• 대한치과보철학회지
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• 제28권2호
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• pp.109-124
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• 1990

The purpose of this study was to investigate the physical propertise and determine whether three were any differences in the amount of porosity of the denture base resins cured by microwave irradiation and conventional water bath heating. The resins used in this study were K-33 resin and Acron MC resin. The properties selected were transverse strength, Knoop hardness, and density. A ten-power eyepiece and scanning electron microscope(Magnification of ${\times}$ 30and ${\times}$150)were used to examine the specimens for porosity. Through analyses of the data from this study, the following conclusions were obtained. 1. Microwave energy can be effectively use dtopolymerize poly(methylmethacrylate) denture base resins. 2. In the transverse strength, K-33 resin cured by microwave irradiation was the first highest, water bath cured K-33 resin the second, microwave cured Acron MC resin the third, water bath cured Acron MC resin the fourth. 3. In the Knoop hardness, K-33 resin cured by microwave irradiation was the first hardest, water bath cured K-33 resin the second, water bath cured Acron MC resin the third, microwave cured Acron MC resin the the fourth. 4. No significant difference was found between the density of resin denture bases polymerized by either method. 5. K-33 resin showed the most porosity for the microwave curing. But there was no significant difference in the Acron MC resin and other curing method.

• 대한치과보철학회지
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• 제34권4호
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• pp.816-822
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• 1996

The purpose of this study was to determine whether there was any difference in the mean porosity of denture base resin cured by microwave energy, when the liquid monomers of denture resin(K-33 : methyl methacrylate for conventional water bath curing or Acron MC : special monomer for microwave curing) and/or the thicknesses of denture base($5{\times}10{\times}60mm\;or\;10{\times}10{\times}60mm$) were varied. The mean porosities of k-33 specimens cured in water bath with two different thicknesses were used as control. The results were as follows : 1. Regardless of specimen thickness, Acron MC cured by microwave energy showed the least mean porosity, followed by K-33 cured by water bath heat, and K-33 cured by microwave energy showed the highest level of mean porosity(P<0.05). 2. In both K-33 and Acron MC cured by microwave energy the mean porosities of 5mm thickness groups were lower than those of 10mm thickness groups(P<0.05). But no significant difference was found in mean porosity between 5mm thickness and 10mm thickness of water bath heat cured groups made of K-33(P>0.05).

• Bulletin of the Korean Chemical Society
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• 제32권3호
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• pp.961-963
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• 2011

Spin-coated waterborne polyurethane to protect glass surface from environmental attacks was cured by using microwave heating. The effect of microwave heating on the reaction kinetics, chemical durability, and transmittance of polyurethane was investigated. In comparison to the conventional heating the results show that the microwave heating substantially accelerates the curing process of waterborne polyurethane and the total time for the completion of the reaction is only 1/7 of that in the conventional process. The microwave cured sample showed an excellent caustic resistance compared to conventional cured one. It means that microwave heating produces dense structure during curing process. The dense structure does not affect to the transmittance in the visible region.

• 한국산업융합학회 논문집
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• 제2권1호
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• pp.69-75
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• 1999

Intending to develop a new rubber curing process using only microwave, the both the characteristics of cure and the mechanical properties of rubbers for the tire tread, for which a green styrene-butadiene compounds had been cured with 2.45 GHz microwave, have been compared with those of the custom thermal cured rubber. The unintentional hot spot formation in the compound during the microwave curing has not found where the compound has a microwave absorbing ceramic powders in 4.18 weight percents and the supplying voltage has been adjusted to 90 volts. The new microwave process accomplished preheating to 418K in a quarter of the thermal cure time. The average tensile strength of the microwave-cured rubber indicating $190kg/cm^3$ was compatible to that of the thermal cure. In conclusion, the new microwave cure had approved to be applicable in a commercial plant.

• 한국식품조리과학회지
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• 제10권2호
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• pp.138-141
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• 1994

Whole, peeled sweetpotatoes were subjected to four different processes: 15 min microwave heating followed by 15 min baking (1), 90 min baking (2), 15 min microwave heating (3), and 15 min boiling followed by 15 min microwave heating (4). Samples of green and cured roots were used in the study. Scanning electron photomicrographs revealed that cured roots contained larger numbers of starch granules in the parenchyma cells than green roots, most of them compounded. The starch in cooked green roots was gelatinized while for cured roots it was mostly hydrolyzed into dextrins and sugars. Starch in process (3) roots was mostly gelatinized while in process (1) and process (2) roots gelatinized starch appeared in little quantity, thus it was primarily converted to dextrins and sugars. The process (4) resulted in little conversion of starch. The process (1) product resulted in a similar product to the process (2) product.

