• Title/Summary/Keyword: Multichannel analyzer

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Interaction of Laser Beam with PZT - Target and Observation of Laser - Induced Plume and Particle Ejection (Laser와 PZT - Target간의 반응과 그에 따른 Plume 형성 및 입자 방출에 관한 연구)

  • Lee, Byeong-U
    • Journal of Advanced Marine Engineering and Technology
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    • v.20 no.5
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    • pp.93-102
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    • 1996
  • Laser-induced plume and laser-target interaction during pulsed laser deposition are demonstrated for a lead zirconate titanate (PZT). A KrF excimer laser (wavelength 248nm) was used and the laser was pulsed at 20Hz, with nominal pulse width of 20ns. The laser fluence was~$16J/cm^2,$ with 100mJ per pulse. The laser-induced plasma plume for nanosecond laser irradiation on PZT target has been investigated by optical emission spectra using an optical multichannel analyzer(OMA) and by direct observation of the plume using an ICCD high speed photography. OMA analysis showed two distinct ionic species with different expansion velocities of fast or slow according to their ionization states. The ion velocity of the front surface of the developing plume was about $10^7$cm/sec and corresponding kinetic energy was about 100eV. ICCD photograph showed another kind of even slower moving particles ejected from the target. These particles considered expelled molten parts of the target. SEM morphologies of the laser irradiated targets showed drastic melting and material removal by the laser pulse, and also showed the evidence of the molten particle ejection. The physics of the plasma(plume) formation and particle ejection has been discussed.

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THE EFFECTS OF WAVELENGTH AND INTENSITY OF VISIBLE LIGHT ON THE CURING OF VISIBLE LIGHT CURED COMPOSITE RESIN (가시광선의 파장과 광도가 광중합형 복합레진의 경화에 미치는 영향)

  • Lee, Chae-Gyeong;Hur, Bok
    • Restorative Dentistry and Endodontics
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    • v.14 no.1
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    • pp.149-159
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    • 1989
  • The purpose of this study was to assess the effects of wavelength and intensity of light curing units on the curing of composite resin. The wavelength and intensity of nine units were evaluated with Optical Multichannel Analyzer and Radiometer. Two-part split stainless steel mold with a cylindrical hole-3.0mm in diameter, 6.0mm in hgieht-was prepared. After placing a Mylar strip between two parts, 100 specimens were made by inserting each of four composite resins into the mold and irradiating for 20 seconds with five light units alternatively. The curing depths were measured by scraping method and evaluated by two-way ANOVA. And Vicker's hardness measurements were made on the longitudinally sectioned surface at 0.5mm interval. The results were as follows: 1. Visilux 2 showed a narrow spectral band within the effective wavelength in initiating polymerization and the highest intensity. Translux showed the diffuse spectrum of wavelength and the lower light intensity. 2. Visilux 2 showed the highest curing effect in any composite resin and then followed by Optilux, Efos 35, Heliomat and Translux. (p < 0.01) 3. Durafill showed the deepest curing depth in any light unit and then followed by Bisfil M, Silux and Heliosit. (p < 0.01). 4. Maximum hardness values showed 0.1mm and 0.5mm under top surface and then gradually decreased with depth.

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The polymer waveguide type SPR sensor using a multi-wavelength light source (다파장 광원을 이용한 폴리머 광도파로형 SPR 센서)

  • Park, Chang-Sub;Yeom, Se-Hyuk;Kim, Do-Eok;Kang, Byoung-Ho;Kim, Kyu-Jin;Kim, Hak-Rin;Kang, Shin-Won
    • Journal of Sensor Science and Technology
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    • v.16 no.6
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    • pp.401-406
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    • 2007
  • In this paper, we fabricated the polymer waveguide type surface plasmon resonance (SPR) sensor using a white light source and optical spectrum analyzer (OSA). Fabricated sensor uses the principle of phase matching between evanescent wave and surface plasmon wave. According to the measuring result, the shift of resonance wavelength conducts the change of the refractive index. The proposed SPR sensor is expected to apply the integrated multichannel SPR sensor and the realtime monitoring system.

