• Journal of the korean academy of Pediatric Dentistry
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• v.24 no.3
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• pp.495-510
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• 1997

The purpose of this study was to evaluate the efficacy of several surface coating agents in preventing microleakage and increasing microhardness of light-cured glass ionomer restoration. 50 and 25 sound molar teeth were used for the microleakage test and microhardness test respectively. Data were analyzed statistically using Kruskal-Wallis and/or Mann-Whitney test. The results of the present study were as follows: 1. The effect of surface coating in reducing microleakage was proven only at the gingival margin of restorations with statistical significance(p<.05). 2. The distribution of microleakage score at gingival margin was shown to be better than that of occlusal margin in general but with no statistically significant differences(p>.05). 3. No statistically significant differences in microhardness could be found between groups (p>.05) regardless of depth of measurement. 4. Under the present experimental conditions, the types or application of surface coating agents did not impose any significant effect on microhardness of glass ionomer restorative material whereas the protective effect of surface coating in reducing microleakage was partly proven.

• Journal of the korean academy of Pediatric Dentistry
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• v.25 no.2
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• pp.312-322
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• 1998

There are many concerns about the erosive effect of acidic beverage. In this study, the erosive effect of bovine enamel caused by $Pepsi-Cola^{(R)}$(pH 2.41) and rehardening effect by intraoral exposure were determined by microhardness test and SEM. The bovine enamel specimen was imbedded in 100ml $Pepsi-Cola^{(R)}$ during 5 minutes and exposed to the intraoral environment with removable resin plate. The microhardness test was performed after 1 hr, 24 hrs, and 48 hrs. The results obtained from this study can be summarized as follows ; 1. The microhardness value was significantly (p<0.05) reduced by cola beverage, and significantly (p<0.05) increased after 1 hr and 24 hrs respectively. 2. The difference in the microhardness between 24 hrs group and 48 hrs group was not significant (p>0.05) and microhardness value of 48 hrs group was significantly less than that of initial group (p<0.05). 3. The erosive effect of cola beverage and remineralization effect by intraoral exposure were visualized by the SEM photo. But, the enamel surfaces did not return to their original state.

• Journal of the korean academy of Pediatric Dentistry
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• v.24 no.4
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• pp.719-726
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• 1997

The aim of this study was to evaluate the in vitro effects of exposure to acidic beverages on microhardness of enamel and dentin. Thirty enamel specimens and thirty dentin specimens were obtained from extracted bovine maxillay incisiors. Enamel and dentin specimens were divided into three groups and treated with acidic beverages as follows; Group 1 : cola(pH 2.52), Group 2 : plain soda water(pH 2.93) and Group 3 : orange juice(pH 3.75). Erosive treatment was performed by storing each specimens for 5 min in 50ml solution of cola, soda water and orange juice. Average microhardness values(VHN) were determined before and after erosive treatment. All beverages produced significant loss of microhardness of enamel and dentin. Microhardness of enamel was reduced in the following order: Group 1 : $42.71{\pm}4.36(%)$, Group 2 : $37.09{\pm}6.25(%)$, Group 3 : $35.46{\pm}4.98(%)$. Microhardness of dentin was reduced in the following order: Group 1 : $17.14{\pm}3.42(%)$, Group 2 : $13.89{\pm}3.18(%)$, Group 3 : $13.82{\pm}3.50(%)$. The differences between group 1 and group 2, 3 were statistically significant(p< 0.05).

• Restorative Dentistry and Endodontics
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• v.17 no.1
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• pp.126-133
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• 1992

Tooth colored resin restorative materials are widely used in anterior teeth restorations. The color instability of resin was the main cause of failure in resin restorations. The purpose of this study was to investigate color stability and microhardness of serval visible light curing resins. Colorimetric measurements(Tokyo Denshoku Co., Japan) and microhardness tests(Matusuzawa, MXT 70, Japan) were made on six composite resins before and after controlled immersion treatments. The six composite resins were BIS - FILM(BISCO, USA), Durafill(Kulzer, Germany), Helioprogess(VIVADENT, Germany), Palfique(TOKUYAMA SODA, Japan), Silux(3M, USA), Photoclearfil(KURARAY, Japen). Six light curing resins showed significant color change after 2 weeks. Palfique exhibited the hightest $dE^*$ values and Helio progress presented the lowest $dE^*$ values. Photoclearfil showed the highest microhardness value. Durafill and Helio progress showed lower microhardness values. Microhardness values were decreased after 8 weeks in Bisfil, Palfique light, and Photoclearfil.

