• Journal of Powder Materials
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• v.20 no.4
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• pp.258-263
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• 2013

We examined various ball-milling parameters which affect the structural and morphological modification of multi-wall carbon nanotubes. In particular, the effect of milling mode and the use of different milling agents were examined. Friction milling mode induced more structural changes than impact milling mode except the use of dry ice as a milling agent. Wet milling was helpful for reducing more effectively the agglomeration of nanotubes than dry milling. The use of hard solid particles such as silica and alumina as milling agents resulted in an effective shortening of nanotubes, but often susceptible to the amorphization and the destruction of crystallinity.

• Proceedings of the KSME Conference
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• 2004.04a
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• pp.1148-1153
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• 2004

Recently the high speed end-milling processing is demanded the high-precise technique with good surface rougj1ness and rapid time in aircraft, automobile part and molding industry. The working factors of high speed end-milling has an effect on surface roughness of cutting surface. Therefore this study was carried out to analyze the working factors to get the optimum surface roughness by design of experiment. From this study, surface roughness have an much effect according to priority on Spindle speed, feed rale, hardness and axial depth of cut By design of experiment, it is effectively represented shape characteristics of surface roughness in high speed end-milling And determination($R^2$) coefficient of regression equation had a satisfactory reliability of 89.7% and regression equation of surface roughness is made by regression analysis.

• 한국정보디스플레이학회:학술대회논문집
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• 2004.08a
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• pp.555-557
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• 2004

We report the effect of the particle size (D50) and PSD (Particle Size Distribution) of glass frit on the transparency of transparent dielectric layer of PDP. The milling efficiency of wet milling with water was the best among the dry milling, wet milling with IPA and wet milling with water. The transparency increased with the reduction of particle size of glass frit as the milling time increased. Also the transparency changed by the PSD of glass frit. Glass frits of broad PSD showed high transparency compared with the glass frits of sharp PSD.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2001.04a
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• pp.95-100
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• 2001

Recently, coated milling cutters are widely used for improving the productivity of cutting processes through high speed cutting and longer tool life. In metal cutting, cutting force increase rate is important factor to diagnose the cutting conditions because the amount of tool wear directly influences the cutting forces. As the cutting length increases, the worn cutter increases the cutting forces. In this study, the effect of coating process of end milling cutter on the cutting performance, especially on the cutting force increase rate, is investigated. The results acquired through the cutting test measuring cutting force increase rate show that not only the injection quantity of $N_2$ and Ar but also mean temperature influence the cutting force increase rate during the end milling process.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2000.04a
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• pp.321-325
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• 2000

To obtain precise surface and high productivity, high speed end milling has been studied recently. Though high speed end milling is explicitly effective for precision surface generation geometrically, tool deflection, chatter vibration and frequency characteristics of end milling system deteriorate the theoretical surface. In this study, simulation algorithm and programming method are suggested to simulate machined surface using acceleration signal in high speed end milling. This simulation is conducted by considering vibrational effect of spindle system which was not considered by other researchers. Between simulated results and experiment results, good agreements were obtained.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.25 no.2
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• pp.228-234
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• 2001

To obtain precise machined surface and high productivity in machining, high speed end milling has beed studied recently. Though high speed end milling is explicitly effective for precision surface generation geometrically, tool deflection, chatter vibration and frequency characteristics of end milling system deteriorate the theoretical surface. In this study, simulation algorithm and programming method are suggested to simulate machined surface using acceleration signal in high speed end milling. This simulation is conducted by considering vibrational effect of spindle system which was not considered by other investigators. Good agreements were obtained between simulated results and experimental results.

• Tribology and Lubricants
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• v.27 no.1
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• pp.1-6
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• 2011

The possibility of Cu-Al-Ni intermetallic coating on the mild steel through the combustion synthesis has been investigated. In particular, the effect of the ball milling energy on the microstructure of the coating layer was examined to obtain the best coating condition. Experimental results show that Cu-Al-Ni powder compact was explosively synthesized and successfully coated with the steel matrix. It was revealed that the formation of $Cu_9Al_4$ intermetallic decreased with increase in the ball milling energy. This result supports that the high energy ball milling would be effective for obtaining the most suitable microstructure for Cu-Al-Ni coating layer. However, the excessive ball milling energy seems to decrease the bonding strength between the coating layer and the matrix.

