• 한국지반공학회논문집
• /
• 제15권5호
• /
• pp.99-110
• /
• 1999

선행하중공법이 실시되는 낙동강 삼각주에서 체계적인 지반조사를 통하여 침하량과 압밀소요 시간이 예측되었으며, 엄선된 각종 계측기를 이용하여 현장계측이 수행되었다. 비교결과, 약20m 두께의 모래층에 대하여 예측침하량은 실측치의 20%에 불과하였다. 이러한 과소평가의 원인은 PBD타입시의 진동, 시간의존적 침하 및 탄성계수의 과대평가 등에서 비롯되었다. 모래층 아래에 위치한 약 20m 두께의 점성토층이 미압밀상태에 있는 것으로 가정하였던 이유 때문에 예측침하량은 실측치에 비하여 약240%까지 과대평가되었다. 그러나 압축곡선을 재구성하고 정규압밀점토를 위한 압밀침하공식을 적용하였을 때 재계산된 침하량은 실측값에 비교적 비슷하였다. 그리고 압밀소요시간은 각종 영향인자로 인하여 실제값에 비하여 약45% 과소평가되었다.

• 한국분말재료학회지
• /
• 제15권6호
• /
• pp.482-488
• /
• 2008

The indentation technique has been one of the most commonly used techniques for the measurement of the mechanical properties of materials due to its experimental ease and speed. Recently, the scope of indentation has been enlarged down to the nanometer range through the development of instrumentations capable of continuously measuring load and displacement. In addition to testing hardness, the elastic modulus of submicron area could be measured from an indentation load-displacement (P-h) curve. In this study, the hardness values of the constituent phases in Ti($C_{0.7}N_{0.3}$)-NbC-Ni cermets were evaluated by nanoindentation. SEM observation of the indented surface was indispensable in order to separate the hardness of each constituent phase since the Ti($C_{0.7}N_{0.3}$)-based cermets have relatively inhomogeneous microstructure. The measured values of hardness using nanoindentation were ${\sim}20$ GPa for hard phase and ${\sim}10$ GPa for binder phase. The effect of NbC addition on hardness was not obvious in this work.

• 폴리머
• /
• 제38권6호
• /
• pp.735-743
• /
• 2014

폴리프로필렌의 분자량 및 분자량 분포를 예측하기 위해 레오메터, 고유점도측정기 및 MI(melt index) 기기 등을 이용하여 유변 물성을 측정하였고, 분자구조해석에는 GPC가 사용되었다. 기존에 사용되어온 동적진동측정을 이용한 교차 모듈러스에서 결정된 유변학적 PI(다분산 지표)와 변형된 Carreau 모델을 이용하여 계산된 분포 폭 매개변수(distribution broadness parameter)를 분자량 분포와의 관계를 비교해보았다. 유변학적 PI의 경우 이론적 근거가 부족하고, 압출에 의해 재 생성된 폴리프로필렌 시료에 대해서는 분자량 분포와 잘 일치하지만 반응기에서 중합된 시료 즉, 분자량 분포가 넓거나 다른 경우 잘 일치하지 않는다는 보고가 지배적인데 비해 분포 폭 매개변수는 폴리프로필렌의 전단담화의 정도를 직접적으로 측정하는 것으로 분자량 분포를 잘 예측할 수 있음을 알았다.

• 대한조선학회논문집
• /
• 제52권2호
• /
• pp.104-109
• /
• 2015

The Korea Research Institute of Ships & Ocean Engineering (KRISO) has an ice tank to make a test environment similar to the real ice in the polar sea in order to carry out model tests. One of the most important task of the ice tank is to generate the model ice to have similar material properties as sea ice. The primary properties of sea ice which influence the ice performance of ice breakers and ice-strengthened vessels traveling in the polar sea are ice thickness, flexural strength, density, modulus of elasticity and crystal structure etc. Among them, since the density of model ice influences the buoyance resistance of ice for the ship model, the accurate measurement of ice density should be used to obtain the accurate analysis results from the model test. In this paper, some existing methods to measure the density of model ice are reviewed and a new one is proposed to measure it accurately and easily as possible. In this study, the measuring system including an UTM and several measuring devices was established to obtain the model ice density. Polyethylene and ice specimens are used for a series of repeatable measurement tests. From the results, it was recognized that both of the displacement method and the weight/weight methods gave the stable and favorable tendency.

