical purity was checked by high performance liquid chromatography (HPLC). The blodistribution of $[^{11}C]$choline and $[^{18}F]$fluorocholine was determined in balb/c mouse at 5 min, 20 min, 40 min and 80 min. The cell uptake was measured using glioma (9L) and colon adenocarcinoma (SW620). Results: The radiochemical purity was more than 98% after purification. In the liver, uptake did not change over time; the uptake was 20%ID/g for $[^{11}C]$choline and 13%ID/g for $[^{18}F]$fluorocholine. In the kidney, radioactivity decreased over time; the uptake was 15%ID/g for $[^{11}C]$choline and 20%ID/g for $[^{18}F]$fluorocholine, 80 min post-injection. The cell uptake of $[^{11}C]$choline was 4.93% for glioma (9L) and 18.69% for colon adenocarcinoma (SW620). For $[^{18}F]$fluorocholine, 1.77% for glioma (9L) and 2.77% for colon adenocarcinoma (SW620). Conclusion: $[^{11}C]$Choline and $[^{18}F]$fluorocholine showed a different cell uptake tendency, depending on cancer cell line.

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X-선 회절분석을 이용한 일라이트-스멕타이트 기본입자의 적층성에 관한 연구

  • 강일모;문희수
    • Proceedings of the Mineralogical Society of Korea Conference
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    • 2003.05a
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    • pp.10-10
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    • 2003
  • 일라이트-스멕타이트 혼합층광물(I-S)은 열역학적으로 상호 대립적인 두 가지 모델로 이해되고 있다. 첫째, MacEwan 결정자 모델은 I-S를 5-20개의 스멕타이트와 일라이트 층으로 구성된 결정자로 해석한다. 이러한 모델은 분산과 재응집 과정을 기초로 하는 X-선 회절분석(XRD)에서 기인한 것으로 Reynolds의 XRD 모델과 동일하다. 둘째, 기본입자 모델은 I-S를 물리적으로 분리될 수 있는 최소 입자인 기본입자가 $c^{*-}$축 방향으로 응집된 응집체로 해석한다. 이러한 모델은 분산 과정을 기초로 하는 주사전자현미경(TEM) 관찰에서 기인한 모델이다. 강일모 등(2002)은 이 두 가지 모델을 비교함으로써 1< $N_{F}$<100/% $S_{XRD}$ ( $N_{F}$=평균 기본입자 층개수, %$S_{XRD}$=XRD 분석을 통하여 측정된 팽창성)을 도출하였다. 이 식은 기본입자모델과 Eberl & Srodon(1988)이 제시한 최대 팽창성(%$S_{MAX}$)을 동시에 해석할 수 있게 해준다. %$S_{MAX}$는 XRD 모델에서는 고려하지 않는 I-S 결정자 상$\cdot$하부에 존재하는 두 개의 0.5nm 규산염층을 하나의 스멕타이트 층으로 간주하여 얻어진 팽창성이다. Srodon et al.(1992)은 %$S_{MAX}$=100/ $N_{F}$을 제시하였으며, 강일모 등(2002)은 %$S_{MAX}$는 기하학적으로 기본입자가 무한적층을 하였을 때 관찰되는 %$S_{XRD}$와 동일함을 밝힌 바 있다. 만약, XRD 분석을 위한 시료 준비과정에서 I-S 결정자가 분산되었다가 재응집을 한다면, XRD에서 관찰되는 결과는 일차적으로 기본입자의 적층성에 영향을 받게 된다. 따라서, 기본 입자의 적층성은 XRD 분석을 이용하여 I-S 구조를 해석하는데 매우 중요한 요인이다. 본 연구는 기본입자의 적층성을 정량화하기 위해 %$S_{XRD}$=A/ $N_{F}$ (0$S_{MAX}$=100/ $N_{F}$로부터 얼마나 벗어나 있는가는 지시해 준다 금성산화산암복합체에서 산출되는 11개 I-S 시료와 14개의 Drits et al.(1998) 자료로부터 1nA=-0.14 $N_{F}$+4.7의 실험식을 도출할 수 있었으며, 기본입자의 적층성은 일차적으로 기본입자의 두께에 의해 영향을 받는 것으로 관찰되었다. Nadeau(1985)는 기본입자두께분포로부터 I-S 결정자의 팽창성을 측정하기 위하여 Ps=$\Sigma$p(N)/N을 제시하였다(Ps=스멕타이트 층 비율, N=기본 입자 층개수, p(N)=N의 확율). 그러나 위식은 실질적으로 %$S_{MAX}$를 제공해주기 때문에 %$S_{XRD}$를 유추하는데는 부적합하다. 본 연구는 이를 변형하여 Ps=$\Sigma$p(N)A(N)/N을 제시하였다(A(N)=N에 대한 A값). 위의 실험식을 사용하여 헝가리산 Zempleni 시료(15%$S_{XRD}$)의 기본입자분포로부터 %$S_{XRD}$를 계산한 결과, 16%$S_{XRD}$의 결과값을 얻을 수 있었다. 따라서, 본 연구에서 도출한 관계식들이 유효함을 확인할 수 있었다.계식들이 유효함을 확인할 수 있었다.

