• 제목/요약/키워드: Mixing firing

검색결과 91건 처리시간 0.024초

감광성 탄소나노튜브 페이스트의 조성과 열처리가 전계방출 특성에 미치는 영향 (Effect of Photosensitive Carbon Nanotube Paste on Field Emission Properties)

  • 오정섭;김대준;정진우;송윤호;조영래
    • 한국재료학회지
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    • 제16권9호
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    • pp.550-556
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    • 2006
  • Photosensitive carbon nanotube (CNT) pastes are explored to develop a CNT field emitter for field emission display (FED) application. We formulated a photosensitive paste including multi-walled CNTs (MWNTs) for screen printing. The photosensitive CNT paste was synthesized by mixing of MWNTs, inorganic fillers (nano metal), organic vehicle, monomers and photo initiator. The CNT paste films were patterned by using backside exposure technique. The CNTs were strongly fixed on a cathode by formation of carbon residue during firing process. For the CNT emitters, current-voltage(I-V) characteristics and images of field emission were evaluated. The emission properties of CNT emitters are dependent on the paste composition. A turn-on electric field for the CNT field emitters is measured to be 1 V/$\mu$m. Additionally, the effect of heat treatment parameter on field emission properties was discussed. The newly formulated photosensitive CNT paste can be potentially applicable to highly reliable CNT field emitters.

다성분계 산화물의 요업재료 제조를 위한 석유 증발 건조 방법 (Hot Petroleum Drying Method to the Preparation of Multicomponent Oxide Ceramic Material)

  • 변수일
    • 한국세라믹학회지
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    • 제14권3호
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    • pp.163-168
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    • 1977
  • As a wet chemical drying process "hot petroleum drying method" was applied and developed for preparing uniformly fine oxide powder with high purity and sinterreactivity. Using this method solution of sulfates was dried in hot petroleum bath (~17$0^{\circ}C$) to sulfate powder from which corresponding mullite doped by Fe3+ ion was formed. Particle size, shape, decomposition by heat, and phase identification of sulfate andoxide powders determined by DTA, TGA, X-ray diffraction, analysis and electron microscopy: sulfate powder prepared by this drying method is an intimate mixture of the amorphous form of uniformly and finely distributed spherical particles (0.05-0.1$\mu$). Mullitization with the sulfate powder occurs at 110$0^{\circ}C$ in air. The morphology of mullite particle made by firing the sulfate powder at 135$0^{\circ}C$ in oxygen atmosphere is granular of 0.1-0.3$\mu$ in size. This drying process proved to be a very effective method for preparing fine, homogeneous, and highly sinterreactive multicomponent oxide powder without conventional ceramic process of mixing, milling, and granulating. This process can be also applied for preparing electronic ceramic materials which are requisite for high purity and homogeneity.mogeneity.

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Al-doped Uvarovite 안료의 합성과 특성 (Synthesis and Characterization of Al-doped Uvarovite Green Pigments)

  • 서성규;이병하
    • 한국세라믹학회지
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    • 제47권6호
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    • pp.608-612
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    • 2010
  • Uvarovite Garnet is green pigment prepared by using $Cr_2O_3$, CaO and $SiO_2$ which are widely used in ceramic industry. The synthesis of above pigment was carried out by mixing $K_2Cr_2O_7$, $SiO_2$ and $CaCO_3$ as formulated and then firing at $1000{\sim}1200^{\circ}C$. To investigate the optimum synthesis condition of the Uvarovite Garnet. it was prepared by using CaO to replace $CaCO_3$, $CaF_2$ and $CaCl_2$. To get green brighter color, $Al^{3+}$ was substituted for $Cr^{3+}$. They were characterized by X-ray diffraction, UV-Vis spectroscopy, Raman spectroscopy and SEM analysis. When the pigments were applied to lime glazes (6 wt%), color parameters of Uvarovite Garnet showed the $L^*$=40.99, $a^*$=-16.23 and $b^*$=17.04.