• 한국구조물진단유지관리공학회 논문집
• /
• 제25권1호
• /
• pp.103-111
• /
• 2021

보물 제49호 나주 석당간은 성능 저하로 인해 해체 및 복원 공사가 이루어 졌다. 공사시 균열 부위가 보강되고 기울어짐이 개선되었다. 이러한 문화재들의 복원 공사 전·후의 강성 변화를 정량적으로 분석하고 데이터베이스로 구축하여 보강 효과에 대한 예측 또는 평가를 할 수 있는 과학적인 비파괴 검사 방법에 대한 연구가 필요하다. 복원 공사 전·후에 진동실험에 의해 측정된 고유진동수와 탄성계수 정보로부터 구조 시스템의 전체적인 강성을 추정할 수 있는 단순 식을 유도하였고, 활용성을 검토하였다. 제시된 방법으로 중요 문화재의 강성을 정기적으로 조사한다면 구조안전진단 필요 시점 또는 보수, 보강의 필요 시점을 추정하는 자료로 활용될 수 있을 것을 판단된다.

• 한국지반공학회논문집
• /
• 제24권1호
• /
• pp.119-130
• /
• 2008

얕은기초 설계시 이용되는 지반의 물리적 공학적 설계변수들은 고유변동성(inherent variability) 및 측정 오차(measurement error) 등과 같은 여러 가지 요인으로 인하여 불확실성이 필연적으로 내포되어 있다. 본 논문에서는 얕은기초 설계시 기존의 결정론적 방법에서 고려하지 못하는 지반 불확실성 등을 포함한 설계 파라미터의 분산을 고려할 수 있는 확률론적 방법의 신뢰성 설계 사례를 제시하였다. 극한지지력 산정시 확률변수(random variable)인 단위중량, 점착력 및 내부마찰각 그리고 침하량 산정시 탄성계수에 대하여 국내 지반에 대한 적정 확률분포 형태 및 통계적 특성치를 결정하였다. 각 확률변수별로 채택된 분포를 적용하여 지지력과 침하량에 관한 신뢰지수와 파괴확률을 결정하였으며, 목표 신뢰지수 또는 확률에 대한 기초폭을 결정하였다. 얕은기초의 신뢰성 설계에 있어서 정규분포의 일괄적 적용보다는 각 확률변수에 해당하는 적합한 분포형태를 적용, 분석하는 것이 바람직한 것으로 나타났다.

• 한국진공학회:학술대회논문집
• /
• 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
• /
• pp.270-270
• /
• 2016

We fabricated an organic-inorganic nano laminated encapsulation layer using molecular layer deposition (MLD) combined with atomic layer deposition (ALD). The $Al_2O_3$ inorganic layers as an effective single encapsulation layer were deposited at 80 degree C using ALD with alternating surface-saturation reactions of TMA and $H_2O$. A self-assembled organic layers (SAOLs) were fabricated at the same temperature using MLD. MLD and ALD deposition process were performed in the same reaction chamber. The prepared SAOL-$Al_2O_3$ organic-inorganic nano laminate films exhibited good mechanical stability and excellent encapsulation property. The measurement of water vapor transmission rate (WVTR) was performed with Ca test. We controlled thickness-ratio of organic and inorganic layer, and specific ratio showed a lowest WVTR value. Also this encapsulation layer contained very few pin-holes or defects which were linked in whole area by defect test. To apply into real OLEDs panels, we controlled a film stress from tensile to compressive and flexibility defined as an elastic modulus with organic-inorganic ratio. It has shown that OLEDs panel encapsulated with nano laminate layer exhibits better properties than single layer encapsulated in acceleration conditions. These results indicate that the organic-inorganic nano laminate thin films have high potential for flexible display applications.

