• Title/Summary/Keyword: Microscopic tensile

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The effects of Graphene Oxide flakes on the mechanical properties of cement mortar

  • Kim, Boksun;Taylor, Lawrence;Troy, Andrew;McArthur, Matthew;Ptaszynska, Monika
    • Computers and Concrete
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    • v.21 no.3
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    • pp.261-267
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    • 2018
  • This paper discusses a study of cement mortar reinforced with Graphene Oxide (GO) flakes carried out at the University of Plymouth. Over 60 specimens were prepared and tested to obtain the tensile, compressive and flexural strengths of cement mortar with/without 0.5% GO flakes by weight of cement. The dispersion of the GO flakes and the effect of the use of polycarboxylate ether superplasticizer (0.2% by weight of cement) on the material strength are discussed. Images of the particle sizes of GO are presented from the transmission electron microscopy analysis. In addition, the images from the field emission scanning electron microscope analysis are also presented to show the difference of the microscopic structure of cement mortar with/without GO. The results of the strength tests are presented. It is shown that the inclusion of the GO flakes in general led to positive results, which suggest that GO improved the tensile, compressive and flexural strengths of cement mortar.

Microscopic Investigation of the Strain Rate Hardening for Polycrystalline Metals (철강재료 변형률속도 경화의 미시적 관찰)

  • Yoon, J.H.;Park, C.G.;Kang, J.S.;Suh, J.H.;Huh, M.Y.;Kang, H.G.;Huh, H.
    • Transactions of Materials Processing
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    • v.17 no.1
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    • pp.46-51
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    • 2008
  • Polycrystalline materials such as steels(BCC) and aluminum alloys(FCC) show the strain hardening and the strain rate hardening during the plastic deformation. The strain hardening is induced by deformation resistance of dislocation glide on some crystallographic systems and increase of the dislocation density on grain boundaries or inner grain. However, the phenomenon of the strain rate hardening is not demonstrated distinctly in the rage of $10^{-2}$ to $10^2/sec$ strain rate. In this paper, tensile tests for various strain rates are performed in the rage of $10^{-2}$ to $10^2/sec$ then, specimens are extracted on the same strain position to investigate the microscopic behavior of deformed materials. The extracted specimens are investigated by using the electron backscattered diffraction(EBSD) and transmission electron microscopy(TEM) results which show the effect of texture orientation, grain size and dislocation behavior on the strain rate hardening.

A Study on the Machining Characteristics by the Internal Quality of Heat Resisting Steel (내열강의 내부품질에 따른 절삭가공 특성에 관한 연구)

  • 채왕석
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.9 no.1
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    • pp.24-29
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    • 2000
  • This paper is experimental study of machining characteristics about martensitic heat resisting steel STR11. Machining characteristics are different according to internal quality(chemical compositions, microscopic structure and nonmetallic inclusion) mechanical properties(tensile strength value impact value and hardness) and dynamic cutting force. Following are the results : 1. In analyzing internal quality test materials have typical martensite structure and a minute needle-shaped structure. 2. Tensile strength and reduction of area and hardness are larger. But values of elongation and impact values are smaller. Fracture surface of tensile specimen is ductile. 3, Cutting force is decreasing with cutting speed increasing 4. Cutting force is increasing with feed speed increasing.

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A Study on the Internal Quality and the Machining Characteristics of Martensitic Heat Resisting Steel (마르텐사이트계 내열강의 금속 및 기계적 특성에 관한 연구)

  • 채왕석;권용기;김동현
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1997.04a
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    • pp.1073-1077
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    • 1997
  • In this paper, we have studied internal quality including chemical compositions, microscopic structure and nonmetalic inclusion of test materials. We have analyzed machining characteristics including tensile strength value, impact value, hardness value etcs. Test materials are usd martensitic heat resisting steel, STR11 and STS420J2. The obtined results are as follows : 1. In analyzing internal quality, STR11 and STR420J2 have typical martensite structure and a minute needle-shaped structure. 2. Tensile strength and reduction of area and hardness value are large STR11 than STS420J2. But elongation impact are smaller STR11 than STS420J2. 3. Fracture surface of tensile speciman is ductile in STR11 and STS420J2.