• Journal of the korean academy of Pediatric Dentistry
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• v.51 no.2
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• pp.165-175
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• 2024

This study aimed to investigate the effects of blood contamination on the Vickers hardness and the surface morphology of premixed MTA and compare them with the effects on conventional MTA. The Vickers microhardness of Endocem MTA Premixed Regular (EP) and ProRoot MTA (PM) was assessed after immersion in fetal bovine serum (FBS) and saline. Stem cells from human exfoliated deciduous teeth (SHED) were seeded on MTA after immersion in FBS, saline, and deionized water (DW). Cell adhesion patterns and surface morphology were visualized via scanning electron microscopy (SEM). The surface microhardness of EP and PM in FBS was lower than in saline. However, short-term exposure of PM to FBS did not reduce the microhardness compared to saline. Angular crystals formed in water, while rounded crystals with more air voids appeared in FBS. Favorable SHED attachment occurred in all groups. Overall, the surface hardness of EP and PM decreased after FBS exposure, although PM was less influenced. We suggest minimizing the amount of bleeding when using MTA clinically; nevertheless, PM remains an option with more expected blood contamination than EP. In summary, exposure to FBS decreased mechanical performance but allowed cell adhesion for both MTAs, with PM being more resistant to these changes.

• Proceedings of the Materials Research Society of Korea Conference
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• 2010.05a
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• pp.26.1-26.1
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• 2010

Ni-SiC nano composite coatings were fabricated using electrodeposition technique with the aid of ultrasound. The properties of the nano composite were investigated by using SEM, XRD, Wear test and Vicker's microhardness test. The results demonstrated that the microhardness of composite coatings under ultrasonic condition was improved significantly as compared to conventional electrodeposition techniques without ultrasound. The nano particles were found to be distributed homogeneously with reduced agglomeration. The synergistic combination of superior wear resistance and improved microhardness was found in ultrasonicated conditions to the Ni-SiC nano composite coatings.

• The korean journal of orthodontics
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• v.48 no.1
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• pp.48-56
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• 2018

Objective: The purpose of this study was to determine the effects of carbonated water on etched or sealed enamel according to the carbonation level and the presence of calcium ions. Methods: Carbonated water with different carbonation levels was manufactured by a soda carbonator. Seventy-five premolar teeth were randomly divided into a control group and 4 experimental groups in accordance with the carbonation level and the presence of calcium ions in the test solutions. After specimen preparation of the Unexposed, Etched, and Sealed enamel subgroups, all the specimens were submerged in each test solution for 15 minutes three times a day during 7 days. Microhardness tests on the Unexposed and Etched enamel subgroups were performed with 10 specimens from each group. Scanning electron microscopy (SEM) tests on the Unexposed, Etched, and Sealed enamel subgroups were performed with 5 specimens from each group. Microhardness changes in different groups were statistically compared using paired t-tests, the Wilcoxon signed rank test, and the Kruskal-Wallis test. Results: The microhardness changes were significantly different between the groups (p = 0.000). The microhardness changes in all experimental groups except Group 3 (low-level carbonated water with calcium ions) were significantly greater than those in the Control group. SEM showed that etched areas of the specimen were affected by carbonated water and the magnitude of destruction varied between groups. Adhesive material was partially removed in groups exposed to carbonated water. Conclusions: Carbonated water has negative effects on etched or sealed enamel, resulting in decreased microhardness and removal of the adhesive material.

