• 제목/요약/키워드: Mixed preparation

검색결과 604건 처리시간 0.029초

Hybrid Plasma Processing에 의한 Si3N4-SiC계 미립자의 합성과정 제어 (Process Control for the Synthesis of Ultrafine Si3N4-SiC Powders by the Hybrid Plasma Processing)

  • 이형직
    • 한국세라믹학회지
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    • 제29권9호
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    • pp.681-688
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    • 1992
  • Ultrafine Si3N4 and Si3N4+SiC mixed powders were synthesized through thermal plasma chemical vapor deposition(CVD) using a hybrid plasma, which was characterized by the supersposition of a radio-frequency plasma and arc jet. The reactant SiCl4 was injected into an arc jet and completely decomposed in a hybrid plasma, and the second reactant CH4 and/or NH3 mixed with H2 were injected into the tail flame through double stage ring slits. In the case of ultrafine Si3N4 powder synthesis, reaction efficiency increased significantly by double stage injection compared to single stage one, although crystallizing behaviors depended upon injection speed of reactive quenching gas (NH3+N2) and injection method. For the preparation of Si2N4+SiC mixed powders, N/C composition ratio could be controlled by regulating the injection speed of NH3 and/or CH4 reactant and H2 quenching gas mixtures as well as by adjusting the reaction space.

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백색광을 발하는 면발광소자의 휘도 및 표면특성 (Luminance and Surface Properties of P-ELD Emitted White Light)

  • 박수길;조성렬;손원근;박대희;이주성
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1998년도 춘계학술대회 논문집
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    • pp.403-406
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    • 1998
  • Electroluminescence(EL) come from the light emission obtained by electrical excitation energy passing through a phosphor layer under applied high electrical field. The preparation and characterizations of light emitting ACPEL(alternating-current powder electroluminescent) cell based on two kinds of phosphor mixed ZnS:Mn, Cu and ZnS:Cu phosphor. Basic structure is ITO/Mixed Phosphor/insulator/Al sheet, each layer was mixed by binder, which concentration 11p for phosphor, 8p for insulator. Dielectric properties was investigated first and emission properties of P-LED based on ZnS:Mn,Cu/ZnS:Cu,Br mixture. Emission spectra exhibits two kinds of main peaks at 100V, 1kHz sinusoidal excitation.

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과채쥬스 제조를 위한 혼합조건의 선정 (Selection of Mixing Ratio for Preparation of Mixed Vegetable Juice)

  • 이규희;고영수;최희숙;김우정
    • 한국식품조리과학회지
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    • 제11권2호
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    • pp.113-118
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    • 1995
  • A preferable mixing ratio of a six-vegetable juice was suggested in this study. The vegetables used for preparation of mixed vegetable juice were carrot(Ct), cabbage(Cg), pear(Pr), cucumber(Cr), celery (Cy) and dongchimi(Di). The characteristics of pH, titratible acidity, reducing sugar, turbidity, solids, color and acceptability were compared to determine the mixing ratio. The vegetables showed a wide ranHe of pH of 3.70-6.01, acidity of 28.92 uv~74.40 nd and reducing sugar of 1.20ft~ 12.69fo. Celery juice showed the higest suspension stability and "b" value and the lowest values in Hunter "L" and "a" values among the 6 vegetable juice. The preferable mixing ratio of two-vegetable juice selected were Ct-Di(1 : 4), Cg-Pr(1 : 3) and Cr-Cy(3 : 1). From the various ratio of the three of biary mixtures of Cg-Pr(1 : 3): Ct-Di(1 : 4): Cr-Sy(3 : 1), two ratio of 5.0 : 2.5 2.5(V-6A) and 6.0 : 2.0 : 2.0(V-6B) were suggested as the most prefered six-vegetable juice. Pear, dongchimi and cucumber were found to be influential on the preference. The pH and titratible acidity of the two juices with different ratios were in the range of 4.92~4.98 and 36.g∼37.4 ml, respectively.

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속경화·저비중 SMC 제조에 관한 연구 (A Study on Preparation of Fast Cure and Low Density SMC)

  • 김은경;이영철;황석호
    • 공업화학
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    • 제7권3호
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    • pp.511-517
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    • 1996
  • 본 논문에서는 속경화 SMC와 저비중 SMC를 제조하기 위한 경화시스템과 배합시스템을 연구하였다. 속경화 SMC를 제조하기 위한 경화시스템으로는 혼합개시제를 사용한 시스템과 촉진제를 사용한 시스템으로 나누어 실험하였고, 저비중용 SMC는 glass micro-baloon(GMB)을 충진제로 사용하여 실험하였다. 본실험에서는 두시스템으로 제조된 시편으로 경화 거동, 기계적 성질, 물리적 성질 등을 측정하였다. 속경화용 SMC 시편의 경우는 혼합개시제의 양 및 촉진제의 양이 증가할수록 경화 속도는 증가하였으나 SMC 성형 시편의 물성은 큰 변화를 보이지 않았다. 저비중용 SMC에서는 GMB의 양이 증가함에 따라 비중이 감소하였으며, 물성치에서도 약간의 감소를 보였다.

