• Title/Summary/Keyword: Mo-99

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The Crystal and Molecular Structure of P-toluenesulfonanilide, $C_{13}H_{13}NO_2S$ (P-toluenesulfonanilide, $C_{13}H_{13}NO_2S$의 결정 및 분자구조)

  • 박권일;조성일
    • Korean Journal of Crystallography
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    • v.6 no.1
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    • pp.43-48
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    • 1995
  • The crystal structure of P-toluenesulfonanilide, C13H13NO2S is monoclinic, space group P21/c, a=8.777(1)Å, b=9.784(2)Å, c=15.139(2)Å, β=99.00(1)°, Z=4, V=1284.0(6)Å3, Dc=1.28g/cm33, λ(Mo-Kα)=0.71069Å, μ=2.3cm-1, F(000)=520, Temperature : 293±3K, R=0.038 for 711 Fo<3.0σ unique observed reflection. The structure was determuned by direct method and refined by full-matrix least squares refinement. Two benzene rings have the dihedral angle of 68.4°. Moleculs are accumulated according to the c axis with two fold screw and contacted by van der Walls force.

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Assessment of inlay ceramic restorations manufactured using the hot-pressing method (열 가압 방식을 사용하여 제작된 인레이 세라믹 수복물의 적합도 평가)

  • Lee, Beom-Il;You, Seung-Gyu;You, Seung-Min;Park, Dong-In;Kim, Ji-Hwan
    • Journal of Technologic Dentistry
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    • v.42 no.1
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    • pp.9-16
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    • 2020
  • Purpose: The purpose of this study was to compare the marginal and internal fit of lithium disilicate ceramic inlay produced by heat pressing that inlay pattern made by subtractive manufacturing and additive manufacturing method. Methods: A mandibular lower first molar that mesial occlusal cavity (MO cavity) die was prepared. After fabricating an epoxy resin model using a silicone impression material, epoxy resin die was scanned with a dental model scanner to design an MO cavity inlay. The designed STL pile was used to fabricate wax patterns and resin patterns, and then lithium disilicate ceramic inlays were fabricated using hot-press method. For the measurement of the marginal and internal gap of the lithium disilicate, silicone replica method was applied, and gap was measured through an optical microscope (x 80). Data were tested for significant differences using the Mann-Whitney Utest. Results: The marginal fit was 103.56±9.92㎛ in the MIL-IN group and 81.57±9.33㎛ in the SLA-IN group, with a significant difference found between the two groups (p<0.05). The internal fit was 120.99±17.52㎛ in the MIL-IN group and 99.18±6.65㎛ in the SLA-IN group, with a significant difference found between the two groups (p<0.05). Conclusion: It is clinically more appropriate to apply the additive manufacturing than subtractive manufacturing method in producing lithium disilicate inlay using CAD/CAM system.

Separation and Simulation for Carbon Dioxide from Flaring Gas Using Polysulfone Hollow Fiber Membrane (폴리술폰 중공사막을 이용한 Flaring Gas에서의 이산화탄소 분리 및 전산모사)

  • Lim, Joo Hwan;Lee, Chung Seop;Kim, Hack Eun;Bae, Myong Won;Mo, Yong Gi;Ha, Seong Yong
    • Membrane Journal
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    • v.25 no.2
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    • pp.99-106
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    • 2015
  • Polysulfone (PSF) hollow fiber membrane was prepared to separate $CO_2$ from the flaring gas. Fabricated PSF membrane system was fulfilled under 1 stage, 2 stage membrane process and simulation in order to confirm the operating condition for 99% of $CH_4$ and 1% of $CO_2$ concentration. Also, $25Nm^3/h$ bench scale $CO_2$ separation membrane system was operated under 1% of $CO_2$ concentration during 100 hr, and $CH_4$ recovery ratio was 98%.

A New Single Mini-gerbera 'Sun Cap' with Bi-color for Cut Flower (홑꽃 소륜 복색 절화용 거베라 '썬캡' 육성)

  • Chung, Yong-Mo;Hwang, Ju-Chean;Chin, Young-Don;Kim, Su-Kyeong;Ro, Chi-Woong;Yi, Young-Byung;Kwon, Oh-Chang
    • Horticultural Science & Technology
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    • v.29 no.1
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    • pp.77-80
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    • 2011
  • A new bi-color mini gerbera (Gerbera hybrida Hort.) 'Sun Cap' was developed from a cross of '99-ga-2' and '99-na-3-1' followed by seedling and line selections at the Flower Research Institute, Gyeongnam Agricultural Research and Extension Services (ARES) in 2007. Characteristic tests were conducted three times from 2004 to 2007. 'Sun Cap' has single type in good harmony with bi-color (Red/Yellow, RHS 45-B/9-A) ray floret and green center. It has good stable flower shape and strong peduncle. Its vase life was 13.5 days. The average yield of 'Sun Cap' was 102.6 flowers per plant a year in greenhouse. Yield trials were carried out from 2004 to 2007. This cultivar was registered for commercialization in 2009. 'Sun Cap' would be cultured under greenhouse condition in Korea.

