• Title/Summary/Keyword: Miniature Specimen

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Development of a Miniature Pendular Type Impact Testing Machine Using a Magnetic Powder Brake (마그네틱 파우더 브레이크를 이용한 소형 진자형 충격시험기 개발)

  • You, In-Dong;Lee, Man-Suk;Kim, Ho-Kyung
    • Tribology and Lubricants
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    • v.27 no.3
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    • pp.140-146
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    • 2011
  • A miniature pendular type impact testing machine was designed and developed, adopting a magnetic powder brake in order to investigate tensile and shear behavior of a small solder ball at high speed. In this testing system, the potential energy of the pendulum is transferred into the impact energy during its drop. Then, the impact energy is transmitted through the striker which is connected to the push rods to push the specimen for tensile loading. The tensile behavior of lead-free solder ball in diameter of 760 ${\mu}m$ was successfully investigated in a speed range of 0.15 m/s~1.25 m/s using this designed device. The maximum tensile strength of the solder joint decreases with the loading speed in the testing condition. The maximum tensile strength of the joint was 56 MPa in the low speed region.

Deployment test of shape memory polymer specimens for space antenna design (우주 안테나 설계용 형상기억 폴리머 시편의 전개 시험)

  • Goo, Nam Seo;Le, Van Luong;An, Yongsan;Yu, Woong-Ryeol;Hwang, Jin Ok;Park, Jongkyoo
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.45 no.12
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    • pp.1007-1012
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    • 2017
  • In this study, we performed the deployment test of shape memory polymer specimens for space antenna design. Poly(cyclootene) was cross-linked by dicumyl peroxide to make a PCO shape memory polymer. A miniature specimen with 120 mm diameter for a deployable antenna was fabricated with the PCO shape memory polymer. To investigate the deployment performance, the folded specimen as a temporary shape was heated by two heaters to the $15^{\circ}C$ higher temperature than the glass transition temperature of shape memory polymer. Firstly, the specimen was installed horizontally and tested. The deploying motion was captured by a digital camera and analyzed by a Tracker program. To reduce the effects of gravity, the specimen was installed vertically and tested again. The deployment performance of a shape memory polymer was investigated by comparing the results of horizontal and vertical installation tests.

Development of High Temperature Creep Properties Evaluation Method using Miniature Specimen (미소시험편을 이용한 고온 크리프 특성 평가법 개발)

  • Yu, Hyo-Sun;Baek, Seung-Se;Lee, Song-In;Ha, Jeong-Soo
    • Proceedings of the KSME Conference
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    • 2000.04a
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    • pp.43-48
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    • 2000
  • In this study, a small punch creep(SP-Creep) test using miniaturized specimen$(10{\times}10{\times}0.5mm)$ has been described for the development of the newly semi-destructive creep test method for high temperature structural components such as headers and tubes of boiler turbine casino and rotor and reactor vessel. The SP-Creep testing technique has been applied to 2.25Cr-1Mo(STBA24) steel used widely as boiler tube material and the creep test temperature are varied at $550^{\circ}C{\sim}600^{\circ}C$. The overall deformations of SP-Creep curves are definitely depended with applied load and creep test temperature and show the creep behaviors of three steps like conventional uniaxial creep curves. The steady state creep rate${\delta}_{ss}$ of SP-Creep curve for miniaturized specimen increases with increasing creep temperature, but the exponential value with creep loading is decreased. The activation energy$(Q_{spc})$ during SP-Creep deformation with various test temperatures shows 605.7kJ/mol that is g.eater than 467.4kJ/mol reported in uniaxial creep test. This may be caused by the difference of stress states during creep deformation In two creep test. But from the experimental results, e.g. SP-Creep curve behaviors, the steady state creep rate${\delta}_{ss}$ with creep temperature, and the exponential value(n) with creep loading, it can be summarized that the SP-Creep test may be a useful test method to evaluate the creep properties of the heat resisting material.