중금속으로 오염된 토양 정화에 있어 폐 소뼈 첨가제의 영향 (Stabilization of Heavy Metal Contaminated Soil Amended with Waste Cow Bone)

  • 임정현;최명찬;문덕현;김지형
    • 한국환경과학회지
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    • 제19권2호
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    • pp.255-260
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    • 2010
  • A stabilization/solidification (S/S) process for lead (Pb) contaminated soils was evaluated using waste cow bone containing apatite like compounds. Soil samples obtained form firing range were treated with waste cow bone. The effectiveness of stabilization was evaluated based on the Korean Standard Leaching Test (KSLT) and soil pH. The leached concentration reduced with increased in dose of waste cow bone. Overall, the KSLT results showed that Pb concentration in soils are significantly affected by amount of waste cow bone. When soil amended with 20 % of waste cow bone, less than 0.1 mg/kg was leached, and soil pH was increased from 6.5 to 8.4. Same results were obtained when finer waste cow bone was applied. The reachable concentration of Pb in soil showed in inversely proportional to solid/liquid ratio. Aging periods indicate improving mix design was applied. Relatively high lead concentrations was observed at the first 1 days, however leaching profile are reduced significantly over time for all mix designs.

액체로켓엔진의 내부 벽면 근처에서의 추진제 혼합비 변화의 영향에 대한 연구 (Influence of Propellant Mixture ]Ratio Variation near Chamber Wall)

  • 한풍규;장행수;조용호;김경호
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2002년도 학술대회지
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    • pp.255-258
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    • 2002
  • Liquid rocket engines using liquefied natural gas (LNG) or methane as a fuel is known to have several good characteristics, such as high specific impulse compared to other hydrocarbon fuels, environment-friendly exhaust gas, low production cost, and re-usability with low soot generation in the cooling channel. In this study, experimental combustion chambers capable of using LNC and $CH_{4}$ are being researched through experimental firing tests, and within easy range of eyes' inspection, there are the periodical existence of soot or discoloration in the chamber wall surface. This result means that mixture ratio of oxidizer and fuel fluctuates periodically between outer-row injectors in the mixing head in the circumferential direction. Therefore, based on this phenomenon, the variation of mixture ratio near the chamber wall caused by the spill pattern of a shear coaxial injector was analyzed quantitatively and the thermal heat flux Into the cooling channel is modified. Then, the calculated and modified results are compared with the measured ones.

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액체로켓엔진에서의 상온 기체를 이용한 라이너 막냉각 특성 연구 (A Study on Film Cooling Characteristics of Liner in Liquid Rocket Engine)

  • 전준수;이양석;이동형;김유;고영성;정해승
    • 한국추진공학회:학술대회논문집
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    • 한국추진공학회 2007년도 제29회 추계학술대회논문집
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    • pp.170-173
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    • 2007
  • 본 연구에서는 액체로켓엔진 내부에 라이너를 설치하고 기체 질소를 이용한 막냉각 방법을 사용하여, 라이너의 막냉각 특성을 살펴보았다. 고온 가스는 액체로켓 연소가스와 액체질소를 혼합하여 사용하였다. 기존의 액체로켓엔진 시험 설비에 추가적으로 라이너 냉각 기체를 공급 설비를 구축하였으며, 라이너 및 냉각 기체 공급부를 제작하였다. 10초 연소 실험을 통해 라이너 내부 고온 가스의 온도와 라이너 외부 벽면 온도를 측정하였으며, 기체 질소에 의한 라이너 냉각 특성을 확인하였다.

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나노입자를 첨가한 전극용 무연 silver 페이스트의 제조 (Preparation of Lead-free Silver Paste with Nanoparticles for Electrode)

  • 박성현;박근주;장우양;이종국
    • 열처리공학회지
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    • 제19권4호
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    • pp.219-224
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    • 2006
  • Silver paste with low sintered temperature has been developed in order to apply electronic parts, such as bus electrode, address electrode in PDP (Plasma Display Panel) with large screen area. In this study, nano-sized silver particles with 10-30 nm were synthesized from silver nitrate ($AgNO_3$) solution by chemical reduction method and silver paste with low sintered temperature was prepared by mixing silver nanoparticles, conventional silver powder with the particle size 1.6 um and Pb-free frit. Conductive thick film from silver paste was fabricated by screen printing on alumina substrate. After firing at $540^{\circ}C$, the cross section and surface morphology of the thick films were analyzed by FE-SEM. Also, the sheet resistivity of the fired thick films was measured using the four-point technique.