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폴리페놀 및 DPPH 라디칼 소거활성 관점에서의 복합갈근탕 및 단미혼합갈근탕의 동등성 (Equivalence of Mixed and Individual Preparation of Galgeun-tang in terms of Polyphenol Contents and DPPH Radical Scavenging Activity)

  • 김동선;엄영란;양민철;윤나영;정상원;이재훈;마진열
    • 약학회지
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    • 제55권1호
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    • pp.45-48
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    • 2011
  • Traditional medicines usually use combinational formula that are prepared by mixing different varieties of medicinal herbs and boiling them in water to yield a decoction. In recent years a modified method has been proposed and practiced wherein the individual herbs are boiled with water separately and later these extracts are mixed together for use. We attempted to evaluate their equivalence in terms of its polyphenol contents and DPPH radical scavenging activity. The polyphenol contents as well as the DPPH radical scavenging activities were very similar to each other.

혼합제제중 Methylephedrine Hydrochloride와 Ephedrine Hydrochloride의 분리정량에 관한 연구 (Study on Isolative Determination Methylephedrine Hydrochloride and Ephedrine Hydrochloride in the Mixed Preparation)

  • 고인석
    • 생약학회지
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    • 제1권3호
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    • pp.93-99
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    • 1970
  • There have been reported by several workers for the isolation and determination of the amine derivatives as Metbylephedrine Hydrochloride and Ephedrine Hydrochloride adopting neutralization method, steam distillation method, non-aqous titration method, ion-exchange resin method, titration method after acetylation, colorimetric method, gravimetric method, iodine titration method and gas chromatography. Those methods mentioned in above, can be practically applied for the sample which is not mixed one mith the other amine compounds. Presently, it has not shown on the isolative determination of the mixed sample of amine derivatives. In this paper, it is discussed on the isolative determination of Methylephedrine Hydrochloride as the tertiary amine compound and Ephedrine Hydrochloride as the secondary amine compound. According to the results of the experiment, it could be summarized as follows: 1. There is no time-variation on the color reaction of Methylephedrine Hydrochloride and Ephedrine Hydrochloride with the color reagent, bromcresolgreen. And Methylephedrine Hydrochloride and Ephedrine Hydrochloride, respectively, can be determined spectrophotometrically by means oft his color reaction. 2. For the isolation of Methylephedrine Hydrochloride and Ephedrine Hydrochloride from the mixed sample, Methylephedrine Hydrochloride can be eluted by chloroform, while Ephedrine Hydrochloride by the mixed solvent of chloroform and ethylalcohol (2:1), from the celite column adsorbed at pH6.4 followed by extraction with ether undersodium hydroxide alkali re action. 3. When the sample is mixed with quinine hydrochloride, dihydrocodeine bitartate, and noscapine, these mixed compounds can be eliminated by means of stram distillation. 4. When the sample is mixed with chlorpheniramine maleate, dextromethorphan hydrobromide and diphenhydramine hydrochloride, the mixed compounds can be eliminated by means of steam distillation and celite adsorption column chromatography, In conclusion, the isolative determination method for Methylephedrine Hydrochloride and Ephedrine Hydrochloride studied in this paper, indicates with the excellent reproducibility and accuracy.

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한지형 잔디의 피복 율과 생육 증진을 위한 유기질비료 제제의 살포 (Application of Organic Fertilizer Preparation for Increasing of Coverage and Growth of Cool Season Turfgrasses)

  • 구준학;허혁재;김양선;윤정호;장석원;전종엽;장태현
    • Weed & Turfgrass Science
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    • 제4권3호
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    • pp.268-277
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    • 2015
  • 유기질비료의 원료를 이용하여 한지형 잔디의 종자 파종후 피복율, 생육 및 질의 증진을 위한 유지질비료 제제를 개발하였다. 개발 제제는 한지형 잔디의 생육에 필수적인 무기영양소와 유기물을 함유하고 있다. 유기질비료로 개발한 제제는 4종류로 creeping bentgrass "Penn-A1" 품종과 Kentucky bluegrass 혼합품종(Midnight 33%, Moonlight 33%와 Prosperity 33%)의 종자를 파종 후 50일에 1회 토양 시비로 시험하였다. creeping bentgrass와 Kentucky bluegrass의 피복율, 생장(생장지수) 및 잔디의 질은 2013년 가을부터 2014년 봄철기간 동안 경시적으로 평가를 하였다. 개발제제의 파종 후 1회 토양살포로 잔디 피복율, 잔디 엽색, 엽록소 함량 및 생장에서 통계적인 유의성의 차이를 보였다. creeping bentgrass와 Kentucky bluegrass의 피복율, 엽록소 함량, 잔디 엽색 및 생장은 봄철 6회 조사까지 통계적으로 유의성 있게 증가하였다. 이 결과에 의하면 일부 개발 제제의 사용은 한자형 잔디의 뗏장잔디의 생산과 잔디관리에 도움의 줄 것으로 생각한다.