• Corrosion Science and Technology
• /
• 제13권5호
• /
• pp.170-177
• /
• 2014

Polyurethane coating was designed to give a hydrophobic property on its surface by modifying it with hydroxyl terminated polydimethylsiloxane and then effects of surface hydrophobic tendency, water transport behavior and hence corrosion protectiveness of the modified polyurethane coating were examined using FT-IR/ATR spectroscopy, contact angle measurement and electrochemical impedance test. As results, the surface of polyurethane coating was changed from hydrophilic to hydrophobic property due primarily to a phase separation tendency between polyurethane and modifier by the modification. The phase separation tendency is more appreciable when modified by polydimethylsiloxane with higher content. Water transport behavior of the modified polyurethane coating decreased more in that with higher hydrophobic surface property. The decrease in the impedance modulus ${\mid}Z{\mid}$ at low frequency region in immersion test for polyurethane coatings was associated with the water transport behavior and surface hydrophobic properties of modified polyurethane coatings. The corrosion protectiveness of the modified polyurethane coated carbon steel generally increased with an increase in the modifier content, confirming that corrosion protectiveness of the modified polyurethane coating is well agreed with its water transport behavior.

• 대한기계학회논문집B
• /
• 제33권6호
• /
• pp.389-395
• /
• 2009

A specially designed flat plate was mounted vertically over the axial line in the wind tunnel of the Pusan National University. Strain balances were mounted in the trailing part of the plate to measure the skin friction drag over removable insertions of $0.55{\times}0.25m^2$ size. A set of the insertions was designed and manufactured: 3 mm thick polished metal surface and three compliant surfaces. The compliant surfaces were manufactured of a silicone rubber Silastic$^{(R)}$ S2 (Dow Corning company). To modify the viscoelastic properties of the rubber, its composition was varied: 90% rubber + 10% catalyst (standard), 92.5% + 7.5% (weak), 85% + 15% (strong). Modulus of elasticity and the loss factor were measured accurately for these materials in the frequency range from 40 Hz to 3 kHz. The aging of the materials (variation of their properties) for the period of one year was documented as well. Along with the drag measurement using the strain balance, velocity and pressure were measured for different coating. The strong compliant coating achieved 5% drag reduction within a velocity range $20{\sim}40$ m/s while standard and weak coatings increased drag reduction.

• Macromolecular Research
• /
• 제15권1호
• /
• pp.44-50
• /
• 2007

This study investigated the effect of ultrasound irradiation on the blend of poly(lactic acid) (PLA) and poly(butylene adipate-co-terephthalate) (PBAT). The blends of PLA/PBAT(50/50) (PBAT50) were prepared in a melt mixer with an ultrasonic device attached. Thermal, rheological, and mechanical properties, morphology, and biodegradability of the sonicated blends were analysed. The viscosity of the sonicated blends was increased by the ultrasound irradiation owing to the strong interaction. The morphology of the sonicated blends was significantly dependent on the duration o the ultrasound irradiation. For PBAT50, the phase size reduction was maximized when the blends were ultrasonically irradiated for 30 sec. At longer duration of ultrasound irradiation, the PBAT phase underwent flocculation. Measurement of the tensile properties showed an increased breakage tensile stress and an enhanced Young's modulus when the blends were properly irradiated. This improvement was ascribed to better adhesion between the PLA matrix and the PBAT domain and to better dispersion of the PBAT phase. However, the tensile properties were maximized after excessive energy irradiation, which was ascribed to an emulsifying effect leading to coalescence of the PBAT phase. Impact strength was increased to reach a peak with the ultrasound irradiation, and was higher than the untreated sample for all sonicated samples due to the difference of failure mechanism between the tensile test and the impact test.