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Small Punch Creep Behavior Analysis for Assessment of Creep Properties (크리프 물성 평가를 위한 소형 펀치 크리프 해석)

  • Im, Jiwoo;Kim, Bum-Joon;Kim, Moon-K;Lim, Byeong-Soo
    • Korean Journal of Metals and Materials
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    • v.48 no.11
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    • pp.965-973
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    • 2010
  • The small punch creep (SPC) test has recently received much attention as a new alternative to the conventional uniaxial creep test because it needs only a miniature-sized specimen directly detached from an operating system or component without any serious sampling damages. However, it is difficult to obtain the equivalent uniaxial creep data directly from the SPC data. As a specimen is deformed by a punch in the SPC test, the test result is sensitive to the friction between them. Finite element analyses with various friction coefficients was performed and showed a tendency of increased SPC life with an increased friction coefficient. The necking position predicted by the SPC simulation with a proper friction coefficient showed good agreement with that observed from the real SPC test. Finally, a noble method to convert the SPC load and displacement rate into the equivalent uniaxial creep stress and strain rate, respectively, was established in this study.

R-curve Analysis of Alumina Ceramics (알루미나 세라믹스의 R-curve 분석)

  • 김성진;손기선;이성학;백성기
    • Journal of the Korean Ceramic Society
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    • v.31 no.10
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    • pp.1099-1106
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    • 1994
  • It is suggested that the microstructural toughening process in the initial rising portion of R-curves observed in polycrystalline alumina should be different from the grain bridging mechanism identified in the long crack regime. Microcracking in the advancing crack front seems to be a prerequisite for the development of unbroken bridging ligaments behind the crack tip. In order to test such a proposition, attempts were made to identify experimentally the presence of microcracks in the frontal zone of propagating cracks. In-situ observation is made of crack growth in a miniature double cantilever beam specimen of a average grain size of 10 ${\mu}{\textrm}{m}$ alumina. Presence of a few microcracks was identified in front of crack tip on the propagating crack plane. The R-curves were re-evaluated based on the observation.

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Successful Combination Chemotherapy for Nasal Carcinoma in a Dog

  • Kim, Su-Gang;Cho, Seok-Ho;Kim, Keon;Park, Hee-Myung;Park, Sang-Ik;Kim, Tae-Jung;Lee, Chang-Min
    • Journal of Veterinary Clinics
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    • v.36 no.5
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    • pp.274-277
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    • 2019
  • A Miniature Schnauzer presented with bilateral mucopurulent nasal discharge and sneezing. Computed tomography of the skull revealed exudates in the nasal cavity and frontal gyrus. Nasal swab cytology showed features of an epithelial-origin tumor. Histopathologic evaluation of the biopsy specimen revealed irregular proliferation of epithelial cells and necrotized tissue. Positive immunohistochemical staining confirmed the epithelial origin of the cells. The dog was diagnosed with nasal carcinoma and was treated with a chemotherapy protocol of carboplatin and piroxicam. This report confirms the effectiveness of combination chemotherapy only without radiotherapy in a dog with nasal carcinoma and provides a guideline for providing alternative treatment.

Effectiveness of autogenous tooth bone used as a graft material for regeneration of bone in miniature pig (미니피그에서 자가치아뼈 이식의 골형성 효과에 대한 연구)

  • Jeong, Hye-Rin;Hwang, Ju-Hong;Lee, Jeong-Keun
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.37 no.5
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    • pp.375-379
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    • 2011
  • Introduction: This study examined the effect of autogenous tooth bone used as a graft material for bone regeneration in an artificial bony defect of minipigs. Materials and Methods: Four healthy minipigs, weighing approximately 35-40 kg, were used. Four standardized artificial two-walled bony defects, 5 mm in length and depth, were made on the bilateral partial edentulous alveolar ridge on the mandible of minipigs, and autogenous tooth bone was augmented in the right side as the experimental group. On the other hand, only alloplastic bone graft material HA was grafted with the same size and manner in the left side as the control group. All minipigs were sacrificed at 4 weeks after a bone graft and evaluated histologically by Haematoxylin-eosin staining. The specimens were also evaluated semi-quantitatively via a histomorphometric study. The percentage of new bone over the total area was evaluated using digital software for an area calculation. Results: All specimens were available but one in the left side (control group) and two in the right side (experimental group) were missing during specimen preparation. The amount of bone formation and remodeling were higher in all experimental groups than the control. The mean percentage area for new bone in the experimental and control groups was $43.74{\pm}11.96%$ and $30.79{\pm}2.93%$, respectively. Conclusion: Autogenous tooth bone is a good alternative to autogenous bone with the possible clinical feasibility of an autogenous tooth bone graft in the reconstruction of bony defects.

