• Geomechanics and Engineering
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• 제15권4호
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• pp.1005-1016
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• 2018

This paper presents an investigation on the properties of two types of cement kiln dust (CKD)-stabilized dredged sediments, silt and clay with a comparison to hydrated lime stabilization. Unconfined compressive strength (UCS) and California bearing ratio (CBR) tests were conducted to examine the optimal stabilizer content and classify the type of highway material. A strength development model of treated dredged sediments was performed. The influences of various stabilizer types and sediment types on UCS were interpreted with the aid of microstructural observations, including X-ray diffraction and scanning electron microscopy analysis. The results of the tests revealed that 6% of lime by dry weight can be suggested as optimal content for the improvement of clay and silt as selected materials. For CKD-stabilized sediment as soil cement subbase material, the use of 8% CKD was suggested as optimal content for clay, whereas 6% CKD was recommended for silt; the overall CBR value agreed with the UCS test. The reaction products calcium silicate hydrate and ettringite are the controlling mechanisms for the mechanical performance of CKD-stabilized sediments, whereas calcium aluminate hydrate is the control for lime-stabilized sediments. These results will contribute to the use of CKD as a sustainable and novel stabilizer for lime in highway material applications.

• 열처리공학회지
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• 제26권1호
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• pp.14-20
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• 2013

Duplex stainless steel, which is a kind of stainless steel with a mixed microstructure of about equal proportions of austenite and ferrite, is generally known as a unique material with excellent corrosion resistance and high strength. However, toughness, strength, and corrosion resistance of the steel could be reduced due to precipitation of topologically closed packed phases such as sigma phase during cooling. In case of large forged products, they have strong possibility that ${\sigma}$-phase precipitates due to difference of cooling rate between surface and inner of the products. Investigation on sigma phase precipitation behavior of duplex stainless steel with change of cooling rate was carried out in this study. Forged SAF 2205 duplex stainless steel was used as specimens to examine the cooling rate effect. Dissolution behavior of sigma phase was also discussed through resolution test of duplex stainless steel containing lots of sigma phase. Experimental results revealed that impact energy was very sensitive to precipitation of small amount sigma phase. However, sigma phase could be removed by short term resolution treatment and impact resistance of the duplex stainless steel was restored.

• 자원리싸이클링
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• 제21권3호
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• pp.28-38
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• 2012

이 논문에서는 시멘트를 전혀 사용하지 않고 결합재로서 플라이애쉬를 100% 사용한 알칼리 활성 콘크리트를 개발할 목적으로 알칼리 활성화제의 화학적 변화에 따른 모르타르의 압축강도에 미치는 영향과 SEM/ EDS 및 XRD 등의 미세구조 분석을 검토하였다. 그 결과, 몰농도가 높을수록 초기강도에 큰 영향을 미치는 것으로 분석되었고, 압축강도의 크기에 비례하여 $Si^{4+}$ 및 $Al^{3+}$량이 용출되었다. 또한 SEM 및 EDS로 조직을 분석한 결과 모르타르의 조직구조에 큰 영향을 미치는 성분은 Al 및 Si 성분이었고, XRD 분석결과 활성화제 성분차이에 따른 세기(intensity)의 차이는 거의 없는 것으로 나타났다.

• Journal of Welding and Joining
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• 제28권4호
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• pp.73-80
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• 2010

In this work, the effect of welding variables on weldability of gas tungsten arc(GTA) welding was investigated with experimental analysis for a commercial pure(CP) titanium (Grade.1). The GTA welding tests on sheet samples with 0.5mm in thick were carried out at different process variables such as arc length, welding speed and electrode shape. In order to search an optimum arc length with full penetration, bead- on-plate welding before butt-welding were performed with different arc length conditions. From the bead- on-plate welding results, the optimum condition considering arc stability and electrode loss was obtained in the arc length of 0.8mm. Butt-welding tests based on the arc length of 0.8mm were carried out to achieve the optimum conditions of welding speed and electrode shape. Optimum conditions of welding speed and electrode shape were suggested as 10 mm/s and truncated electrode shape, respectively. It was successfully validated by the microstructural observation, tensile tests, micro-hardness tests and formability tests.