DEVELOPMENT OF THE MATRA-LMR-FB FOR FLOW BLOCKAGE ANALYSIS IN A LMR

  • Ha, Kwi-Seok;Jeong, Hae-Yong;Chang, Won-Pyo;Kwon, Young-Min;Cho, Chung-Ho;Lee, Yong-Bum
    • Nuclear Engineering and Technology
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    • v.41 no.6
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    • pp.797-806
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    • 2009
  • The Multichannel Analyzer for Transient and steady-state in Rod Array - Liquid Metal Reactor for Flow Blockage analysis (MATRA-LMR-FB) code for the analysis of a subchannel blockage has been developed and evaluated through several experiments. The current version of the code is improved here by the implementation of a distributed resistance model which accurately considers the effect of flow resistance on wire spacers, by the addition of a turbulent mixing model, and by the application of a hybrid scheme for low flow regions. Validation calculations for the MATRA-LMR-FB code were performed for Oak Ridge National Laboratory (ORNL) 19-pin tests with wire spacers and Karlsruhe 169-pin tests with grid spacers. The analysis of the ORNL 19-pin tests conducted using the code reveals that the code has sufficient predictive accuracy, within a range of 5 $^{\circ}C$, for the experimental data with a blockage. As for the results of the analyses, the standard deviation for the Karlsruhe 169-pin tests, 0.316, was larger than the standard deviation for the ORNL 19-pin tests, 0.047.

Trace Element Analysis by Neutron Activastion Analysis in the Human Cancer Tissue (폐암조직에서 중성자 방사화 분석법을 이용한 미량 원소 분석)

  • Lim, Sang-Moo;Zo, Jae-Il;Shim, Young-Mog;Chung, Young-Ju;Cho, Seung-Yeon;Chung, Yong-Sam
    • The Korean Journal of Nuclear Medicine
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    • v.27 no.1
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    • pp.104-111
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    • 1993
  • Trace elements are important components in the biological system, as a structural material and metabolic controller. Neutron activation analysis (NAA) with high neutron flux and high energy resolution Ge (Li) detector coupled to multichannel analyzer (MCA) has been one of the most accurate method for the determination of ultra-trace level components, and is applicable to biological material. In human body, the NAA can be used for quantitation of trace elements in various organs and tissue with endocrinological and metabolic disease and industrial metal poisoning. In this study, Triga Mark III nuclear reactor in Korea Atomic Research Institute was used for quantitation of trace eleement in human lung cancer tissues by neutron activation analysis. In the squamous cell carcinoma tissues, Br, Hg, La, Sb, Sc, Cl, Fe and I content were lower than normal lung tissues, and K, Rb and Se content were higher. In the adenocarcinoma tissues, Fe, Au, La, Sc and Zn content were lower than normal lung tissues, and Rb, Co and Se content were higher. Rb content was higher in the adenocarcinoma tissues than in the squamous cell carcinoma tissues. Fe and Na content were higher in the squamous cell carcinoma tissues than in the adenocarcinoma tissues.

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Fabrication and Characterization of a Fiber-Optic Alpha/Beta Detector for Nuclear Medicine Application (핵의학 적용을 위한 광섬유 기반의 알파/베타 검출기의 제작 및 특성분석)

  • Hong, Seung-Han;Yoo, Wook-Jae;Shin, Sang-Hun;Seo, Jeong-Ki;Han, Ki-Tek;Jeon, Da-Yeong;Cho, Seung-Hyun;Lee, Bong-Soo
    • Journal of Sensor Science and Technology
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    • v.21 no.5
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    • pp.367-373
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    • 2012
  • We fabricated a fiber-optic alpha/beta detector, which is composed of a sensing probe, a plastic optical fiber, a photomultiplier tube, and a multichannel analyzer, to obtain the energy spectra of radioactive isotopes. As inorganic scintillators of a sensing probe, a ZnS(Ag) film was coupled with a $CaF_2$(Eu) crystal for alpha and beta spectroscopy. In this study, $^{210}Po$ and $^{90}Sr$ were used as alpha and beta sources, respectively, and we measured the radiation energy spectra using a fiber-optic alpha/beta detector to identify alpha and beta emitting radionuclides for nuclear medicine application. Also, the variations of energy spectrum were obtained according to the length of plastic optical fiber.

Study on the Dosimetry and Assessment of Terrestrial Radiation Exposure (지각 방사선에 의한 피폭선량측정 및 해석)

  • Jun, Jae-Shik;Oh, Hi-Peel;Ha, Chung-Woo
    • Journal of Radiation Protection and Research
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    • v.15 no.2
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    • pp.87-100
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    • 1990
  • For the quantitative evaluation and assessment of radiation exposure from terrestrial component of natural environmental radiation, successive thermoluminescence dosimetry and periodical in-situ gamma ray spectrometry were carried out for a period of 24 months. LiF PTFE dise TLDs and $3&{\phi}{\times}3'$cylindrical NaI(Tl)scintill ation detector in association of portable multichannel analyzer (4096 ch) were used in this study. The doses measured were evaluated and assessed in terms of effective dose equivalent. As a concomitant output, the dose equivalent due to ionizing component of cosmic ray was able to be evaluated. According to the results obtained in terms of variance weighted mean, the annual effective dose equivalents of terrestrial gamma ray and cosmic ray ionizing component in Taejeon area came out to be $564{\pm}4\;{\mu}Sv(64.8{\pm}0.5nSv{\cdot}h^{-1}$ and $300{\pm}2\;{\mu}Sv(34.3{\pm}0.2nSv{\cdot}h^{-1}$, respectively, which are reasonable comparably with that appeared in UNSCEAR Report[28]as per caput annual effective dose equivalent in 'areas of normal background radiation'.

