• 제목/요약/키워드: Microstructural factor

검색결과 88건 처리시간 0.028초

복합조직강의 기계적 특성에 미치는 미시조직인자의 영향 (Effect of microstructure on mechanical properties in dual phase steel)

  • 김정규;유승원
    • 오토저널
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    • 제9권3호
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    • pp.76-84
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    • 1987
  • A study has been made to clarify the microstructural effect on static tensile properties of the dual phase steel, in which the martensitic phase encapsulated islands of ferritic phase. The main results are as follows: Yield strength is associated with the degree of plastic constraint factor and tensile strength increases with increasing of strain hardening exponent. Also, the variation of ductility is dependent upon the amount of micro-brittle facets.

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BiFe3첨가에 따른 저온소결 PSN-PZT세라믹스의 유전 및 압전 특성 (Dielectric and Piezoelectric Properties of Low Temperature Sintering PSN-PZI Ceramics with BiFe3 Substitution)

  • 류주현;정광현;정영호
    • 한국전기전자재료학회논문지
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    • 제17권5호
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    • pp.492-496
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    • 2004
  • In this study, (0.96 -x)(PSN-PZT)-xBF-0.04 PNW+0.3wt%MnO$_2$+0.6wt%CuO ceramics were fabricated with the variations of the amount of BiFeO$_3$substitution and sintering temperature for the development of modified ceramics which can be sintered in the low temperature($\leq$100$0^{\circ}C$ ), and their microstructural, dielectric and piezoelectric characteristics were investigated. As the amount of BiFeO$_3$ substitution was increased, the density, mechanical quality factor(Q$_{m}$) and electromechanical coupling factor(k$_{p}$) showed the maximum value at each of sintering temperature. At sintering temperature of 98$0^{\circ}C$ and BiFeO$_3$substitution of 2 mol%, the density, dielectric constant and electromechanical coupling factor(k$_{p}$) showed the maximum value of 7.84 g/㎤, 1415 and 0.49, respectively. And at sintering temperature of 95$0^{\circ}C$ and BiFeO$_3$substitution of 3mol%, mechanical quality factor showed the maximum value of 1062. 1062.

보자력 측정에 의한 아공석강 및 공석강의 열처리에 따른 미세조직 평가 (Characterization of Microstructures of Variously Heat Treated Hypoeutectoid and Eutectoid Steel by Magnetic Coercivity Measurement)

  • 변재원;김정석;권숙인
    • 한국재료학회지
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    • 제14권8호
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    • pp.565-572
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    • 2004
  • The microstructures of variously heat treated hypoeutectoid($0.45\%$ carbon) and eutectoid($0.85\%$ carbon) steel were characterized by magnetic coercivity measurement. The effect of spheroidization of cementites on the coercivity was investigated for $0.45\%$ carbon steel. In case of $0.85\%$ carbon steel, microstructural parameters such as prior austenite grain size, phase and pearlite interlamellar spacing were measured along with coercivity to investigate the relationships between them. Prior austenite grain size had little effect on the measured coercivity. Coercivity was observed to be high in order of martensite, pearlite and ferrite phases. The linear decrease of coercivity with increasing pearlite interlamellar spacing was found. The effect of each microstructural factor on the coercivity and the potential of coercivity as a nondestructive evaluation parameter for assessing microstructures of steel products are discussed.

복합조직강의 미시조직변화가 피로파괴전파에 미치는 영향 (The Effects of the Microstructural Change of Dual Phase Steel on Fatigue Fracture Propagation)

  • 오세욱;김웅집
    • 한국해양공학회지
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    • 제5권2호
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    • pp.198-198
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    • 1991
  • Not only difference of fatigue crack growth and propagation behavior resulted from the grain size, the hardness ratio and volume fraction in M.E.F. dual phase steel composed of martensite in hard phase and ferrite in soft phase, but also the effects of the plastic constraint were investigated by fracture mechanics and microstructural method. The main results obtained are as follows: 1) The fatigue endurance of M.E.F. steel increases with decreasing the grain size, increasing the ratio of hardness and volume fraction. 2) The initiation of slip and crack occures faster as the stress level goes higher. These phenomena result from the plastic constraint effect of the second phase. 3) The crack propagation rate in the constant stress level is faster as the grain size gets larger, the ratio of hardness lower and volume fraction smaller.

Particle Size Effects on Microstructure Evolution and Microwave Dielectric Characteristics in $0.93MgTiO_3-0.07CaTiO_3$Ceramics

  • Lee, Jung-A;Kim, Jeong-Joo;Kim, Nam-Kyong;Cho, Sang-Hee;Hahn, Jin-Woo
    • The Korean Journal of Ceramics
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    • 제5권3호
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    • pp.260-264
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    • 1999
  • Effect of the particle size of $MgTiO_3$ and $CaTiO_3$ on the microstructural evolution during sintering of $0.93MgTiO_3-0.07CaTiO_3$ system was investigated. Microwave dielectric characteristics of the sintered ceramics were also measured. The microstructural evolutions were explained with an emphasis on the entrapping behavior of $CaTiO_3$ grain into the $MgTiO_3$ grain and were correlated with microwave dielectric characteristics. With an increasing particle size ratio between $CaTiO_3$and $MgTiO_3$, the fraction of entraped $CaTiO_3$ grains increased, which grain growth of $MgTiO_3$were concurrently accelerated due to decreasing drag force of its boundary migration. Besides, $CaTiO_3$-grain entrapment into the $MgTiO_3$grain interior led to decreaseing quality factor values.