개구리 좌골신경에 대한 Buprenorphine의 작용 양상 (Agonist-Antagonist Effects of Buprenorphine on Action Potentials of Frog Sciatic Nerve Fibers)

  • 이종화
    • 대한약리학회지
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    • 제25권1호
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    • pp.23-30
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    • 1989
  • 함께 투여되는 마약성진통제에 따라 효능제 또는 길항제(mixed agonist-antagonist)로 작용하는 buprenorphine을 사용하여 개구리 좌골신경에 존재하는 아편수용체의 성질을 검토하였다. 실험은 sucrose-gap apparatus를 사용하여 활동전압에 대한 영향을 관찰하였으며 약물의 상호작용을 검토하고자 meperidine 또는 naloxone을 사용하여 다음과 같은 결과를 얻었다. 1) Buprenorphine은 현저하게 개구리 좌골신경의 활동전압을 저하시켰다. 2) 두 개의 최고작용농도를 보였는데 저농도에서는 $10^{-8}\;M$, 또 고농도에서는 $10^{-4}\;M$에서 현저하게 작용을 나타내었다. 3) Buprenorphine은 meperidine의 활동전압 저하작용을 의의있게 억제하였다. 4) Naloxone에 의하여 Buprenorphine의 저하 작용이 억제되었다. 위의 실험결과로 Buprenorphine은 순수 마약성진통제의 작용을 억제하여 차단제로 작용하는 한편 또한 효능제로 활동전압을 의의있게 억제하였다. 이로써 개구리 좌골신경에 있는 아편수용체는 세포막에 또는 세포막 주위에서 $Na^+-Channel$이 활성화되는 데 중요한 역할을 하는 것으로 간주되며 이 수용체는 또한 Naloxone에 매우 민감한 반응을 나타낸다.

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마요네즈 제조시 품질특성에 미치는 저에루신산 유채유 혼합의 영향 (The Effect of Low Erucic Acid Rapeseed Oil for the Preparation of Mayonnaise on Quality Characteristics)

  • 김재욱;손양도;홍기주;유무영;정계환;허종화
    • 한국식품과학회지
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    • 제27권3호
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    • pp.298-302
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    • 1995
  • 본 연구는 상업적인 마요네즈 제조시의 원료유로서 저에루신산 유채유의 사용가능성을 알아보기 위하여 실시하였다. 일반적으로 사용되는 식물유인 대두유에 저에루신산 유채유를 일정한 비율로 섞은 혼합유 및 이들 혼합유를 사용한 마요네즈를 제조하고 이들의 품질특성을 비교하였다. 식물유 자체의 산화안정성을 랜시매트법에 의한 유도기간으로 비교한 결과 유채유가 대두유보다 길었으며, 대두유와 유채유를 혼합하였을 때는 유채유의 비율이 높을수록 유도기간이 긴 것으로 나타났다. 이들 식물유를 사용한 마요네즈의 냉동분리 안정성, 풍미, 산화안정성 등의 품질 특성에 대한 시험 결과, 저에루신산 유채유를 단독으로 사용하는 것보다는 대두유와 혼합하여 사용하는 것이 좋은 것으로 나타났다. 특히, 대두유에 저에루신산 유채유를 $40{\sim}80%$ 혼합한 식물유를 사용한 마요네즈는 대두유만을 사용한 마요네즈에 비해 저온분리에 대한 안정성이 증가하여 더 바람직한 품질 특성을 나타내었다.

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Preparation and characterization of PVDF/TiO2 composite ultrafiltration membranes using mixed solvents

  • Tavakolmoghadam, Maryam;Mohammadi, Toraj;Hemmati, Mahmood
    • Membrane and Water Treatment
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    • 제7권5호
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    • pp.377-401
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    • 2016
  • To study the effect of titanium dioxide ($TiO_2$) nanoparticles on membrane performance and structure and to explore possible improvement of using mixed solvents in the casting solution, composite polyvinylidene fluoride (PVDF) ultrafiltration membranes were prepared via immersion precipitation method using a mixture of two solvents triethyl phosphate (TEP) and dimethylacetamide (DMAc) and addition of $TiO_2$ nanoparticles. Properties of the neat and composite membranes were characterized using scanning electron microscope (SEM), energy dispersive X-ray spectroscopy (EDS), Atomic force microscopy (AFM) and contact angle and membrane porosity measurements. The neat and composite membranes were further investigated in terms of BSA rejection and flux decline in cross flow filtration experiments. Following hydrophilicity improvement of the PVDF membrane by addition of 0.25 wt.% $TiO_2$, (from $70.53^{\circ}$ to $60.5^{\circ}$) degree of flux decline due to irreversible fouling resistance of the composite membrane reduced significantly and the flux recovery ratio (FRR) of 96.85% was obtained. The results showed that using mixed solvents (DMAc/TEP) with lower content of $TiO_2$ nanoparticles (0.25 wt.%) affected the sedimentation rate of nanoparticles and consequently the distribution of nanoparticles in the casting solution and membrane formation which influenced the properties of the ultimate composite membranes.