• 열처리공학회지
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• 제9권1호
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• pp.34-44
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• 1996

Austenite stainless steel was produced by arc welding with current 650A, voltage 50V and welding speed 10cm/min. It was post-welded and then heat treated at $1,050^{\circ}C$ for 120min. And then it was immersed in water or in air. The microstructural changes, ferrite contents, mechanical properties, and stress corrosion cracking(SCC) were investigated. The SCC was studied in 42wt% boiling $MgCl_2$($140^{\circ}C$) under the constant stress using SCC elongation curve. The results showed that; 1. The as-welded spedimen seemed to increase ${\delta}$-ferrite content largely, and revealed continuous network of lathy and vermicular type. The post-welded heat treatment changed the morphologies of ferrite from continuous type to island type. 2. The as-welded, air and water quenched specimens had the ${\delta}$-ferrite content 9.7%, 3.2% and 2.1% respectively. We also showed that ${\delta}$-ferrite was Cr-rich and Ni-poor by EPMA. 3. The time of failure on the SCC was measured and it was used for corrosion elongation curve. The condition of SCC was investigated under $35kgf/mm^2$ load and the results were as follows; 4. The intergranullar cracking by stress corrosion was most distinct in weld metal while the transgranular cracking occurred in the air cooled specimen.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2015년도 추계학술대회 논문집
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• pp.249-249
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• 2015

Silver films have been of considerable interest for years due to their better performance relative to other metal films for engineering applications. A series of multi-layer silver coatings with different thickness (i.e. 0.3 um to 1.5 um) were prepared on Aluminium substrate containing copper undercoat by direct current (DC) magnetron sputtering method. For the comparative purpose, similar thickness silver coatings were prepared by electrolytic deposition method. Microstructural, morphological, and mechanical characteristics of the silver coatings were evaluated by means of scanning electron microscope (SEM), X-ray diffraction (XRD), Surface roughness test, microhardness test and nano-scratch test. From the results, it has been elucidated that the silver films prepared by DC magnetron sputtering method has superior properties in comparison to the wet coating method. On the other hand, DC magnetron sputtering method is relatively easier, faster, eco-friendly and more productive than the electrolytic deposition method that uses several kinds of hazardous chemicals for bath formulation. Therefore, a New Work Item Proposal (NWIP) for the test methods standardization of DC magnetron sputtered silver coatings has recently been proposed via KATS, Korea and a NP ballot is being progressed within a technical committee "ISO/TC107-metallic and other inorganic coating".

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2005년도 춘계학술대회 논문집
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• pp.287-290
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• 2005

Once hot forgings for automotive parts such as wheel bearing flange to which cyclic asymmetric bending stress is continuously applied are produced, it is necessary to control their microstructure to obtain superior mechanical properties. It is however hard to control the microstructure uniformly because the strength is reduced as coarsening of ferrite grains. To investigate the microstructural alteration according to process variables during hot working, the variation of the ferrite grain size was studied by utilizing of the computer aided servo-hydraulic Gleeble tester which is hot deformation behavior reproduction equipment. In addition, the effect of the ferrite grain size of raw material on the austenite grain behavior of hot forgings was also examined. The rolling contact fatigue resistance of the induction hardened SAE 1055 steel was compared with the occasion of the same condition of SAE52100 bearing steel. As a result, it was confirmed that the ferrite grain sizes of the forgings depend on the heating temperature and cooling start temperature during hot forging and cooling processes. The induction hardened SAE1055 steel showed a superior rolling contact fatigue resistance to the induction hardened SAE52100 steel. The reason is that SAE1055 steel is freer from the material defect such as segregation than the comparative steel.

