• 제목/요약/키워드: Micro-structural property

검색결과 44건 처리시간 0.028초

라만 분광법을 활용한 마모 중 DLC 코팅의 구조적 변화 조사 (Investigation of Structural Change of DLC Coating during Frictional Wear by Raman Spectroscopy)

  • 김송희;장재철
    • 한국표면공학회지
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    • 제52권1호
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    • pp.16-22
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    • 2019
  • The structural change of DLC coatings during long-term wear test and dicing test under the low loading condition was investigated. DLC coatings were applied for the precision injection molds of a modified SNCM steel for the extension of life and the micro-diamond blades for the high cutting efficiency and the increase in life. A ball-on-disc wear tests in the mold steel and a dicing tests in the micro-diamond blades were conducted to understand degradation of DLC coatings. The degradation of DLC coatings for the injection mold steel and the micro-diamond blades during the wear and dicing tests were studied with Raman Spectroscopy. Raman peaks were divided two bands(D band and G band) to study the degradation process of DLC structure. By the wear test, polished condition of wear marks were observed to be maintained until 10 hrs of wear test period is given, but small striation marks appeared in 20 hours wear test. It was observed that $I_D/I_G$ ratios changed as the degradation of DLC coatings is proceeded during the wear tests and the dicing tests. It is suggested that the change in $I_D/I_G$ value possibly reflected from the composition of $sp^2$ and $sp^3$ bondings in DLC layers relevant to the change in mechanical and physical property.

화학기상증착 및 마그네트론 스퍼터링 방법으로 증착된 절연박막의 물성 분석 및 전기적 특성 (Characterization of microstructures and electrical properties of insulating thin films deposited by PECVD and RF magnetron sputtering)

  • 윤상한;이재엽;박창균;서수형;김용상;박진석
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1999년도 하계학술대회 논문집 D
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    • pp.1707-1709
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    • 1999
  • Insulating thin films for strain gauge application, such as $SiO_2$ single layers and $SiO_2/Si_3N_4$ multilayers, are deposited by using both PECVD and RF magnetron sputtering techniques. Micro-structural analysis and electrical characterization are carried out on those films. It has been observed that PECVD films have a smoother surface and a denser micro-structure than sputter films. It should be also found out that the electrical insulation property of $SiO_2$ film can be significantly improved by adding the $Si_3N_4$ layer.

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Effects of nano-silica and micro-steel fiber on the engineering properties of ultra-high performance concrete

  • Hakeem, Ibrahim Y.;Amin, Mohamed;Abdelsalam, Bassam Abdelsalam;Tayeh, Bassam A.;Althoey, Fadi;Agwa, Ibrahim Saad
    • Structural Engineering and Mechanics
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    • 제82권3호
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    • pp.295-312
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    • 2022
  • This study investigates the effects of nano silica (NS) and micro steel fiber on the properties of ultra-high-performance concrete (UHPC). The experimental consists of three groups, each one with five percentages of NS content (0%, 2%, 4%, 6% and 8%) in addition to the 20% silica fume and 20% quartz powder proportioned according to the weight of cement added to the mixtures. In addition, three percentages of micro steel fibers (0%, 1% and 2%) were considered. Different mixtures with varying percentages of NS and micro steel fibers were prepared to set the water-to-binder ratio, such as 0.16% and 1.8% superplasticizer proportioned according the weight of the binder materials. The fresh properties, mechanical properties and elevated temperatures of the mixtures were calculated. Then, the results from the microstructure analyses were compared with that of the reference mixtureand it was found that 6% replacement of cement with NS was optimum replacement level. When the NS content was increased from 0% to 6%, the air content and permeability of the mixture decreased by 35% and 39%, the compressive and tensile strength improved by 21% and 18% and the flexural strength and modulus of elasticity increased by 20% and 11.5%, respectively. However, the effect of micro steel fibres on the compressive strength was inconclusive. The overall results indicate that micro steel fibres have the potential to improve the tensile strength, flexure strength and modulus of elasticity of the UHPC. The use of 6% NS together with 1% micro-steel fiber increased the concrete strength and reduce the cost of concrete mix.

Nano 및 Micro 크기의 Fe3O4 분말이 첨가된 열경화성 에폭시 접착제의 유도가열 및 접착 특성 (Heating Behavior and Adhesion Property of Epoxy Adhesive with Nano and Micro Sized Fe3O4 Particles)

  • 황지원;임태규;최승용;이남규;손민영
    • Composites Research
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    • 제33권2호
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    • pp.55-60
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    • 2020
  • 구조용 일액형 에폭시 접착제에 나노 및 마이크로 크기의 Fe3O4 분말을 첨가하여 유도가열용 접착제를 제조하였고, 제조된 접착제를 이용하여 GFRP 피착재의 두께 및 Fe3O4 분말의 첨가량 변화에 따른 가열 성능을 평가하였다. 실험 결과, 접착제의 승온 거동이 유도 가열로 가열한 경우 오븐경화에 비해 GFRP 피착재의 두께에 영향을 작게 받는 것이 관찰되었으며 접착제 내의 Fe3O4 분말의 함량이 증가할수록 가열 속도와 전단 강도가 증가하는 경향을 나타냈다.