• 한국산학기술학회논문지
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• 제16권7호
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• pp.4388-4397
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• 2015

이 연구는 아크릴 수지의 유도광선변화에 따른 속성 변화를 연구하여 최적의 특성을 가진 아크릴 수지를 개발할 수 있도록 건열 및 마이크로파 경화 의치상 아크릴 수지의 향상된 물성에 대한 연구이다. 굽힘강도와 경도, 색차를 관찰한 결과 Vertex RS 및 Paladent 20는 건식 열 경화 시편 5, 15, 25 kGy의 조사에 이상적인 속성을 보였다. 마이크로 웨이브 경화에서는 5 kGy의 조사에서 이상적인 속성을 보였다. 상관관계 분석은 ARD와 굴곡 강도 (0 418), E 계수 (0.675), 및 바콜 경도 (0 588) 사이의 긍정적인 상관관계를 보여 주었다. 방사선 경화형 기술은 고분자 복합 재료의 제작으로 인한 오염 문제를 완화하는 데 도움이 될 수 있으며 고분자의 가공성에 영향을 주지 않고 자외선 경화 기술과 나노 기술 융합 및 기계적 특성의 향상에 크게 기여할 수 있다.

• 대한치과보철학회지
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• 제30권3호
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• pp.401-410
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• 1992

The purpose of this study was to investigate the dimensional changes and surface morphology of dentures processed by various polymerization conditions. The measurements were done by taking radiograph and using vernier calipers and each specimen was observed on scanning electron microscope. Results obtained were as follows. 1. The difference of dimensional stability was not recognized between various polymerization conditions(heat-cured resin, pour-type resin, microwave-cured resin, and injection molding resin). 2. There were expansion and shrinkage in the occlusal dimension, shrinkage in the frontal dimension, and expansion in the lateral dimension. 3. Scanning electron microscope pictures of heat-cured resin showed dense and regular surface morphology. 4. Microwave-cured resin surface appeared more regular and smooth than pour-type resin but less dense and more irregular than heat-cured resin. 5. Scanning electron microscope pictures of pour-type resin with the lowest dimensional change showed the most irregular surface morphology.

• 한국철도학회논문집
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• 제17권5호
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• pp.365-372
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• 2014

콘크리트 공사에서 공기단축과 시공비 절감을 위하여 가장 핵심적인 기술 중 하나는 온도 제어 양생기술이다. 최근에 마이크로웨이브를 이용한 발열 촉진 양생방법이 개발되었다. 본 연구에서는 개발된 기술을 적용한 콘크리트의 조기 강도발현특성을 실험적으로 고찰하였다. 총 6차에 걸친 대형 Mock-up 실험을 수행하였으며 실험결과를 성숙도이론에 근거하여 해석하였다. 개발된 방법으로 양생된 콘크리트의 압축강도 발현과 성숙도는 로그함수의 관계를 나타내었으며, 일반적인 고온 증기 양생된 콘크리트에 적용되는 등가재령이론으로 강도예측이 가능한 것으로 확인되었다. 개발된 마이크로웨이브 발열거푸집에 의해 동절기에도 하루면 거푸집 탈형을 위한 소요강도를 확보할 수 있는 것으로 나타났다.

• 콘크리트학회논문집
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• 제27권6호
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• pp.669-676
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• 2015

본 연구에서는 촉진양생기술 중 하나인 마이크로웨이브 발열거푸집으로 양생된 콘크리트의 재령에 따른 압축강도를 예측할 수 있는 모델을 제시하였다. 제시된 모델은 ACI 209R-92에서 제시하고 있는 모델식과 유사하지만 시멘트종류와 양생방법에 따른 계수를 실험과 그 결과의 회귀분석에 근거하여 수정하여 제안하였다. 실험실 규모의 실험체를 타설한 후 마이크로웨이브 발열거푸집으로 촉진양생한 후 실험체로부터 채취된 코어의 압축강도를 측정하였다. 측정강도결과는 표준코어강도와 현장 콘크리트강도로 보정되었으며, 이 자료를 근거로 회귀분석을 수행하였다.

• 한국공작기계학회논문집
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• 제16권2호
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• pp.106-111
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• 2007

In this research work attempts were made to study the bonding of thermo-plastics with adhesives using solar radiation. In order to study the curing behaviour necessary experiments were conducted under varying conditions of temperature, exposure time and power of solar energy. The cured samples were then studied under the optical microscope before subjecting to tensile testing in order to study their mechanical properties of thermo-plastics. The fracture surfaces were further studied under the Scanning Electron Microscopy(SEM) in order to research the microstructural changes that are taken place during curing. In order to measure the performance of solar energy cured joints the parameters such as; bond strength, surface morphology, the microstructual changes, variation in properties of adhesives bonded joints are compared to that of specimen cured at ambient conditions and specimen cured using microwave techniques.