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The Mechanical Appearances and Microscopic Tissue Reactions of the Suture Materials in vivo (생체내 이식된 흡수성 봉합사들의 물리적 성질 변화와 조직 소견에 관한 연구)

  • 김남중;김명철
    • Journal of Veterinary Clinics
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    • v.13 no.2
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    • pp.184-194
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    • 1996
  • A comparative study of three absorbable suture materials of chromic catgut, Dexon II (a polyglycolic acid suture with a polycaprolate coating system) and Coated Vicryl (a polyglactin 910 suture with a glycolide-lactide-calcium stearate coating system) was undertaken in terms of tensile strength, breaking elongation, appearances of the suture materials in the subcutaneous layer of rats and of tissue reaction in the intramuscular layer of rats. The initial tensile strength of chromic catgut and the tensile strength after 21 days were about 1.55 kg and 0.19 kg, respectively. Those of Dexon II were about 2.01 kg and 0. 20 kg, respectively. Those of Coated Vicryl were about 2.39 kg and 0.48 kg, respectively. Coated Vicryl showed the highest tensile strength among the three materials during the whole period. On the other hand, Dexon II showed the highest breaking elongation among the three materials during the first week. But the breaking elongation of Dexon II rapidly continuously decreased during the whole period. The appearances of the suture materials in the subcutaneous layer of rats showed that chromic catgut was the fastest among the three materials, whereas it formed comparatively much connective tissue. The intramuscular absorption rate and tissue reaction of Dexon II were similar to those of Coated Vicryl. The intramuscular absorption rate of these was fairly late when compared with chromic catgut. And the tissue reaction appearance of these showed the formation of a granuloma with foreign body giant cells, macrothages and epitheloid cells by the 28th day in the experimental period.

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HIP Diffusion Bonding of Two Types of Superalloys for Engine Blisk Applications (엔진 블리스크 제조를 위한 초내열합금 이종재의 HIP Diffusion Bonding)

  • 나영상;황형철;염종택;권영삼;박노광
    • Transactions of Materials Processing
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    • v.12 no.1
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    • pp.60-65
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    • 2003
  • HIP diffusion bonding of Ni-based superalloys, cast Mar-M247 (MM247) and Udimet 720 (U720) powder, was experimentally and numerically studied. Subsolvus HIP treatment was optimized by investigating the variations of high temperature tensile properties of HIP-bonded specimens with powder size, HIP'ing time, etc. While the tensile strength at high temperatures showed no detectable changes, the tensile elongation and reduction in area were slightly increased as the powder size decreased from -140 mesh to -270 mesh. While as-HIP'ed U720 showed a high tensile strength comparable to that of lorded U720 alloy, the HIP diffusion-bonded specimen showed a strength lower than the forged U720 alloy and the cast MM247 alloy The increase of HIP'ing tune from 2 hours to 3 hours resulted in a rapid risc of tensile strength and elongation due to the disappearence of microvoids in the cast MM247. FEM simulation for HIP process was conducted by applying the McMeeking micromechanical model, which uses power-law creep model as constitutive equations. ABAQUS user subroutine CREEP with an implemented microscopic model was used for the simulation. Numerical simulation was shown to be essential for the near-net shape manufacturing as well as the HIP process optimization.

Color Change and Tensile Properties of Wood Flour Reinforced Polypropylene Composites; Influence of Photostabilizers

  • Lee, Sun-Young
    • Journal of the Korean Applied Science and Technology
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    • v.26 no.2
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    • pp.171-178
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    • 2009
  • A comparative analysis of the hindered amine light stabilizers (HALS) and UV abosrber (UVA) and their respective photostabilizing effect on wood plastic composites (WPCs) are reported in this study. The influence of accelerated weathering on the mechanical properties of the composites and the microscopic morphology of a degraded layer on the cross section and the surface were studied. UV absorbers were more efficient at preventing composite lightening than was UV stabilizer. The amount of whitening decreased with the increase of photostabilizers. With the addition of a UV absorber (Tinuvin360), the tensile modulus and strength of the composites increased slightly. However, the addition of a light stabilizer (Tinuvin770) and a UV absorber decreased the tensile modulus and strength of the composites. After 250 and 500 hr exposure, tensile modulus and strength of the un stabilized and stabilized composites decreased. The tensile strength of UV absorber (Chimassorb81)-stabilized composites was significantly greater than that of control and light stabilizer (Tinuvin770)- and UV absorber (Tinuvin360)-stabilized composites. UV absorber-stabilized samples showed less whitening and photodegradation than control and light stabilizer-stabilized samples.

