• 제목/요약/키워드: Micro-Tube

검색결과 301건 처리시간 0.023초

Material Properties of Ni-P-B Electrodeposits for Steam Generator Tube Repair

  • Kim, Dong Jin;Seo, Moo Hong;Kim, Joung Soo
    • Corrosion Science and Technology
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    • 제3권3호
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    • pp.112-117
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    • 2004
  • This work investigated the material properties of Ni-P-B alloy electrodeposits obtained from a Ni sulfamate bath as a function of the contents of the P and B sources($H_3PO_3$ and dimethyl amine borane complex(DMAB), respectively) with/without additives. Chemical composition, residual stress, microstructure and micro hardness were investigated using ICP(inductively coupled plasma) mass spectrometer, flexible strip, XRD, TEM and micro Vickers hardness tester, respectively. From the results of the compositional analysis, it was observed that P and B are incorporated competitively during the electrodeposition and the sulfur from the additive is codeposited into the electrodeposit. The measured residual stress value increased in the order of Ni, Ni-P, Ni-B and Ni-P-B electrodeposits indicating that boron affects the residual tensile stress greater than phosphorus. As the contents of the alloying element sources of P and B increased, crystallinity and the grain size of the electrodeposit decreased. The effect of boron on crystallinity and grain size was also relatively larger than the phosphorus. It can be explained that the boron with a smaller atomic radius contributes to the increase of residual stress in the tensile direction and the larger restraining force against the grain growth more significantly than the phosphorus with a larger atomic radius. Introduction of an additive into the bath retarded crystallization and grain growth, which may be attributed to the change of the grain growth kinetics induced by the additive adsorbed on the substrate and electrodeposit surfaces during electrodeposition.

이상 유동 수치해석을 이용한 기포 구동 생물 반응기 내부 최적 구조에 관한 연구 (Study on optimum structure of air-lift bio-reactor using numerical analysis of two-phase flow)

  • 김산;정지홍;이재원;손동기;고한서
    • 한국가시화정보학회지
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    • 제17권3호
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    • pp.24-31
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    • 2019
  • Recently, an air-lift bio-reactor operated by micro bubbles has been utilized to product hydrogen fuel. To enhance the performance, characteristics of hydrodynamics inside the bio-reactor were analyzed using a numerical simulation for two-phase flow. An Eulerian model was employed for both of liquid and gas phases. The standard k-ε model was used for turbulence induced by micro bubbles. A Population Balance Model was employed to consider size distribution of bubbles. A hollow cylinder was introduced at the center of the reactor to reduce a dead area which disturbs circulation of CO bubbles. An appropriate diameter of the draft tube and hollow cylinder were optimized for better performance of the bio-reactor. The optimum model could be obtained when the cross-sectional area ratio of the hollow cylinder to the reactor, and the width ratio of the riser to the downcomer approached 0.4 and 3.5, respectively. Consequently, it is expected that the optimum model could enhance the performance of the bio-reactor with the homogeneous distribution and higher density of CO, and more effective mixing.

반응소결법으로 제조한 Al기 복합재용 Fe-Al합금 예비성형체의 특성평가 (Characteristic Evaluation of the Fe-Al Alloy Preform Fabrication by Reactive Sintering Process for the Al Matrix Composites.)

  • 최답천;박성혁;주형곤
    • 한국주조공학회지
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    • 제19권6호
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    • pp.493-500
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    • 1999
  • Squeeze casting was used for fabricating a light metal base composite having high strength and wearresistance. Reactive sintering was used to prepare the preform of Squeeze casting. To utilize Fe-Al intermetallic compounds and SiC particle as a reinforcement, there needs to prepare Fe-Al mixed powder at 50, 60, 70at.%Al, and add SiC powder to the above mixture at 4, 7, 16, 24wt.%. The prepared mixture with SiC was reactive sintered in a tube furnace at $660^{\circ}C$ to get a porous hybrid preform of intermetallic compound and SiC. The preform prepared above was placed in a metal mold, preheated at $660^{\circ}C$ AC4C matrix was injected into the mold with the temperature of the melt at $610^{\circ}C$ After these processes, 66MPa was applied to the mold for 5 minute to finish the whole procedure. The maximum reaction temperature was increased with the increased Al amount, but decreased with the increased SiC amount. The density of the preform was decreased with SiC amount increase in the compacts due to swelling of the preform. An optical microscope was applied to observe the micro structure and the dispersion of the reinforcements. To analyze phases, We utilized XRD, EDS. Hardness test were chosen to get the information of mechanical properties. There were no significant changes in micro structure between the composite and preform. However, it was shown that uniform dispersion of the reinforcers and complete infiltration of the melt into the preform were achieved through the procedure of the squeeze casting. It was observed that the hardness of the composite is decreased with increased SiC amount, resulting from the volumetric expansion of the preform.