ICP 광원 시스템의 Ne:Xe 및 Ne:Ar 혼합가스의 전자온도 및 전자밀도 특성 (The Electron Temperature and Density Properties of Mixed Gases in ICP Lighting System : (Ne:Xe, Ne:Ar))

  • 이종찬;최용성;박대희;최기승
    • 대한전기학회논문지:전기물성ㆍ응용부문C
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    • 제55권3호
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    • pp.156-160
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    • 2006
  • In whole world consciousness of environment maintenance have increased very quickly for the end of the 20th century. To use and disuse toxic substances have been controled at the field of industry. Also the field of lighting source belong to environmental control. And in the future the control will be strong. In radiational mechanism of fluorescence lamp mercury is the worst environmental problem and root. In the mercury free lighting source system the Xe gas lamp is one type. And the Ne:Xe and Ne:Ar mixed gas lamp improve firing voltage of Xe gas lamp. Purpose of this study is to understand ideal mixing-ratio of Ne:Xe and Ne:Ar gas by electron temperature and electron density for mercury free lamp. Before ICP was designed, basic parameters of plasma, which are electron temperature and electron density, were measured and calculated by single-Langmuir probe. Property of electron temperature and electron density were confirmed by changing ratio of Ne:Xe and Ne:Ar.

소형 연소장치를 이용한 음식폐기물 연소 특성 연구 (A Study on the Combustion Characteristics of Food Waste Using the Experimental Apparatus for Combustibility)

  • 채종성;양승재;김석완;이재희;엄태인
    • 신재생에너지
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    • 제16권2호
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    • pp.47-53
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    • 2020
  • The amount of food waste and its water content depends on both the season and region. In particular, the water content typically varies between 73.8 wt.% and 83.3 wt.%, depending on the proportion of vegetables. Current food waste drying technologies are capable of reducing the water content to less than 10 wt.%, while increasing the heating value. Ongoing studies aim to utilize dried food waste as fuel. Food waste can be used to produce solid refuse fuel (SRF) by mixing it with various solid fuels or other types of waste. The analysis of specimens is very important when considering the direct combustion of food waste or its co-firing with solid fuels. In this study, the weight reduction of specimens after burning them in a small combustor, and compared with the results of thermogravimetric analysis (TGA). The concentration of various chemicals was also measured to define the characteristics of waste generation. Performed proximate analysis, elemental analysis, TGA, combustion experiment, the heating value, and derivative thermogravimetry (DTG).

ICP 광원 시스템의 Ne:Xe, Ne:Ar 혼합가스의 단일탐침법을 이용한 플라즈마 진단 (Plasma Diagnosis of Ne:Xe, Ne:Ar Mixed Gases by Single Langmuir Probe in Inductively Coupled Plasma Light Source System)

  • 최용성;이우기;;이경섭;이상헌
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2006년도 영호남 합동 학술대회 및 춘계학술대회 논문집 센서 박막 기술교육
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    • pp.91-95
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    • 2006
  • In whole world consciousness of environment maintenance have increased very quickly for the end of the 20th century. To use and disuse toxic substances have been controled at the field of industry. Also the field of lighting source belong to environmental control. And in the future the control will be strong. In radiational mechanism of fluorescence lamp mechanism is the worst environmental problem. In radiational mechanism of fluorescence lamp mercury is the worst environmental problem root. In the mercury free lighting source system the Xe gas lamp is one type. And the Ne:Xe mixing gas lamp improvements firing voltage of Xe gas lamp. Purpose and subject of this study are understand, efficiency, ideal of Ne:Xe plasma which mercury free lamp. Before ICP was designed, basic parameters of plasma, which are electron temperature and electron density, were measured and calculated by Langmuir probe data. Property of electron temperature and electron density were confirmed by changing ratio of Ne:Xe.

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