Diagnostic Utility of Tc-99m DISIDA Hepatobiliary Scintigraphy in the Diagnosis of Biliary Atresia (담도폐쇄증 진단에서 DISIDA 간담도주사의 진단적 의의)

  • Lee, Byeong-Seon;Choi, Bo-Hwa;Kim, Kyung-Mo;Kim, Jae-Seung;Moon, Dae-Hyeok
    • Pediatric Gastroenterology, Hepatology & Nutrition
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    • v.3 no.1
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    • pp.63-67
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    • 2000
  • Purpose: Biliary atresia, one of the major causes of neonatal cholestais, is an idiopathic, serious disorder, affecting the newborn that results in complete obstruction of biliary tract. Successful reestablishment of bile flow is dependent on early surgical intervention, early diagnosis is imperative. The authors evaluate the utility of Tc-99m-labeled diisoprpyliminodiacetic acid (DISIDA) hepatobiliary scintigraphy in the diagnosis of biliary atresia. Methods: From January, 1995 to August, 1999, total 60 patients with neonatal cholestasis underwent Tc-99m DISIDA hepatobiliary scintigraphy at Asan Medical Center. Results: The undelying causes of neonatal cholestasis were biliary atresia in 14, neonatal hepatitis in 33, intrahepatic bile duct paucity in 9, and total parenteral nutrition induced cholestasis in 4. All patient with biliary atresia were interpreted correctely in DISIDA hepatobiliary scintigraphy, showing 100% sensitivity. Of the 46 patients with neonatal hepatitis and other causes, 37 patients had intestinal radioactivity showing 80% specificity. Conclusion: Visualization of DISIDA in the intestinal tract indicates patency of the biliary ducts and excludes the diagnosis of biliary atresia. But the absence of intestinal excretion on the DISIDA hepatobiliary scintigraphy dose not necessarily indicate biliary atresia.

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Recovery of phosphoric acid from the waste acids in semiconductor manufacturing process (반도체 제조공정에서 발생하는 혼산폐액으로부터 고순도 인산 회수)

  • Park, Sung-Kook;Roh, Yu-Mi;Lee, Sang-Gil;Kim, Ju-Yup;Shin, Chang-Hoon;Ahn, Jae-Woo
    • Proceedings of the Korean Institute of Resources Recycling Conference
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    • 2006.05a
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    • pp.90-94
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    • 2006
  • The waste solution discharged from the LCD manufacturing process contains acids like nitric, acetic and phosphoric acid and metal ions such as Al, Mo and other impurities. It is important to removal of impurities to tess than 1ppm in phosphoric acid to reuse as an etchant because the residual impurities even in sub-ppm concentration in semiconductor materials play a major role on the electronic properties. In this study, we have been clearly established that a mixed system of solvent extraction, diffusion dialysis and ion-exchange technique, which made individually the most of characteristics is developed to commercialize in an efficient system for recovering the high-purity phosphoric acid. By applying vacuum evaporation, the yield of the process are almost 99% removal of nitric acid and acetic acid was achieved. And by applying the solvent extraction method with tri-octyl phosphate(TOP) as an extractant, the removal of acetic and nitric acid from the acid mixture was achieved effectively at the ratio O/A=1/3 with four stages and the stripping of nitric acid from organic phase is attained at a ration of O/A=1 with six stages by distilled water. About 97% and 76% removal of Al and Mo were achieved by diffusion dialysis. Essentially complete less than 1ppm removal of Al, Mo by using ion exchange ion resin and purification of the phosphoric acid was obtain.

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MINERAL CONCENTRATION IN RICE STRAW AND SOIL IN KYONGBUK PROVINCE, KOREA

  • Ramirez, C.E.;Kumagai, H.;Hosoi, E.;Yano, F.;Yano, H.;Jung, K.K.;Kim, S.W.
    • Asian-Australasian Journal of Animal Sciences
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    • v.7 no.1
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    • pp.125-129
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    • 1994
  • A field survey was carried out in Korea to assess the mineral composition of rice straw since it is a cheap and available cattle feedstuff. Forage and soil samples were collected in 4 localities in the Kyongbuk province. Soil analysis were also carried out in order to establish the relationships between soil composition and mineral content in the rice straw. Based on NRC tables, the rice straw samples provided adequate amounts of Mg, Ca, K, S, Mo, Mn and Zn. Percentages of samples deficient in P, Na, Cu and Se were 83, 50, 67 and 83 respectively. Soil samples, whose mean pH was 5.8 and mean organic matter content was 3.99%, were comparatively acidic and had high organic matter content. They also had high amounts of extractable Fe and Mn. Correlation coefficients between mineral content in soil and rice straw were low, i.e., 0.42 for Me (p < 0.05), and 0.37 for Mo (p < 0.05). The low or nonexistent correlation between soil and forage composition indicates the difficulty of establishing appropriate methods of mineral availability to the plants.