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The improved Goldschmidt floating point reciprocal algorithm (개선한 Goldschmidt 부동소수점 역수 알고리즘)

  • 한경헌;최명용;김성기;조경연
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2004.05b
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    • pp.247-250
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    • 2004
  • Goldschmidt 알고리즘에 의한 부동소수점 1.f2의 역수는 q=NK1K2....Kn (Ki=1+Aj, j=2i)이다. 본 논문에서는 N과 A 값을 1.f2의 값에 따라서 선정하고 Aj의 값이 유효자리수의 반이하 값을 가지면 연산을 종료하는 개선된 Goldschmidt 부동소수점 역수 알고리즘을 제안한다. 1.f2가 1.01012보다 작으면 N=2-1.f2, A=1.f2-1로 하며, 1.01012보다 크거나 같으면 N=2-0.lf2, A=1-0.lf2로 한다. 한편 Goldschmidt 알고리즘은 곱셈을 반복해서 수행하므로 계산 오류가 누적이 된다. 이러한 누적 오류를 감안하면 배정도실수 역수에서는 2-57, 단정도실수 역수에서는 2-28의 유효자리수까지 연산해야 한다. 따라서 Aj가 배정도실수 역수에서는 2-29, 단정도실수 역수에서는 2-14 보다 작아지면 연산을 종료한다. 본 논문에서 제안한 개선한 Goldschmidt 역수 알고리즘은 N=2-0.1f2, A=1-0.lf2로 계산하는 종래 알고리즘과 비교하여 곱셈 연산 회수가 배정도실수 역수는 22%, 단정도실수 역수는 29% 감소하였다. 본 논문의 연구 결과는 테이블을 사용하는 Goldschmidt 역수 알고리즘에 적용해서 연산 시간을 줄일 수 있다.

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The Effect of Pilates Stabilization Exercise and Kinesio taping on the Dysmenorrhea and Prostaglandin F2α of Female University Students

  • Chang, Eun A;Koo, Il Seob;Choi, Jung Hyun
    • Journal of International Academy of Physical Therapy Research
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    • v.9 no.3
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    • pp.1558-1563
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    • 2018
  • This study, based on physical therapy interventions for menstruation disorders, observed the effect of Pilates stabilization exercises and Kinesio taping on dysmenorrhea and prostaglandin $F2{\alpha}$ levels. Female college students (n=37) who had >70 points on the mood disorder questionnaire (MDQ) and >4 points on the visual analogue scale (VAS) were divided into three different groups, the Pilates group (PG, n= 13), Pilates and Taping group (PTG, n=12), Taping group (TG, n=12). Pilates and taping were performed 3 times a week for 6 weeks. Pre- and post-menstruation difficulties were measured through the MDQ. Changes in blood prostaglandin $F2{\alpha}$ levels were also measured. Changes in pre- and post-menstrual pain and prostaglandin $F2{\alpha}$ levels were significantly reduced in the PG, PTG, and TG. Changes in pre- and post-menstrual pain and prostaglandin $F2{\alpha}$ levels resulted in significant differences in the PTG and TG. Dysmenorrhea and prostaglandin $F2{\alpha}$ levels were significantly decreased in the TG than in the PTG. These findings suggest that Pilates stabilization exercises and Kinesio taping are effective in decreasing menstrual difficulties and pain in female college students.

SOME PROPERTIES OF THE BEREZIN TRANSFORM IN THE BIDISC

  • Lee, Jaesung
    • Communications of the Korean Mathematical Society
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    • v.32 no.3
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    • pp.779-787
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    • 2017
  • Let m be the Lebesgue measure on ${\mathbb{C}}$ normalized to $m(D)=1,{\mu}$ be an invariant measure on D defined by $d_{\mu}(z)=(1-{\mid}z{\mid}^2)^{-2}dm(z)$. For $f{\in}L^1(D^n,m{\times}{\cdots}{\times}m)$, Bf the Berezin transform of f is defined by, $$(Bf)(z_1,{\ldots},z_n)={\displaystyle\smashmargin{2}{\int\nolimits_D}{\cdots}{\int\nolimits_D}}f({\varphi}_{z_1}(x_1),{\ldots},{\varphi}_{z_n}(x_n))dm(x_1){\cdots}dm(x_n)$$. We prove that if $f{\in}L^1(D^2,{\mu}{\times}{\mu})$ is radial and satisfies ${\int}{\int_{D^2}}fd{\mu}{\times}d{\mu}=0$, then for every bounded radial function ${\ell}$ on $D^2$ we have $$\lim_{n{\rightarrow}{\infty}}{\displaystyle\smashmargin{2}{\int\int\nolimits_{D^2}}}(B^nf)(z,w){\ell}(z,w)d{\mu}(z)d{\mu}(w)=0$$. Then, using the above property we prove n-harmonicity of bounded function which is invariant under the Berezin transform. And we show the same results for the weighted the Berezin transform in the polydisc.