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Molecular Imaging of Arthritis in the Angiogenic Vasculature Using A 123I-Vascular Endothelial Growth Factor Receptor Antibody

  • Kim, Sung-Min;Choi, Na-Eun;Song, Young-Kyu;Cho, Gyung-Goo;Bang, Jeong-Kyu;Kim, Sang-Mi;Lee, Sang-Hoon;Ryu, Eun-Kyoung
    • Bulletin of the Korean Chemical Society
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    • 제33권6호
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    • pp.1890-1894
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    • 2012
  • Vascular endothelial growth factor (VEGF) and its receptor (VEGFR) have been implicated in the pathogenesis of rheumatoid arthritis, which is angiogenesis dependent. Antibody-based molecular imaging improves targeting, and antibody radiolabeling is useful for monitoring biological events $in$ $vivo$ $via$ PET or SPECT. We investigated the potential of molecular imaging to diagnose arthritis with VEGFR-2 $in$ $vivo$. The $^{123}I$-VEGFR-2 antibody was prepared by the iodogen tube method. The radioligand was injected into arthritic mice, and micro SPECT/CT was performed. The arthritic mice were examined by 4.7-T MRI and immunohistochemistry. The $^{123}I$-VEGFR-2 antibody showed high uptake in the arthritic region at 1 h postinjection on SPECT/CT but no uptake in the control animals after radioligand injection. In MR images, the arthritic tissue of the mice was correlated with regions labeled by the $^{123}I$-VEGFR-2 antibody. Immunohistochemical localization showed markedly increased expression of VEGFR-2 in the endothelial cells, fibroblasts, and macrophages of the arthritic mice.

원추형 금속 기판의 팁 각도에 따른 탄소 나노튜브 이미터의 전계방출 특성 (Field-emission characteristics of carbon nanotube emitters in terms of tip angles of conical-type metal substrates)

  • 김종필;노영록;장한빛;박진석
    • 반도체디스플레이기술학회지
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    • 제10권2호
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    • pp.115-119
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    • 2011
  • A tip-type carbon nanotube(CNT)-based field emitter was studied to consider it as electron source for micro-focused x-ray tube. The CNT was grown directly on a metal (tungsten) substrate by using an inductively coupled plasma-chemical vapor deposition (ICP-CVD) method. Prior to CNT growth, the metal substrate was etched to have various tip angles from $10^{\circ}$ to $180^{\circ}C$ (flat-type). The morphologies and microstructures of all the grown CNTs were analyzed via field-emission SEM. Furthermore, the effects of substrate tip-angles on the emission properties of CNT-based field emitters were characterized to estimate the maximum current density, the turn-on voltage, and the spatial distribution of electron beams. Prolonged long-term stability testing of the CNT emitters was also performed. All the experiment results obtained from this study indicated why a tip-type CNT emitter, compared with a flat-type CNT emitter, would be more desirable for a micro-focused x-ray system, in terms of the emission current level, the focused beam area, and the emission stability.

수소취화된 CANDU 압력관 재료의 파괴강도 평가를 위한 SP시험에 관한 연구 (A Study on the Small Punch Test for Fracture Strength Evaluation of CANDU Pressure Tube Embrittled by Hydrogen)

  • 노승환;옹장우;유효선;정세희
    • 비파괴검사학회지
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    • 제15권4호
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    • pp.549-560
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    • 1996
  • 본 연구의 목적은 지금까지 적용되지 않은 극소형시험편을 이용한 소형펀치(small punch : SP)시험과 비파괴시험방법(non-destructive test: NDT)으로 알려진 음항방출(acoustic emission : AE)시험에 의해 수소취화된 압력관 재료의 새로운 파괴강도 평가법으로서 SP시험의 적용 가능성을 조사하는데 있다. 시험결과, 300ppm-H까지의 수소농도에서, 수소농도에 따른 Esp의 저하가 상온보다 $-196^{\circ}C$의 경우가 뚜렷하여, 수소취화정도에 따른 Zr-2.5%Nb 압력관 재료의 파괴강도 평가는 상온보다 $-196^{\circ}C$의 저온환경하에서의 평가가 더욱 우수함을 알 수 있었다. 또한 수소농도의 증가에 따라 재료의 파괴과정에서 발생하는 AE신호의 평균에너지의 peak와 누적 평균에너지 그리고 단위 등가파괴변형률(equivalent fracture strain : ${\epsilon}_{qf}$)당 누적 평균에너지의 값이 크게 증가하였다. 그리고 하중-변위거동, Esp 거동, 거시적, 미시적 SEM 관찰 그리고 AE 시험 결과들로부터 미소시험편을 이용한 SP시험법은 수소취화된 CANDU 압력관 재료의 새로운 파괴강도 평가법으로 유용성이 있음을 알 수 있었다.

