• 제목/요약/키워드: Microstructural control

검색결과 125건 처리시간 0.034초

철 구조물의 부식방지를 위한 Mg-Ca 희생양극의 전기화학적 특성과 제조에 관한 연구 (A Study on the Electrochemical Properties Fabrication Process of Mg-Ca Sacrificial Anode for the Corrosion Protection of Steel Structures)

  • 박강근;김혜성
    • 한국공간구조학회논문집
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    • 제6권4호
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    • pp.73-80
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    • 2006
  • 본 논문은 지하매설 철 구조물의 전기적 부식방지를 위해 Mg 희생양극을 사용하는 부식방지 기술에 대한 연구 또한 활발히 진행되고 있다. Mg 희생양극은 지하에 매설되는 철 구조물(파이프, 탱크, 파일, 고정 앵커 등)을 부식으로부터 보호하기 위하여 사용되는 것이다. 본 연구에서는 종래의 산화 소화용 표면 보호재로 이용되고 있는 비교적 값이 싼 CaCl2 염화물을 이용하여 마그네슘 합금제조 시 CaCl2 염화물의 표면보호 효과 및 제조된 Mg-Ca 합금들의 전기화학적 특성을 조사하였다 금속 Ca가 아닌 산화방지 및 소화 용제로 이용되고 있는 염화물(CaCl2)을 이용하여 자연부식 전위 값이 -1.695VSCE 이하, 사용효율도 59% 이상인 Mg-Mn-Ca 희생양극제의 제조기술을 확립하였다.

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전자부품용 메탈라이즈드 알루미나 세라믹스의 미세구조 제어 (Microsturcture Control of Metallized Alumina Ceramics for Electronic Devices)

  • 조범래
    • 한국재료학회지
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    • 제11권12호
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    • pp.1086-1090
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    • 2001
  • Composition effects on microstructure and metallizing properties of the alumina sintered body were evaluated to develop the metallized alumina tubes having superior properties for electronic devices. SEM observation revealed that resultant micrographs and fractographs were varied with composition chance of additives and $SiO_2$-rich specimens showed better microstructural characteristics with uniform distribution of fine and round particles than other CaO-rich or MgO-rich ones. The resultant interfacial microstructure of the $SiO_2$-rich metallized alumina tubes also showed good metallizing properties with no defects between layers and uniform thickness of metallizing layer.

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An Onboard Measurement System of Ultrasonic Velocity and Attenuation using the Wavelet Transform

  • Cho, Seog-bin;Ha, Sung-kil;Jung, Sung-Yun;Baek, Kwang-ryul
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 2004년도 ICCAS
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    • pp.1826-1828
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    • 2004
  • In this paper, we present an ultrasonic velocity and attenuation measurement system. There are many ultrasonic measurement methods that are used in nondestructive testing applications. They include material property determination, microstructural characterization, and flaw detection. Ultrasonic parameters such as velocity and attenuation are most commonly used in them. Advanced signal analysis which is called "ime-frequency analysis"has been used widely in nondestructive evaluation applications. Wavelet transform is the most advanced technique for processing signals with time-varying spectra. Using the echo waveform gathered by the designed hardware system, we performed simulation of the signal processing algorithms. Then the algorithm is implemented on the system.

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Thermally Sprayed WC-Co 코팅층의 미세조직 및 특성 (Microstructural Characteristics of Thermally Sprayed WC-Co Coatings)

  • 강희수;백경호
    • 한국분말재료학회지
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    • 제16권1호
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    • pp.56-62
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    • 2009
  • The degree of WC decomposition and hardness of thermally sprayed WC-Co coatings are important factors determining the wear resistance of the coatings. In order to minimize the degree of decomposition and to increase hardness, the effects of processing parameters of high velocity oxyfuel(HVOF) spraying on various characteristics of nanostructured WC-12Co coating have been evaluated by an experimental design method. The HVOF sprayed WC-12Co coatings consisted of various carbide phases including WC, $W_2C$ and $W_3Co_3C$, with a much reduced carbon content. The degree of WC decomposition and decarburization was affected by changing barrel length and spray distance. The hardness of WC-Co coatings was strongly related to droplet temperature at substrate, and increased with increasing fuel addition and/or decreasing spray distance. The effective control of processing parameters was discussed in detail for manufacturing a high performance WC-Co coating.

분말 응집체의 치밀화에 관한 모델 (A Model on the Densification of Agglomerates of Powders)

  • 김형섭;이재성
    • 한국분말재료학회지
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    • 제11권4호
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    • pp.301-307
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    • 2004
  • Successful implementation of the powder forming process requires a detailed understanding of several interacting phenomena. The aim is to better control the process variables and to optimize the design parameters. A number of studies were carried out using various constitutive models that take the density change during powder forming into account. Most of them were developed for powders and sintered porous metals, but few of them can describe powder agglomerates, whose behaviour is different from that of uniformly arranged powders. The modification is needed to account for the effect of agglomeration on densification behaviour. Incorporating powder agglomeration into a constitutive model is of considerable importance, as it provides a possibility of relating the powder densification response to microstructural characteristics of powder particles, especially in case of nano powders. In this paper, we proposed a new powder agglomerate model in order to describe the unique densification behaviour of nano powders. The proposed model was applied to the densification of powder agglomerates during cold isostatic pressing.