슈퍼 듀플렉스 스테인리스강 다층용접부의 미세조직 및 공식(Pitting Corrosion)에 미치는 용접열사이클의 영향 (Effect of Welding Thermal Cycle on Microstructure and Pitting Corrosion Property of Multi-pass Weldment of Super-duplex Stainless Steel)

  • 남성길;박세진;나혜성;강정윤
    • Journal of Welding and Joining
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    • 제28권4호
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    • pp.18-25
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    • 2010
  • Super-duplex stainless steels (SDSS) have a good balance of mechanical property and corrosion resistance when they consist of approximately equal amount of austenite and ferrite. The SDSS needs to avoid the detrimental phases such as sigma(${\sigma}$), chi(${\chi}$), secondary austenite(${\gamma}2$), chromium carbide & nitride and to maintain the ratio of ferrite & austenite phase as well known. However, the effects of the subsequent weld thermal cycle were seldom experimentally studied on the micro-structural variation of weldment & pitting corrosion property. Therefore, the present study investigated the effect of the subsequent thermal cycle on the change of weld microstructure and pitting corrosion property at $40^{\circ}C$. The thermal history of root side was measured experimentally and the change of microstructure of weld root & the weight loss by pitting corrosion test were observed as a function of the thermal cycle of each weld layer. The ferrite contents of root weld were reduced with the subsequent weld thermal cycles. The pitting corrosion was occurred in the weld root region in case of the all pitted specimen & in the middle weld layer in some cases. And the weight loss by pitting corrosion was increased in proportional to the time exposed at high temperature of the root weld and also by the decrease of ferrite content. The subsequent weld thermal cycles destroy the phase balance of ferrite & austenite at the root weld. Conclusively, It is thought that as the more subsequent welds were added, the more the phase balance of ferrite & austenite was deviated from equality, therefore the pitting corrosion property was deteriorated by galvanic effect of the two phases and the increase of 2nd phases & grain boundary energy.

마이크로기포제를 사용한 콘크리트의 열적 특성에 관한 연구 (Study on the Thermal Characteristics of Concrete Using Micro Form Admixture)

  • 박영신;김정호;전현규;서치호
    • 한국구조물진단유지관리공학회 논문집
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    • 제17권2호
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    • pp.101-109
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    • 2013
  • 최근 전세계는 급격한 기후조건과 환경변화에 의해 냉난방 에너지 사용이 증가되고 있으며 이는 화석 연료 사용량 증가와 함께 $CO_2$ 배출량 상승, 지구 온난화 등 환경과 에너지에 대한 수많은 문제를 유발하고 있어 세계 각국은 온실가스 배출 및 에너지 소비 감소를 위한 대응책을 마련하고 있다. 우리나라 또한 정부의 '저탄소 녹색 성장' 및 '친환경 주택 건설기준 및 성능' 등의 정책을 선포하는 등 건물 부분에 있어 환경과 에너지 관리에 대한 노력을 하고 있다. 우리나라의 총 에너지 소비량 중 건물 부문이 차지하는 비율은 약 25%에 달하며 다른 산업 분야에 비해 연간 에너지 소비 증가율이 높은 편이다. 건물에서 에너지 손실이 가장 큰 부위는 외피로서, 이 부분의 에너지 손실을 감소하기 위한 연구가 활발히 진행되고 있으나 이는 대부분 창호 및 단열재를 사용한 연구이며 건물 외피의 70% 이상을 차지하고 있는 콘크리트에 대한 연구는 미미한 실정이다. 따라서 건물의 에너지 손실을 최소화하기 위해서는 콘크리트 자체에서 단열성능을 확보할 수 있어야 하며 이에 대한 연구가 필요하다. 따라서 본 연구는 콘크리트의 단열성능을 확보하면서 구조용으로 사용이 가능한 콘크리트를 개발하기 위한 실험을 진행하였다. Test 1의 실험결과로써, Micro Foam Admixture (MFA)를 사용한 콘크리트는 슬럼프 경시변화가 개선되었으며, MFA의 혼입율을 증가할 경우 압축강도는 감소되고 열전도율은 증가되는 결과를 나타내었다. Test 2의 실험결과에서는 물시멘트비 변화시 물시멘트비 증가에 따라 압축강도는 감소하였고 열전도율은 증가하였다. 그러나 잔골재율 변화에 대한 물성 및 열적 특성은 큰 차이를 나타내지 않았다.