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An Improved Method for the Determination of Scandium by Neutron Activation Analysis (스칸듐定量을 위한 改良된 放射化分析法)

  • Chung, Koo-Soon;Lee, Chul
    • Journal of the Korean Chemical Society
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    • v.8 no.2
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    • pp.88-91
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    • 1964
  • A rapid and simple method is described here for the determination of scandium in monazite by neutron activation analysis. The sample is irradiated for 20 hours at the neutron flux of $10^{12}$ thermal neutrons/$cm^2$/sec in the TRIGA MARK Ⅱ reactor, after which the sample is decomposed by fusion with concentrated sulfuric acid. The scandium-46 together with scandium carrier are separated from the irradiated sample by precipitating with ammonia, and are extracted by solvent extraction of the thiocyanate complex into ether. The induced radioactivity is measured by gamma scintillation spectrometry using the Multichannel Pulse Height Analyzer connected with 2"${\times}$2" NaI(Tl). The chemical yield is determined gravimetrically by precipitating scandium with mandelic acid. In order to check the efficiency of scandium separation and the errors from interfering activities of the other elements, scandium was separated by the cation exchange resin column, and the results from both samples were compared each other, which showed that the chemical procedure used in this work was as selective as the ion-exchange method with respect to scandium separation. The scandium contents in Korean monazite were found to be about 12 p. p. m.

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Determination of Spectrum-Exposure Rate Conversion Factor for a Portable High Purity Germanium Detector (휴대형 고순도 게르마늄검출기에 대한 스펙트럼-조사선량율 변환연산자의 결정)

  • Kwak, Sang-Soo;Park, Chong-Mook;Ro, Seung-Gy
    • Journal of Radiation Protection and Research
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    • v.13 no.2
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    • pp.29-40
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    • 1988
  • A spectrum-exposure rate conversion operator G(E) for a portable HPGe detector used for field environmental radiation survey was theoretically developed on the basis of a space distribution function of gamma flux emitted from a disk source and an areal efficiency of the detector. The radiation exposure rates measured using this G(E) and the portable HPGe. detector connected to a portable multichannel analyzer were compared with those measured by a 3' ${\phi}\;{\times}$3' NaI(Tl) scintillation detector with the reported G(E) and a pressurized ionization chamber. A comparison of the three results showed that the result obtained using the HPGe detector was lower than those determined using the NaI(Tl) detector and ionization chamber by 17% to 29%, The difference obtained is close to that reported in literature. The method developed here can be easily applicable to obtain a G(E) factor suitable to any detector for detecting the exposure rate of environmental gamma radiation, since the spectrum-exposure rate conversion operator can be calculated by a hand calculator.

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A Spectroscopic Study on Singlet Oxygen Production from Different Reaction Paths Using Solid Inorganic Peroxides as Starting Materials

  • Li, Qingwei;Chen, Fang;Zhao, Weili;Xu, Mingxiu;Fang, Benjie;Zhang, Yuelong;Duo, Liping;Jin, Yuqi;Sang, Fengting
    • Bulletin of the Korean Chemical Society
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    • v.28 no.10
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    • pp.1656-1660
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    • 2007
  • Using solid inorganic peroxides (including Li2O2, Na2O2, SrO2 and BaO2) as starting materials, three reaction paths for singlet oxygen (1O2) production were developed and studied. Their 1O2 emission spectra in the near- IR region and visible region from these reaction paths were simultaneously recorded by a near-IR sensitive Optical Multichannel Analyzer and a visible sensitive Optical Spectrum Analyzer, respectively. The comparison of their 1O2 emission spectra indicated that: (1) in term of the efficiency for 1O2 production, the gasliquid- solid reaction path (in which Cl2 or HCl and H2O reacted with the solid inorganic peroxides suspension in CCl4) was prior to the gas-solid reaction path (in which Cl2 or HCl reacted with the solid inorganic peroxides suspension in CCl4), but was inferior to the gas-liquid reaction path (in which Cl2 or HCl reacted with the solid inorganic peroxides solution in H2O or D2O); (2) the alkali metal peroxides (such as Li2O2 and Na2O2) was prior to the alkaline earth metal peroxides (such as SrO2 and BaO2) as the solid reactants, and Cl2 was favorable than HCl as the gas reactant in efficiency for 1O2 production in these reaction paths.