• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.24 no.3
• /
• pp.256-260
• /
• 2011

ZnO nanostructures with tetrapod, needle and multipod shapes were synthesized without catalysts through a simple thermal oxidation of metallic Zn powder in alumina crucible under air atmosphere. X-ray diffraction data revealed that the ZnO nanostructures had wurtzite structure of hexagonal phase. Energy dispersive X-ray (EDX) spectra showed that the ZnO was of high purity. After the oxidation of Zn powder, white colored product was mainly observed and yellow colored product was observed only a very little on the surface of the oxidized source materials. The white product consisted of tetrapods, while yellow product was composed of needles and multipods. Cathodoluminescece spectra showed that the crystalline quality of tetrapods was better that those of needles and multipods.

• New & Renewable Energy
• /
• v.6 no.3
• /
• pp.47-54
• /
• 2010

Foundation plays an important role in the offshore wind turbine system. Different from conventional foundations, the suction caisson is proven to be economical and reliable. In this work, three-dimensional finite element method is used to check the suitability of suction caisson foundation. NREL 5MW wind turbine is chosen as a baseline model in our simulation. The maximum overturning moment and vertical load at the mudline are calculated using FAST and Bladed. Meanwhile the soil-structure interaction response from our simulation is also compared with the experiment data from Oxford university. The design parameter such as caisson length, diameter of skirt and spacing of multipod are investigated. Accordingly based on these parameters suggestions are given to use suction caisson foundations more efficiently.

• Journal of the Korean Vacuum Society
• /
• v.18 no.1
• /
• pp.44-48
• /
• 2009

The effect of temperature gradient between the substrate and ambient gas on the structural characteristics of GaN nanorods grown on r-plane sapphire substrates by hydride vapor phase epitaxy was investigated. The density, diameter, and length strongly depended on the tempearture gradient. In addition, the cross-sectional shape of the nanorrods at the end of growth was found to be more dependedent on the temperature of a substrate itself than the temperature gradient.

• Journal of the Korean Crystal Growth and Crystal Technology
• /
• v.26 no.5
• /
• pp.175-180
• /
• 2016

ZnO nanoparticles were synthesized by aqueous preparation routes of a precipitation and a hydrothermal process. In the processes, the powders were formed by mixing aqueous solutions of Zn-nitrate hexahydrate ($Zn(NO_3)_2{\cdot}6H_2O$) with NaOH aqueous solution under controlled reaction conditions such as Zn precursor concentration, reaction pH and temperature. Single ZnO phase has been obtained under low Zn precursor concentration, high reaction pH and high temperature. The synthesized particles exhibited flakes (plates), multipods or rods morphologies and the crystallite sizes and shapes would be efficiently controllable by changing the processing parameters. The hydrothermal method showed advantageous features over the precipitation process, allowing the precipitates of single ZnO phase with higher crystallinity at relatively low temperatures below $100^{\circ}C$ under a wider pH range for the Zn precursor concentration of 0.1~1 M.