• Journal of Powder Materials
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• v.18 no.6
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• pp.496-501
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• 2011

In this study, the effect of milling time on the microstructure and phase transformation behaviors of Ni-12 wt.%B powders was investigated using vibratory ball milling process. X-ray diffraction patterns showed that the phase transformation of mixed Ni-B elemental powder occurred after 50 hours of milling, with a formation of nickel boride phases. Through the study of microstructures in mechanical alloying process, it was considered that ball milling strongly accelerates solid-state diffusions of the Ni and B atoms during mechanical alloying process. The results of X-ray photoelectron spectroscopy showed that most of B atoms in the powder were linked to Ni with a formation of nickel boride phases after 200 hours of milling. It was finally concluded that mechanical alloying using ball milling process is feasible to synthesize fine and uniform nickel boride powders.

• Journal of Powder Materials
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• v.5 no.1
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• pp.64-70
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• 1998

Milling media of steel and partially stabilized zirconia(PSZ) were used to produce $Mo_3$Si by mechanical alloying(MA) of Mo-25.0at%Si elemental powder mixture. The effect of milling medium materials on MA of the powder mixture have been investigated by XRD and DTA. The reaction rate and the end-product noticeably depended upon the milling medium material. The formation of $Mo_3$Si and $Mo_5Si_3$phases by PSZ ball-milling took place after 15 hr of MA and was characterized by a slow reaction rate as Mo, Si, $Mo_5Si_3$ and $Mo_3$Si coexisted for a long period of milling time. The formation of a new phase by steel ball-milling, however, did not take Place even after 96 hr of MA. DTA and annealing results showed that $Mo_5Si_3$ and $Mo_3$Si were formed after heating the ball-milled powder specimens to different temperatures. At low temperatures, Mo and Si were transformed into $Mo_5Si_3$. At high temperatures, the formation of $Mo_3$Si can be partially attributed to the reaction, 7Mo+Si+$Mo_5Si_3$-.4$Mo_3$Si . The formation of $Mo_3$Si and Mo5Si3 phases by mechanical alloying of the powder mixture and the relevant reaction rate appeared to depend upon the milling medium material as well as the thermodynamic properties of the end-products.

• Journal of Powder Materials
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• v.4 no.3
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• pp.179-187
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• 1997

Milling media of steel and zirconia were used to produce $MoSi_2$ by mechanical alloying (MA) of Mo and Si powders. The effect of milling media on MA of Mo-65.8at%Si powder mixture has been investigated by SEM, XRD, DTh and in-situ thermal analysis. The powders mechanically alloyed by milling medium of steel for 8 hours showed the structure of fine mixture of Mo and Si, and those mechanically alloyed by milling medium of zirconia for longer milling time showed the structure of fine mixture of Mo and Si. The tetragonal $\alpha$-$MoSi_2$ Phase and the tetragonal $Mo_5Si_3$ phase appeared with small Mo peaks in the powders milled by milling medium of steel for 4 and 8 hours. The $\alpha$-$MoSi_2$ phase and the hexagonal $\beta$-$MoSi_2$ phase were formed after longer milling time. The $\alpha$-$MoSi_2$ phase appeared with large Mo peaks in the powders milled by milling medium of zirconia for 4 hours. The phases, $\alpha$-$MoSi_2$ and $\beta$-$MoSi_2$. were formed in the powders milled for longer milling time. DTA and annealing results showed that Mo and Si were transformed into $\alpha$-$MoSi_2$ and $Mo_5Si_3$, while $\beta$-$MoSi_2$ into $\alpha$-$MoSi_2$. In-situ thermal analysis results demonstrated that there were a sudden temperature rise at 212 min and a gradual increase in temperature in case of milling media of steel and zirconia, respectively. The results indicate that MA can be influenced by materials of milling medium which can give either impact energy on powders or thermal energy accumulated in vial.