Steel nitriding optimization through multi-objective and FEM analysis

  • Cavaliere, Pasquale;Perrone, Angelo;Silvello, Alessio
    • Journal of Computational Design and Engineering
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    • 제3권1호
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    • pp.71-90
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    • 2016
  • Steel nitriding is a thermo-chemical process leading to surface hardening and improvement in fatigue properties. The process is strongly influenced by many different variables such as steel composition, nitrogen potential, temperature, time, and quenching media. In the present study, the influence of such parameters affecting physic-chemical and mechanical properties of nitride steels was evaluated. The aim was to streamline the process by numerical-experimental analysis allowing defining the optimal conditions for the success of the process. Input parameters-output results correlations were calculated through the employment of a multi-objective optimization software, modeFRONTIER (Esteco). The mechanical and microstructural results belonging to the nitriding process, performed with different processing conditions for various steels, are presented. The data were employed to obtain the analytical equations describing nitriding behavior as a function of nitriding parameters and steel composition. The obtained model was validated, through control designs, and optimized by taking into account physical and processing conditions.

Control of secondary electron emission coefficient with microstructural change of polycrystalline MgO films

  • Yu, Hak-Ki;Lee, Jong-Lam;Park, Eung-Chul;Kim, Jae-Sung;Ryu, Jae-Hwa
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2008년도 International Meeting on Information Display
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    • pp.1445-1447
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    • 2008
  • Micro crystal structure of polycrystalline MgO film is controlled by adjusting the energy of particles arrived at the substrate during deposition. The change of crystal structure affects on the total area of (200) surface where the oxygen vacancies are formed easily, resulting in the change of secondary electron emission (SEE) coefficient($\gamma$).

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B2형 금속간화합물 β-NiAl중에 α-Cr입자의 석출거동 (Precipitation Behavior of α-Cr Particle in B2-type Intermetallic Compounds β-NiAl)

  • 한창석;김윤채
    • 열처리공학회지
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    • 제9권2호
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    • pp.91-102
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    • 1996
  • Microstructural control to produce multiphase structure has received much attention to improve the high temperature strength as well as low temperature ductility of intermetallics. Transmission electron microscopic investigation has been carried out concerning the effect of Cr-precipitation on the mechanical properties of B2-ordered NiAl containing 4 to 8 mol% of Cr. By aging at temperatures around 973 K after solution annealing, fine spherical precipitates took place homogeneously in the NiAl matrix and the alloys hardened appreciably. Selected area electron diffraction (SAED) patterns have not revealed any additional extra-spots during aging, because the Cr-particles show cube-cube orientation relationship and keep a perfect coherency with the ordered matrix lattice. Dislocations were confirmed to bypass the particles during deformation. Although the dispersion of Cr-particles increased the yield strength of NiAl at intermediate temperature, the strength decreased appreciably at higher temperatures.

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Ti과 Nb에 의한 HSS 작업롤재의 미세조직 제어 (Microstructural Control of High Speed Steel Roll Material with Titanium and Niobium)

  • 김진수;김동규;최진원;이희춘
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 1999년도 제3회 압연심포지엄 논문집 압연기술의 미래개척 (Exploitation of Future Rolling Technologies)
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    • pp.262-271
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    • 1999
  • This work was intended to modify the solidification structure of high speed steel roll material for hot strip mill, by the introduction of alloying elements designed to form primary carbide dispersions via melt treatment procedure. Solidification structure was modified by the melt treatment with titanium and distribution. This modifying effect could be attributed to the fact that the nuclie formed at high temperature upon inoculation induce the formation of fine equiaxed grain and primary carbide during solification, which is also likely to be responsible for the fact that TiC acts as effective nuclie for primary VC solidification.

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분말야금방법으로 제조된 2XXX Al-${SiC}_{p}$ 복합재료의 미세조직과 기계적 성질 (Microstructure and Mechanical Properties of P/M Processed 2XXX Al-${SiC}_{p}$ Composites)

  • 심기삼
    • 한국분말재료학회지
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    • 제4권1호
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    • pp.26-41
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    • 1997
  • The powder metallurgy (P/M) processed 2009 and 2124 Al composites reinforced with SiC particulates were studied by focusing on the effect of consolidation temperature on the microstructural and mechanical Properties. The mechanical properties such as tensile properties and microhardness of the second phases were analysed in relation to the microstructures observed by a SEM and an optical microscope. The in situ fracture process study using SEM showed that the grain refinement and the removal of manganese-containing particles often observed in the 2124 Al-${SiC}_{p}$ composites were important for the improvement of the mechanical properties. This study offers an optimum consolidation temperature for the control of the manganese-containing particles in the 2124 Al-${SiC}_{p}$ composites that yields mechanical properties higher than those of the 2009 Al-${SiC}_{p}$ composites.

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