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운동 강도가 수면장애 모델 쥐의 혈 중 멜라토닌 농도에 미치는 영향 (Effect of Different Exercise Intensity on Blood Melatonin Density in Sleep Disordered Rats)

  • 김희정;김동현
    • 대한물리의학회지
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    • 제9권1호
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    • pp.45-53
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    • 2014
  • PURPOSE: In this study, we tried to find out what kind of exercise was more effective in sleep disorder by comparing melatonin in blood after applying low intensity with high intensity exercise to sleep disordered rats induced by experiment. METHODS: We used male Sprague-Dawley rats which were 8weeks old and weighted 300g. They were supplied with water and food without any restriction. We kept the room temperature at $25^{\circ}C$ and controld the length of day and night in 12 hours blocks, respectively. We divided the rats 60 into 2 groups. To one group we applied low intensity exercise, and to the other we applied high intensity exercise for 15minutes per day over a period of 4 weeks. We extracted the blood from abdominal aorta before, after exercise, moved into EDTA tube, performed centrifugation. We decanted the serum $200{\mu}l$ from the blood into microcentrifuge tube by samples and moved into polypropylene culture tubes with micro pipette. We split enzyme solution $50{\mu}l$ into the tubes with melatonin direct kits and make them react at $37^{\circ}C$ for 2 hours. We split assay buffer $50{\mu}l$ into each tube and mixed melatonin tracer $50{\mu}l$ and melatonin antiserum $50{\mu}l$, respectively. After we made them react in room temperature, we decanted the superficial layer with a centrifuge and measured the activity for 1 minute by competitive method with ${\gamma}$-counter equipment. We draw a standard curve through logit-log graph with CPM(counts per minute) and counted the melatonin by B/B0. We conducted independent t-test to examine the homogeneous of melatonin value of before low-intensity and high-intensity exercise. We performed paired t-test to compare before and after low-intensity and high-intensity exercise, respectively. We carried out independent t-test to compare melatonin value after low-intensity and high-intensity exercise. Significance level was .05. RESULTS: The results were as follows; firstly melatonin was more increased in the group who was exposed to high intensity exercise when we compared before to after high and low intensity exercise, respectively. Secondly, high intensity exercise was more effective than low intensity exercise when we compared the two. CONCLUSION: In conclusion, secretion of melatonin which is the material of sleep improvement could be promoted by high intensity exercise. Low intensity exercise acted as a stress rather than improving sleep and had a negative effect on the secretion of melatonin because the melatonin was affected by stress.

등속공급 튜브연소로를 이용한 각 연소조건에서의 연기입자 형상 분석 (Studies on the Morphology of Smoke Particles for Each Type of Fire by Using Steady State Tube Furnace)

  • 구재학
    • 한국화재소방학회논문지
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    • 제28권1호
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    • pp.44-51
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    • 2014
  • 화재현장에서 발생하는 연기는 일반적으로 연소가스와 더불어 여러 가지 성분의 유기증기 및 미연탄소로부터 생성된 미세입자로 되어 있다. 연기는 호흡기로 흡입되어 장단기 인체피해를 유발한다. 화재 시 발생하는 유독가스나 입자에 의한 피해를 예측하기 위해서는 연기입자의 호흡기관 내 이송과 침전, 그리고 입자를 매개로 한 유독가스의 흡수와 흡착등의 현상 파악이 필수적이며 이에 연기입자의 크기 및 형상은 이와 같은 현상의 변화에 중요한 변수로서 작용한다. 이 연구에서는 화재 시 발생하는 연기입자의 흡입에 의한 인체피해 특성을 예측하기 위하여 가연물 및 화재 조건에 따른 연기입자의 크기 및 형상에 대한 분석을 수행하였다. 국제표준에 따른 연소생성물 분석을 위하여 ISO/TS 19700 기준에 따라서 등속연소로를 제작하고 각 가연물에 대하여 연소로 온도 및 당량비 조건으로 정해지는 4가지 대표적인 화재조건, 즉, 저온불완전연소, 완전불꽃연소, 불완전불꽃연소, 고온불완전연소 조건에서 연기입자를 발생시켰다. 발생된 연기입자는 다단 충돌집진기를 이용하여 채집한 다음 투과전자현미경으로 크기 및 형상을 분석하였다.