• 한국재료학회지
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• 제19권6호
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• pp.293-299
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• 2009

The microstructures and mechanical properties of Dual Phase (DP), Transformation-Induced Plasticity (TRIP), and Quenching & Partitioning (Q&P) steels were investigated in order to define the strengthening mechanism of 0.2 C steel. An intercritical annealing between Ac1 and Ac3 was conducted to produce DP and TRIP steel, followed by quenching the DP and TRIP steel being quenched at to room temperature and by the TRIP steel being austemperingaustempered-air cooling cooled the steel toat room temperature, respectively. The Q&P steel was produced from full austenization, followed by quenching to the temperature between $M_s$ and $M_f$, and then enriching the carbon to stabilize the austenite throughout the heat treatment. For the DP and TRIP steels, as the intercritical annealing temperature increased, the tensile strength increased and the elongation decreased. The strength variation was due to the amount of hard phases, i.e., martensite and bainite, respectively in the DP and TRIP steels. It was also found that the elongation also decreased with the amount of soft ferrite in the DP and TRIP steels and with the amount of the that was retained in the austenite phasein the TRIP steel, respectively for the DP and TRIP steels. For the Q&P steel, as the partitioning time increased, the elongation and the tensile strength increased slightly. This was due to the stabilized austenite that was enriched with carbon, even when the amount of retained austenite decreased as the partitioning time increased from 30 seconds to 100 seconds.

• 한국레이저가공학회지
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• 제3권1호
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• pp.29-37
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• 2000

For a development purpose of thick metal / metal Graded-Boundary Materials(GBM), a basic research on the fabrication of Ni-Cr/steel GBM was carried out by a laser beam and its mechanical properties and thermal characteristics were investigated. In order to produce a compositionally graded boundary region between substrate steel and added Ni-Cr alloy, a series of surface alloying treatments was performed with a high power CO$_2$ laser beam. Ni-Cr sheet was placed on a low carbon steel plate(0.18%C), and then a CO$_2$ laser beam was irradiated on the surface to produce a homogeneous alloyed layer. On this first surface-alloyed layer, another Ni-Cr sheet was placed and then the CO$_2$ laser beam was irradiated again to produce second surface-alloyed layer. Sequential repetitions of laser surface alloying treatment 4 times resulted in a graded-boundary region with the thickness of about 1.4mm. Simultaneous concentration profiles of different kinds of alloying elements(Ni and Cr) showed from 42%Ni, 45%Cr and 13%Fe on surface region to 0%Ni, 0%Cr and 99%Fe in substrate region. Also a thermal conductivity gradient resulted in graded-region and its value changed from 0.03㎈/cm s$\^{C}$ in surface region to 0.1㎈/cm s$\^{C}$ in substrate region. Microstructural observation showed that any visible root porosities and solidification shrinkage cracks were not formed in graded region between alloyed layer and substrate region during rapid cooling.

• 한국표면공학회지
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• 제45권3호
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• pp.130-135
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• 2012

Hydrogen charging was electrochemically conducted at high strength DP steels and TRIP steel with varying charging time. The penetration depths and the mechanical properties with charging conditions were investigated through the distribution of micro-hardness and the microstructural observation of the subsurface zone. The micro-Vickers hardness was measured to evaluate the hydrogen embrittlement of subsurface zone in addition to the microscope investigation. It was shown that the hydrogen amounts decreased in DP steels and TRIP steel with increasing hydrogen charging time. As shown by micro-Vickers hardness test and small punch test results, micro-Vickers hardness and SP energy for DP steels and TRIP steel decreased with increasing hydrogen charging time, for constant value of charging current density. SEM investigation results for the hydrogen contained samples showed that the major fracture behavior was brittle fracture which results in dimples on fractured surface and the size of dimples were decreased with increasing hydrogen charging time. These results indicate that hydrogen embrittlement is the major cause for the fracture of high strength steels and also micro-Vickers hardness test and small punch test is a valuable test method for hydrogen embrittlement of high strength sheet steels.