• Journal of Korean society of Dental Hygiene
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• v.12 no.3
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• pp.533-541
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• 2012

Objectives : The purpose of this study was to evaluate the effects of tooth bleaching agent contained 35% hydrogen peroxide on the color, microhardness and surface roughness of tooth-colored restorative materials. Methods : Four types of tooth-colored restorative materials, including a composite resin(Filtek Z350 ; Z350), a flowable composite resin(Filtek P60 : P60), a compomer(Dyract$^{(R)}$ AP ; DY), and a glass-ionomer cement(KetacTM Molar Easymix ; KM) were used in the study. The specimens($8mm{\times}5mm$) were made by using a customized acrylic mold. Each material was divided into two groups equally(n=40) : experimental group(35% HP) and control group(distilled water). 35% HP group was treated 30 mim/5 days for 15 days. Each 30 minute treatment session consisted of two 15 minute cycles of gel application with 20 second light exposure. The authors measured the color, microhardness, and roughness of the specimens before and after bleaching. The data were analyzed with ANOVA and T-test. Results : 35% HP group showed an apparent color change(${\Delta}E^*$) than control group. In particular, DY and KM showed a noticeable color change and statistically significant differences(p<0.05). 35% HP group showed a reduction in microhardness. Z350 and P60 does not have a statistically significant difference(p>0.05), DY and KM showed a statistically significant difference(p<0.05). Percentage microhardness loss(PML) of control group was 0.6 to 5.5% in the group, 35% HP group was 6.6 to 34.6%. Roughness was increased in 35% HP group after bleaching. Especially DY and KM were significantly increased(p<0.05). Conclusions : Bleaching agents may affect the surface of existing restorations; therefore, they should not be used indiscriminately when tooth-colored restorations are present.

• The Journal of the Korea Contents Association
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• v.13 no.10
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• pp.427-433
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• 2013

The aim of this study was to evaluate the efficacy of bleached tooth with white toothpaste on the whitening effect, microhardness test. Forty-four human interior teeth were randomly assigned to two groups as follows: Group 1 was used general toothpaste as control, Group 2 exposed to white toothpaste at 3 times a day for 3 minutes. The total application time was 4 weeks. After each application, all tooth were washed with distilled water and immersed in artificial saliva. The color change and microhardness were measured using CIELab Color system and microhardness tester. The data were analyzed by student t-test, using SPSS 20.0 statistical computer program (SPSS Inc., USA). The overall color changes (${\Delta}E$) by white toothpaste have a capability of the whitening efficacy by factor of 2.3 times larger compared with general toothpaste. Moreover, the application of white toothpaste did not cause any microhardness reduction on enamel surface.

• Restorative Dentistry and Endodontics
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• v.43 no.3
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• pp.27.1-27.9
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• 2018

Objectives: The aim of this in vitro study was to evaluate the effects of the thickness and shade of 3 types of computer-aided design/computer-aided manufacturing (CAD/CAM) materials. Materials and Methods: A total of 120 specimens of 2 shades (A1 and A3) and 2 thicknesses (1 and 2 mm) were fabricated using VITA Mark II (VM; VITA Zahnfabrik), IPS e.max CAD (IE; IvoclarVivadent), and VITA Suprinity (VS; VITA Zahnfabrik) (n = 10 per subgroup). The amount of light transmission through the ceramic specimens was measured by a radiometer (Optilux, Kerr). Light-cured resin cement samples (Choice 2, Bisco) were fabricated in a Teflon mold and activated through the various ceramics with different shades and thicknesses using an LED unit (Bluephase, IvoclarVivadent). In the control group, the resin cement sample was directly light-cured without any ceramic. Vickers microhardness indentations were made on the resin surfaces (KoopaPazhoohesh) after 24 hours of dark storage in a $37^{\circ}C$ incubator. Data were analyzed using analysis of variance followed by the Tukey post hoc test (${\alpha}=0.05$). Results: Ceramic thickness and shade had significant effects on light transmission and the microhardness of all specimens (p < 0.05). The mean values of light transmittance and microhardness of the resin cement in the VM group were significantly higher than those observed in the IE and VS groups. The lowest microhardness was observed in the VS group, due to the lowest level of light transmission (p < 0.05). Conclusion: Greater thickness and darker shades of the 3 types of CAD/CAM ceramics significantly decreased the microhardness of the underlying resin cement.