ISOMORPHISM CLASSES OF HYPERELLIPTIC CURVES OF GENUS 2 OVER $F_{2_}{N}$ FOR EVEN n

  • Park, Chun-Soo;Rhee, Min-Surp
    • Journal of applied mathematics & informatics
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    • v.13 no.1_2
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    • pp.413-424
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    • 2003
  • L. H Encinas, A. J. Menezes and J. M. Masque in [3] proposed a classification of isomorphism classes of hyperelliptic curve of genus 2 over finite fields with characteristic different from 2 and 5. Y. Choie and D. Yun in [2] obtained the number of isomorphic classes of hyperelliptic curves of genus 2 over $F_{2-}$ using direct counting method. We have obtained isomorphism classes of hyperelliptic curves of genus 2 over $F_{2n}$ for odd n, represented by an equation of the form $y^2$ + $a_{5}$ y = $x^{5}$ + $a_{8}$ x + $a_{10}$ ( $a_{5}$ $\neq$0) [1]. In this paper we characterize hyperelliptic curves of genus 2 over $F_{2n}$ for even n, represented by an equation of the form $y^2$ + $a_{5}$ y = $x^{5}$ + $a_{5}$ x + $a_{10}$ ( $a_{5}$ $\neq$0).>0).

A Characteristic of Nitrogen and Phosphorus Removal in Anoxic/Oxic Basins combined with Iron Electrolysis (철 전기분해장치와 무산소/호기공정을 결합한 질소, 인제거 특성에 관한 연구)

  • Kim, Young-Gyu
    • Journal of Environmental Health Sciences
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    • v.43 no.6
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    • pp.525-531
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    • 2017
  • Objectives: The purpose of this experiment is to better understand the nitrogen and phosphorus removal ratio according to operating conditions in an iron electrolysis system consisting of an anoxic basin, aerobic basin, and iron precipitation apparatus. Methods: Iron electrolysis consists of an iron precipitation reactor composed of iron plates in oxic and anoxic basins. We studied the interrelation coefficient between T-N and T-P removal rates and F/M ratio, and the C/N ratio and BOD removal rate. Results: The F/M ratio and the T-N and T-P removal rate per unit area have interrelation coefficients of 0.362 and 0.603, respectively. The removal rate per MLVSS and the T-N and T-P removal rate per unit area have respective interrelation coefficients of 0.49 and 0.59. Conclusions: The removal rate of T-N and T-P increased with the increasing F/M ratio in the influent, and they also linearly increased in proportion to the C/N ratio of influent and BOD removal rate of the reactor.

SELF-ADJOINT INTERPOLATION PROBLEMS IN ALGL

  • Kang, Joo-Ho;Jo, Young-Soo
    • Journal of applied mathematics & informatics
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    • v.14 no.1_2
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    • pp.387-395
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    • 2004
  • Given operators X and Y acting on a Hilbert space H, an interpolating operator is a bounded operator A such that AX = Y. An interpolating operator for n-operators satisfies the equation $AX_{i}\;=\;Y_{i}$, for i = 1,2,...,n. In this article, we showed the following: Let H be a Hilbert space and let L be a subspace lattice on H. Let X and Y be operators acting on H. Assume that range(X) is dense in H. Then the following statements are equivalent: (1) There exists an operator A in AlgL such that AX = Y, $A^{*}$ = A and every E in L reduces A. (2) sup ${\frac{$\mid$$\mid${\sum_{i=1}}^n\;E_iYf_i$\mid$$\mid$}{$\mid$$\mid${\sum_{i=1}}^n\;E_iXf_i$\mid$$\mid$}$:n{\epsilon}N,f_i{\epsilon}H\;and\;E_i{\epsilon}L}\;<\;{\infty}$ and = for all E in L and all f, g in H.

Dentinal Tubules Occluding Effect Using Nonthermal Atmospheric Plasma

  • Lee, Chang Han;Kim, Young Min;Kim, Gyoo Cheon;Kim, Shin
    • International Journal of Oral Biology
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    • v.43 no.2
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    • pp.83-91
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    • 2018
  • Nonthermal atmospheric plasma has been studied for its many biomedical effects, such as tooth bleaching, wound healing, and coagulation. In this study, the effects of dentinal tubules occlusion were investigated using fluoride-carboxymethyl cellulose (F-CMC) gel, nano-sized hydroxyapatite (n-HA), and nonthermal atmospheric plasma. Human dentin specimens were divided to 5 groups (group C, HA, HAF, HAP, and HAFP). Group HA was treated with n-HA, group HAF was treated with n-HA after a F-CMC gel application, group HAP was treated with n-HA after a plasma treatment and group HAFP was treated with n-HA after a plasma and F-CMC gel treatment. The occlusion of dentinal tubules was investigated using scanning electron microscopy (SEM) and energy dispersive x-ray spectroscopy (EDS), which shows Ca/P ratio. In the EDS results, a higher Ca/P ratio was shown in the groups including n-HA than in the control group. The specimens of group HAP and HAFP had a higher Ca/P ratio in retentivity. In the SEM results, there was not a significant difference in the amount of times applied. Therefore, this study suggests F-CMC gel and n-HA treatment using nonthermal atmospheric plasma will be a new treatment method for decreasing hypersensitivity.