• Title/Summary/Keyword: Microwave-assisted

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Polyphenol Contents and Physiological Activity of the Lespedeza bicolor Extracts (싸리 추출물의 폴리페놀 함량과 생리활성)

  • Lee, Yang-Suk;Joo, Eun-Young;Kim, Nam-Woo
    • Food Science and Preservation
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    • v.13 no.5
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    • pp.616-622
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    • 2006
  • This study was intended to analyze the contents of polyphenol compounds and vitamin C, and the inhibitory activities of xanthine oxidase and tyrosinase to measure physiological efface of various extract of Lespedeza bicolor. The vitamin C content was $26.42{\pm}0.08mg/100g$. The content of phenolic compounds included in the flesh L bicolor was $1.14{\pm}0.02mg/g$. The ethanol extract by reflux method and water extracts by the microwave-assisted method showed the highest content as 154.95 mg/g and 145.17 mg/g, respectively. The xanthine oxidase inhibitory tate of water extracts was the highest value of 87.85% at the concentration of 1,000 ug/mL. All kinds of extracts showed the highest inhibitory activity for the xanthine oxidase at the concentration of 1,000 ug/mL and a decreasing pattern of the inhibitory race over the concentration of 1,000 ug/mL. The tyrosinase inhibitory rate was increased with an increment of the extract concentrations, and the activity of ethanol extracts was the highest as 55.22% at the concentration of 3,000 ug/mL.

Analytical Method to Quantify Sodium Metasilicate in Shark Fins (샥스핀 가공 중 사용된 메타규산나트륨 분석)

  • Park, Se-Jong;Jang, Su-Jin;Choi, Jae-Chon;Kim, Meehye
    • Korean Journal of Food Science and Technology
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    • v.47 no.2
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    • pp.145-148
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    • 2015
  • According to the Korea Food Additives Code, sodium metasilicate is permitted for use as a filtering agent for edible oils and fats. Sodium metasilicate is currently used as a food additives to increase the weight of shark fins. In this study, we developed an analytical method to quantify sodium metasilicate in food. Sodium metasilicate content was estimated by measuring the moisture content, pH and silicon content of shark fins. Silicon content was analyzed using inductively coupled plasma-optical emission spectrometry (ICP-OES) following microwave-assisted digestion with $HNO_3$ (65%) and $H_2O_2$ (30%). Shark fin total silicon content was $7.17{\pm}8.92mg/kg$, while the soluble silicon content was $2.34{\pm}3.80mg/kg$. After soaking raw shark fin in an aqueous solution of sodium metasilicate, fin weight, pH and silicon content were measured. These results would be used as the basic information for shark fins safety management.

Degradation of Antibiotics Using Silver Decorated Heterojunction Carbon Nitride under Visible Light (은 장식 이종접합 질화탄소를 이용한 가시광선 조건에서의 항생제 분해 연구)

  • Taeyoon, Lee
    • Journal of the Korean GEO-environmental Society
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    • v.24 no.3
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    • pp.23-27
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    • 2023
  • Graphitic carbon nitride (g-C3N4) has been used as effective photocatalyst for degradation of antibiotics under visible light irradiation. However, the fast recombination of hole-electron pair may limit their photocatalytic efficiency. In our study, Ag was grafted on g-C3N4/g-C3N4 isotype heterojunction by a microwave-assisted decomposition method. The structure and physical properties of heterojunction photocatalyst were characterized through X-ray diffraction, UV-DRS, FT-IR, and Photoluminescence analyses. Ag decorated g-C3N4/g-C3N4 isotype heterojunction exhibited excellent photocatalytic activity for degradation of sulfamethoxazole under irradiation under visible light irradiation within 210 min, which is higher than g-C3N4/g-C3N4 isotype heterojunction and bulk g-C3N4. The addition of Ag may broaden the visible light absorption and restrict the recombination of hole-electron pair because of the surface plasmons resonance, resulting in the improving the photocatalytic activity.

Comparison of the Mineral Contents of Sun-dried Salt Depending on Wet Digestion and Dissolution (습식분해 및 직접용해법에 따른 천일염 중 무기성분 함량 비교)

  • Jin, Yong-Xie;Je, Jeong-Hwan;Lee, Yeon-Hee;Kim, Jin-Hyo;Cho, Young-Suk;Kim, So-Young
    • Food Science and Preservation
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    • v.18 no.6
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    • pp.993-997
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    • 2011
  • The aims of this research were to determine the proximate composition of various salts and to compare two digestion methods (direct digestion without heating, and microwave digestion) for the determination of the main mineral contents of various salts. Twelve salt samples were divided into three groups of four samples each (imported, Korean gray, and Korean white salts). As a result, the NaCl contents of the Korean white, Korean gray, and imported salts were 85.1, 89.3, and 91.3%, respectively. The salts in the three groups were analyzed for their main mineral contents via AAS. The sodium (Na) content of the Korean white salt was found to be slightly lower than that of the imported salt while the magnesium (Mg) and potassium (K) contents of the Korean white salt were found to be higher than those of the imported salt. The mineral composition (% Na:Mg) obtained using microwave-assisted digestion procedures, and the other dissolutions for the subsequent sample analysis, were 89:1 (for both the imported and Korean gray salts) and 82:3 vs. 81:3 (Korean white salt), respectively. The data regarding the mineral contents and composition of the sun-dried salts obtained through the analysis method of wet digestion and the dissolution procedure were compared, and no significant difference was found between the two datasets. Consequently, in this paper, a direct dissolution procedure is suggested for the analysis of the mineral composition of salt.