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기계적 밀링법으로 제조된 마그네슘 분말의 밀링시간에 따른 미세구조 변화와 부식거동 (Corrosion Behavior and Microstructural Evolution of Magnesium Powder with Milling Time Prepared by Mechanical Milling)

  • 안진우;황대연;김긍호;김혜성
    • 대한금속재료학회지
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    • 제49권6호
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    • pp.454-461
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    • 2011
  • In this study, the relationship between corrosion resistance and microstructural characteristics such as grain size reduction, preferred orientation, and homogenous distribution of elements and impurity by mechanical milling of magnesium powder was investigated. Mechanical milling of pure magnesium powder exhibited a complex path to grain refinement and growth together with preferred orientation reversal with milling time. It was also found that anisotropic formation of dislocation on the basal plane of magnesium was initially the dominant mechanism for grain size reduction. After 60 hrs of milling, grain coarsening was observed and interpreted as a result of the strain relaxation process through recrystallization. In spite of the finer grain size and strong (002) texture developed in the sample prepared by spark plasma sintering at $500^{\circ}C$ for 5 min after mechanical milling for 2hrs, the sample showed a higher corrosion rate. The results from this study will be helpful for better understanding of the controlling factor for corrosion resistance and behaviors of mechanical milled magnesium powders.

Importance of Green Density of Nanoparticle Precursor Film in Microstructural Development and Photovoltaic Properties of CuInSe2 Thin Films

  • Hwang, Yoonjung;Lim, Ye Seul;Lee, Byung-Seok;Park, Young-Il;Lee, Doh-Kwon
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2014년도 제46회 동계 정기학술대회 초록집
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    • pp.471.2-471.2
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    • 2014
  • We demonstrate here that an improvement in precursor film density (green density) leads to a great enhancement in the photovoltaic performance of CuInSe2 (CISe) thin film solar cells fabricated with Cu-In nanoparticle precursor films via chemical solution deposition. A cold-isostatic pressing (CIP) technique was applied to uniformly compress the precursor film over the entire surface (measuring 3~4 cm2) and was found to increase its relative density (particle packing density) by ca. 20%, which resulted in an appreciable improvement in the microstructural features of the sintered CISe film in terms of lower porosity, reduced grain boundaries, and a more uniform surface morphology. The low-bandgap (Eg=1.0 eV) CISe PV devices with the CIP-treated film exhibited greatly enhanced open-circuit voltage (VOC, from 0.265 V to 0.413 V) and fill factor (FF, from 0.34 to 0.55), as compared to the control devices. As a consequence, an almost 3-fold increase in the average power conversion efficiency, 3.0 to 8.2% (with the highest value of 9.02%), was realized without an anti-reflection coating. A diode analysis revealed that the enhanced VOC and FF were essentially attributed to the reduced reverse saturation current density (j0) and diode ideality factor (n). This is associated with the suppressed recombination, likely due to the reduction in recombination sites such as grain/air surfaces (pores), inter-granular interfaces, and defective CISe/CdS junctions in the CIP-treated device. From the temperature dependences of VOC, it was confirmed that the CIP-treated devices suffer less from interface recombination.

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미세구조 관찰에 의한 철제금속유물의 특성화 (Characterization of Ferrous Metal Artifacts by Microstructure Observation)

  • 허우영;이철
    • 분석과학
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    • 제11권4호
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    • pp.316-320
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    • 1998
  • An image analysis was used for the interpretation of microstructures of ferrous metal artifacts. For the purposes, various microstructural features such as average grain size, phase area, shape factor, and composition of the inclusions, were parameterized for the information about manufacturing techniques such as casting, heating and tempering. The carbon content was determined through the evaluation of the amount of pearlite phase. As the amount of pearlite phase increased the shape factor also increased. Grain size was relatively smaller in trans-section than in cross-section. The manufacturing direction was trans-sectional because the orientation of inclusions was elongated lengthwise. All inclusions was of silicate groups and the manufacturing temperature was estimated up to $1450^{\circ}C$.

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소결조제 Li2CO3 첨가에 따른 PZW-PMN-PZT 압전 세라믹의 압전 및 유전 특성 (Piezoelectric and Dielectric Properties of PZW-PMN-PZT Piezoelectric Ceramic according to Sintering Aid Li2CO3 Addition)

  • 이갑수;이일하;류주현;류성림
    • 한국전기전자재료학회논문지
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    • 제20권12호
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    • pp.1034-1038
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    • 2007
  • In order to develop the composition ceramics capable of being sintered at low temperature with high piezoelectric properties for multilayer piezoelectric actuator application, PZW-PMN-PZT system ceramics were manufactured according to sintering aid $Li_2CO_3$ addition and their microstructural, dielectric and piezoelectric properties were investigated. The crystal structure of the specimens showed a perovskite phase and no pyrochlore or other second phase was detected. At the sintering temperature of $900\;^{\circ}C,\;0.2\;wt%Li_2CO_3$ added specimen showed a optimum values of kp = 0.562, $d_{33}\;=\;360\;pC/N$ and Qm = 1184, respectively.

스테인리스강 용접부의 잔류응력이 피로특성에 미치는 영향 (Effect of Residual Stress on Fatigue Characteristics at the Welds of Stainless Steel)

  • 권종완;양현태
    • 한국공작기계학회논문집
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    • 제10권5호
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    • pp.110-117
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    • 2001
  • In the weldments, the crack propagation rate is changed due to the residual stress. The crack propagation rate is high in the region with the residual stress. However it shows the same behavior with the base metal in the region that does not include the residual stress. The fatigue crack growth rate for the material with residual stresses can be predicted more precisely by using the effective stress ratio. The difference between experimental results and prediction results seems to be due to the redistribution of the residual stresses and microstructural change.

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