Motion behavior research of liquid micro-particles filtration at various locations in a rotational flow field

  • Yan, Yan;Lin, Yuanzai;Cheng, Jie;Ni, Zhonghua
    • Structural Engineering and Mechanics
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    • 제62권2호
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    • pp.163-170
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    • 2017
  • This study presents a particle-wall filtration model for predicting the particle motion behavior in a typical rotational flow field-filtration in blower system of cooker hood. Based on computational fluid dynamics model, air flow and particles has been simulated by Lagrangian-particle/ Eulerian-gas approaches and get verified by experiment data from a manufacturer. Airflow volume, particle diameter and local structure, which are related to the particle filtration has been studied. Results indicates that: (1) there exists an optimal airflow volume of $1243m^3/h$ related to the most appropriate filtration rate; (2) Diameter of particle is the significant property related to the filtration rate. Big size particles can represent the filtration performance of blower; (3) More than 86% grease particles are caught by impeller blades firstly, and then splashed onto the corresponding location of worm box internal wall. These results would help to study the micro-particle motion behavior and evaluate the filtration rate and structure design of blower.

렌즈 구동을 위한 선형 초음파 전동기 설계 (Design of Linear Ultrasonic Motor for Small tong Actuation)

  • 권태성;이승엽;김수경
    • 정보저장시스템학회:학술대회논문집
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    • 정보저장시스템학회 2005년도 추계학술대회 논문집
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    • pp.190-194
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    • 2005
  • There is a great demand of micro-actuators for mobile information devices such as SFF optical drives and mobile camera phones. However, conventional magnetic coils of electromagnetic motors are a major obstacle for miniaturization because of their complicated structures and large power consumption. In this paper, a linear ultrasonic motor to actuate focusing lens of mobile devices is proposed. The new actuator uses a ring type bimorph piezoelectric material, and $d_{31}$ mode is adopted for applying linear motion. The interaction between inertia force and friction force makes linear motion by high-frequency saw signal input. The saw signal gives steady forces on the one direction by asymmetric inclination property of the signal itself on time domain. A commercial FEM (ANSYS) was used in this investigation for simulating structural analysis, identification of dynamic property, such as resultant displacement and coupled analysis with piezoelectric material. To evaluate the performance of the new design, a prototype was manufactured and experiments were carried out. Experimental results show the actuator motion of 1.52 mm/s at 10 kHz input signal in 5 V.

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초소형 렌즈 구동을 위한 선형 초음파 구동기 설계 (Design of a Linear Ultrasonic Actuator for Small Lens Actuation)

  • 권태성;최요한;이승엽
    • 정보저장시스템학회논문집
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    • 제2권4호
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    • pp.251-256
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    • 2006
  • There is a great demand of micro-actuators for mobile information devices such as SFF optical drives and mobile phone cameras. However, the magnetic coils used in conventional electromagnetic motors are a major obstacle for the miniaturization because of their complicated structures and large power consumption. In this paper, a linear ultrasonic motor to actuate focusing lens of mobile devices is proposed. The new actuator uses a ring type bimorph piezoelectric material, and $d_{31}$ mode is adopted for applying linear motion. The interaction between inertia force and friction force makes linear motion by high-frequency saw signal input. The saw signal gives steady forces on the one direction by asymmetric inclination property of the signal itself on time domain. A commercial FEM(ANSYS) was used in this investigation for simulating structural analysis, identification of dynamic property, such as resultant displacement and coupled analysis with piezoelectric material. To evaluate the performance of the new design, a prototype was manufactured and experiments were carried out. Experimental results show the actuator motion of 5.4 mm/s at 10V saw signal of 41 kHz.

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탄성형 에폭시의 흡습 열화에 따른 열적 및 기계적 특성에 관한 연구 (A Study on Thermal and Mechanical Properties of Elastic Epoxy with Water Aging)

  • 이관우;민지영;한기만;최용성;박대희
    • 대한전기학회논문지:전기물성ㆍ응용부문C
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    • 제53권6호
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    • pp.293-299
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    • 2004
  • In this paper, thermal and mechanical properties of electric epoxy with water aging were discussed. We made elastic epoxy specimen adding a ratio of 0〔phr〕20〔phr〕, 35〔phr〕 and 53〔phr〕 with modifier to existing epoxy. We studied mechanical property of elastic resin after absorption in water from 0 to 484 hours. As a result, diffusion factor of elastic epoxy showed 20-21${\times}$10$^{-4}$ $\textrm{mm}^2$/s and general epoxy showed 9.5${\times}$10$^{-4}$ $\textrm{mm}^2$/s. Elastic property increased linearly according to addiction and decreased according to water absorption. Tensile strength was reduced according to addition. It was affected by water absorption of micro-void of elastic epoxy. Hardness inclined to decrease after increasing according to absorbed time. In water-absorption state, it was experimented a change of heat flow by temperature of elastic epoxy and change of thermal expansion coefficient. DSC (Differential Scanning Calorimetry) and TMA (Thermomechanical Analysis) equipments were used to measure Tg. A temperature ringe of DSC was from -0($^{\circ}C$) to 200($^{\circ}C$). One of TMA was from -0($^{\circ}C$) to 350($^{\circ}C$). In addition, we investigated structural analysis of water absorbed specimen using SEM (Scanning Electron Microscope).