응축기의 설계조건에서 R22와 R134a의 압력강하 예측 및 실험 (Prediction and Experiment of Pressure Drop of R22 and R134a on Design Conditions of Condenser)

  • 강신형;변주석;김창덕
    • 에너지공학
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    • 제15권4호
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    • pp.243-249
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    • 2006
  • 본 실험적 연구는 슬릿휜-관열교환기의 냉매측 압력강하에 대하여 수행하였다. 응축기의 설계조건에서 미세휜관내 냉매 R22와 R134a의 압력강하에 대한 실험데이터와 앞서 제안한 상관관계식과 상호 비교하였다. 실험은 냉매 R22와 Rl34a의 응축기 입구온도 $60^{\circ}C$, 질량유속 $150{\sim}250\;kg/m^{2}s$ 범위에서 수행하였다. 공기의 유입조건은 건구온도 $35^{\circ}C$, 상대습도 40%이며, 공기유속의 범위는 $0.68{\sim}1.43\;m/s$이다. 실험결과 응축기의 과냉도 $5^{\circ}C$ 조건에서 R134a의 압력강하는 R22보다 $22{\sim}22.6%$ 높게 나타났으며, 냉매의 질량유속 $200{\sim}250\;kg/m^{2}s$의 범위에서 실험으로부터 측정한 R22와 Rl34a의 압력강하는 예측결과와 ${\pm}20%$내에 일치하였다.

설비공학 분야의 최근 연구 동향 : 2012년 학회지 논문에 대한 종합적 고찰 (Recent Progress in Air-Conditioning and Refrigeration Research : A Review of Papers Published in the Korean Journal of Air-Conditioning and Refrigeration Engineering in 2012)

  • 한화택;이대영;김사량;김현정;최종민;박준석;김수민
    • 설비공학논문집
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    • 제25권6호
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    • pp.346-361
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    • 2013
  • This article reviews the papers published in the Korean Journal of Air-Conditioning and Refrigeration Engineering during 2012. It is intended to understand the status of current research in the areas of heating, cooling, ventilation, sanitation, and indoor environments of buildings and plant facilities. The conclusions are as follows : (1) The research works on thermal and fluid engineering have been reviewed as groups of fluid machinery, pipes and valves, fuel cells and power plants, ground-coupled heat pumps, and general heat and mass transfer systems. Research issues are mainly focused on new and renewable energy systems, such as fuel cells, ocean thermal energy conversion power plants, and ground-coupled heat pump systems. (2) Research works on the heat transfer area have been reviewed in the categories of heat transfer characteristics, pool boiling and condensing heat transfer, and industrial heat exchangers. Researches on heat transfer characteristics included the results for natural convection in a square enclosure with two hot circular cylinders, non-uniform grooved tube considering tube expansion, single-tube annular baffle system, broadcasting LED light with ion wind generator, mechanical property and microstructure of SA213 P92 boiler pipe steel, and flat plate using multiple tripping wires. In the area of pool boiling and condensing heat transfer, researches on the design of a micro-channel heat exchanger for a heat pump, numerical simulation of a heat pump evaporator considering the pressure drop in the distributor and capillary tubes, critical heat flux on a thermoexcel-E enhanced surface, and the performance of a fin-and-tube condenser with non-uniform air distribution and different tube types were actively carried out. In the area of industrial heat exchangers, researches on a plate heat exchanger type dehumidifier, fin-tube heat exchanger, an electric circuit transient analogy model in a vertical closed loop ground heat exchanger, heat transfer characteristics of a double skin window for plant factory, a regenerative heat exchanger depending on its porous structure, and various types of plate heat exchangers were performed. (3) In the field of refrigeration, various studies were executed to improve refrigeration system performance, and to evaluate the applicability of alternative refrigerants and new components. Various topics were presented in the area of refrigeration cycle. Research issues mainly focused on the enhancement of the system performance. In the alternative refrigerant area, studies on CO2, R32/R152a mixture, and R1234yf were performed. Studies on the design and performance analysis of various compressors and evaporator were executed. (4) In building mechanical system research fields, twenty-nine studies were conducted to achieve effective design of mechanical systems, and also to maximize the energy efficiency of buildings. The topics of the studies included heating and cooling, HVAC system, ventilation, renewable energy systems, and lighting systems in buildings. New designs and performance tests using numerical methods and experiments provide useful information and key data, which can improve the energy efficiency of buildings. (5) In the fields of the architectural environment, studies for various purposes, such as indoor environment, building energy, and renewable energy were performed. In particular, building energy-related researches and renewable energy systems have been mainly studied, reflecting interests in global climate change, and efforts to reduce building energy consumption by government and architectural specialists. In addition, many researches have been conducted regarding indoor environments.