Analysis of the Dynamic Balance Recovery Ability by External Perturbation in the Elderly

  • Park, Da Won;Koh, Kyung;Park, Yang Sun;Shim, Jae Kun
    • Korean Journal of Applied Biomechanics
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    • v.27 no.3
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    • pp.205-210
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    • 2017
  • Objective: The aim of the study was to investigate the age-related ability of dynamic balance recovery through perturbation response during standing. Method: Six older and 6 younger adults participated in this study. External perturbation during standing as pulling force applied at the pelvic level in the anterior direction was provided to the subject. The margin of stability was quantified as a measure of postural stability or dynamic balance recovery, and using principal component analysis (PCA), the regularity of the margin of stability (MoS) was calculated. Results: Our results showed that in the older adult group, 60.99% and 28.63% of the total variance were captured using the first and second principal components (PCs), respectively, and in the younger adult group, 81.95% and 10.71% of the total variance were captured using the first and second PCs, respectively. Conclusion: Ninety percent of the total variance captured using the first two PCs indicates that the older adults had decreased regularity of the MoS than the younger adults. Thus, the results of the present study suggest that aging is associated with non-regularity of dynamic postural stability.

A Study on the Use of "Concept" or the Word "Kyoung" (경관개념어 사용방향 설정(1) -송강, 노계, 고산의 시가에 나타나는 '景'을 중심으로)

  • 정하광
    • Journal of the Korean Institute of Landscape Architecture
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    • v.19 no.1
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    • pp.99-121
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    • 1991
  • A purpose of this study is to identify the concept formation and classify the diverse concepts which related to Kyoung(景) in the Classical Korean Poems(Chong, Chol(鄭澈, 1536-1593), Pak, Inno(朴仁老, 1561-1642), Yun Sondo(尹善道, 1587-1671) on the Yi dynasty period and to construct the direction of the use of that concepts in the future. The results were as follows ; The type of landscape concept was 9 types and had the following frequencies in order ; Kyoung(景)(3), Pung-Kyoung(風景)(2), Kyoung-Chi(景致)(2), Yeo-Kyoung(麗景), Cheong-Kyoung(淸景), Jin-Kyoung(眞景)(1), Mo-Kyoung(暮景)(1), Ka-Kyoung(佳景)(1), Kyoung-Mul(景物). Types of landscape concepts in Yi dynasty period were classified into 9 according to the many characteristics ; personal situations, faith, religion, confucianism in the specific time of Yi dynasty. The most popular type of landscape concepts in general was Kyoung(景). The word, "Pung-Kyoung(風景)" was used in expressing personal thoughts and feelings in one's recollection in terms of landscape elements. The word, "Mo-Kyoung(暮 景)" was used in expressing specific time and the dejection in one's heart in that time. The words, "yeo-Kyoung(麗景)" and "Ka-Kyoung(佳 景)" was used in expressing the landscape elements. The nine concepts had a grest deal to do with defining and perpetuating a personal characteristics, the place and landscape elements, and a society's character in the Yi dynasty period.ty's character in the Yi dynasty period.

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In-Process Evaluation of Surface Characteristics in Machining

  • Jang, Dong-Young;Hsiao, Alex
    • Tribology and Lubricants
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    • v.11 no.5
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    • pp.99-107
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    • 1995
  • This paper reported research results to develop an algorithm of on-lin evaluation of surface profiles and roughness generated by turning. The developed module consisted of computer simulation of surface profiles using mechanism of cutting mark formation and cutting vibrations, and online measurement of cutting vibrations. The relative cutting vibrations between tool and worpkiece were measured through an inductance pickup at the rate of one sample per rotation of the workpiece. The sampling process was monitored using an encoder to avoid conceling out the phase lag between waves. The digital cutting signals from the Analog-to-Digital converter were transferred to the simulation module of surface profile where the surface profiles were generated. The developed algorithm or surface generation in a hard turning was analyzed through computer simulations to consider the stochastic and dynamic nature of cutting process. Cutting tests were performed using AISI 304 Stainless Steel and carbide inserts in practical range of cutting conditions. Experimental results showed good correlation between the surface profiles and roughness obtained using the developed algorithm and the surface texture measured using a surface profilemeter. The research provided the feasibility to monitor surface characteristics during tribelogical tests considering wear effect on surface texture in machining.