A Study on the Microscopic Damage Behavior and the Damage Position Evaluation of TiNi/Al6061 Share Memory Alloy Composite (TiNi/A16061 형상기억복합재료의 미시적 손상거동과 손상위치측정에 관한 연구)

  • Lee, Jin-Gyeong;Park, Yeong-Cheol;Gu, Hu-Taek;Lee, Gyu-Chang
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.9
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    • pp.1787-1794
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    • 2002
  • TiNi alloy fiber was used to solve the problem of the tensile residual stress as the reinforced material. TiNi alloy fiber improves the tensile strength of composite by occurring compressive residual stress in the matrix using shape memory effect. In order to generate compressive residual stress in TiNi/Al6061 shape memory alloy(SMA) composite, 1, 3 and 5% pre-strains were applied to the composite in advance. It was also evaluated the effect of compressive residual stress corresponding to the pre-strain variation and the volume fraction of TiNi alloy. AE technique was used to clarify the microscopic damage behavior at high temperature and the effect of pre-strain in TiNi/Al6061 SMA composite. The results of the microscopic damage evaluation of TiNi/Al6061 SMA composite under various pre-strain using AE technique can be divided into three stage corresponding to the AE signals. AE counts and events were useful parameters to evaluate the fracture mechanism according to the variation of pre-strain. In addition, two dimensional AE source location technique was applied for monitoring the crack initiation and propagation in composite.

Bend Resistance of Polymer Cement Slurry Coated Reinforcing Bars

  • Kim, Wan-Ki;Chang, Sung-Ju;Kim, Hyun-Ki;Soh, Yang-Seob
    • KCI Concrete Journal
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    • v.13 no.2
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    • pp.42-48
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    • 2001
  • The bend resistance of coated reinforcing bar is greatly influenced by both the adhesion strength between bar and coating materials, and the followed transformation of coating material as bars bend. Especially, tearing state or partial microscopic cracks are predicted on the inside and outside of bending angle, because tensile strength and elongation of polymer film are very different according to types of polymer dispersions in bar coating, and these damaged parts are rapidly corroded by penetration of corrosive factors. In this study, polymer cement slurry coated reinforcing bars with various polymer dispersions are prepared by following combined conditions, polymer-cement ratio of 50% and 100%, coating thickness of 250$\mu$m and 450$\mu$m, coating number, curing age of 3, 7, 14 and 28days. Then the specimens are tested for working life and bend resistance at bending angles $90^{\circ}$, $135^{\circ}$and $180^{\circ}$ to observe the microscopic damage effect as the bars bend. Also, epoxy-coated reinforcing bars for control experiment were used with 250$\mu$m of coating thickness. The tensile strength for polymer films is performed. From the test results, the working life of the polymer cement slurry is within 90 seconds. Among four types of polymer dispersion, polymer cement slurry coated reinforcing bar using St/BA-1 emulsion has the excellent bend resistance, which is remarkably improved than that of epoxy-coated reinforcing bar. And the bend resistance is more related to elongation than tensile strength of polymer film. Polymer cement slurry with a polymer-cement ratio of 100%, a coating thickness of $450\mu$m and one coating using St/BA emulsion is selected as a most suitable coating material for coated reinforcing bar.

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Fracture Characteristic of TiNi/A16061 Share Memory Alloy Composite using Acoustic Emission Technique (AE 기법을 이용한 TiNi/A16061 형상기억복합재료의 파괴특성평가)

  • Lee, Jin-Kyung;Park, Young-Chul;Ku, Hoo-Taek;Park, Dong-Sung;Lee, Kyu-Chang
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.2
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    • pp.275-282
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    • 2002
  • Tensile residual stress happen by difference of coefficients of thermal expansion between fiber and matrix is one of the serious problems in metal matrix composite(MMC). In this study, TiNi fiber was used to solve the tensile residual stress as the reinforced material. TiNi fiber improves the tensile strength of composite by occurring compressive residual stress in matrix using shape memory effect of it. Pre-strain was added to generate compressive residual stress inside TiNi/A16061 composite. It was also evaluated the effect of compressive residual stress corresponding to pre-strains variation. AE technique was used to clarify the microscopic damage behavior at high temperature and the effect of pre-strain difference of TiNi/A16061 shape memory alloy composite.