Evaluation of Fracture Toughness Using Small Punch Test for Aluminum 6061-T6 Type-3 Cylinder Liner (소형펀치시험법을 이용한 알루미늄 6061-T6 Type-3 용기 라이너의 파괴인성 평가)

  • Ma, Young-Wha;Lee, Seong-Hoon;Yoon, Kee-Bong
    • Journal of the Korean Institute of Gas
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    • v.15 no.4
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    • pp.21-26
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    • 2011
  • Type-3 cylinder liner has a limitation of machining the standard specimen for fracture toughness test because it has approximately 5 mm in thickness as well as a curvature. Hence, it needs to be employed a miniature specimen test technique to evaluate fracture toughness of the cylinder liner. In this study, small punch (SP) test method was employed to evaluate fracture toughness of the cylinder liner. Load-displacement curve result measured from the SP test showed that the liner material was failed during membrane stretching in the general SP load-displacement curve. Additionally, it was shown that liner material was isotropic although the amount of plastic deformation was different depending on the direction due to manufacturing process characteristics. Fracture toughness, $J_{Ic}$, was evaluated using the SP test data. The value of fracture toughness obtained was $13.0kJ/m^2$. This value was similar to that of the same kind of materials. Therefore, the fracture toughness evaluated using the SP test data was reasonable.

Development and Applications of Material Testers for the Thin Films (박막 재료 시험기 개발 및 응용)

  • Ahn Hyun-Gyun;Lee Hak-Joo;Oh Chung-Seog
    • Journal of the Korean Society for Precision Engineering
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    • v.23 no.3 s.180
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    • pp.163-170
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    • 2006
  • Thin films play an important role in many technological applications including microelectronic devices, magnetic storage media, MEMS and surface coatings. It is well known that a thin film's material properties can be very different front the corresponding bulk properties and thus there has been a strong need for the development of a miniature tester to measure the mechanical properties of a thin film. Two testers are designed and set up in small size of 62 mm width, 20 mm depth and 90-120 mm height to fit in a chamber of scanning electron microscope (SEM). One tester has a homemade 0.2 N load cell and a low-priced electromagnetic actuator. The other has a commercial 5 N load cell, a $52{\mu}m$ piezoelectric actuator and some novel grips. Two types of 3.5 microns thick polysilicon specimen are tested to prove the testers' applicability. The strain is measured by the two ways. Firstly, it is measured by an ISDG system in the atmosphere far the reference. Secondly, the same test is repeated in a SEM chamber to monitor the strain as an in-situ experiment. The strain is evaluated by observing the gap change between two markers.

Porcine study on the efficacy of autogenous tooth bone in the maxillary sinus

  • Lee, Du Han;Yang, Keun Yong;Lee, Jeong Keun
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.39 no.3
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    • pp.120-126
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    • 2013
  • Objectives: This study sought to elucidate the effect of autogenous tooth bone material by experimenting on minipig's maxillary sinus and performing histological and histomorphometric analyses. Materials and Methods: Five 18-24 month-old male minipigs were selected, and right maxillary sinuses were grafted with bone graft material made of their respective autogenous teeth extracted eight weeks earlier. The left sides were grafted with synthetic hydroxyapatite as control groups. All minipigs were sacrificed at 12 weeks after bone graft, which was known to be 1 sigma (${\sigma}$) period for pigs. Specimens were evaluated histologically under a light microscope after haematoxylin-eosin staining followed by semi-quantitative study via histomorphometric analysis. The ratio of new bone to total area was evaluated using digital software for calculation of area. Results: All specimens were available, except one on the right side (experimental group), which was missing during specimen preparation. This study demonstrated new bone at the periphery of the existing bone in both groups, showing evidence of bone remodeling, however, encroachment of new bone on the central part of the graft at the 1 ${\sigma}$ period was observed only in the autogenous tooth bone group (experimental group). Histomorphometric analysis showed more new bone formation in the experimental group compared to the control group. Although the difference was not statistically significant (P>0.05), the mean percentage area for new bone for the experimental and control groups were $57.19%{\pm}11.16%$ and $34.07%{\pm}13.09%$, respectively. Conclusion: The novel bone graft material using autogenous tooth is a good alternative to autogenous bone, comparable to autogenous bone, and outperforming synthetic hydroxyapatite bone graft materials in terms of bone regeneration capacity. Augmentation with autogenous tooth bone materials will reduce donor site morbidity without hampering the safety of the autogenous bone graft.