• 제목/요약/키워드: Micro strength

검색결과 1,201건 처리시간 0.028초

Fabrication and Characterization of Electrospun PLGA/Gelatin Nanofiber Tube for Potential Intestinal Stent Application

  • Son, So-Ra;Franco, Rose-Ann;Bao, Trinh-Quang;Bae, Sang-Ho;Min, Young-Ki;Lee, Byong-Taek
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2011년도 춘계학술발표대회
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    • pp.51.1-51.1
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    • 2011
  • An electrospun Poly (lactice-co-glycolide acid) (PLGA) and Gelatin nanofiber tube was fabricated for potential intestinal stent application. Mechanical properties of tube were evaluated by tensile strength and burst strength tests. Physical and chemical properties were evaluated by contact angle measurement, swelling rates and porosity measurements. Biodegradability was investigated by immersion in simulated body fluid (SBF). Biocompatibility was investigated in vitro by cytotoxicity and proliferation studies by MTT assay, confocal microscopy and western blot using IEC-18 (Rat intestinal epithelial cell). After intestinal stent was implanted into rat bowel for periods from 7 to 10days, it was then analyzed using micro-computed tomography (Micro CT) and X-ray techniques. Futhermore, histological analysis was performed by hematoxylin-eosin (H&E) stain.

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계면확산에 의한 Poly(hydroxy ether) 코팅된 탄소섬유의 계면접착력 변화 연구 (Effect of Diffusion on the Interfacial Adhesion of Poly(hydroxy ether) Coated Caron Fibers)

  • 강현민;윤태호
    • Composites Research
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    • 제12권6호
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    • pp.15-21
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    • 1999
  • 비닐에스테르 수지와 탄소섬유의 계면접착력 향상을 위하여 탄소섬유에 물에 분산된 carboxy modified poly(hydroxy ether) (C-PHE)와 수용성 고분자인 poly(hydroxy ether ethanol amine) (PHEA) 및 비수용성인 poly(hydroxy ether) (PHE) 로 코팅하였다. 고분자로 코팅된 탄소섬유와 수지의 계면전단강도는 micro-droplet 시편을 제조하여 측정하였으며,각 시료마다 30개 이상의 시편을 사용하였다. 접착기구 규명을 위하여 코팅재로 사용된 고분자와 비닐에스테르 수지와 계면에서 확산현상을 고찰하였으며, 접착성 시험 후 탄소섬유의 표면을 SEM을 이용하여 분석하였다. PHE와 C-PHE코팅으로 탄소섬유의 계면전단강도가 크게 증가하였으며, 이는 이들 고분자의 비닐에스테르에 대한 우수한 용해도(solubility)때문으로 보여진다. 하지만 용해도가 낮은 PHEA코팅은 접착력 향상에 효과가 없었다.

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인장시험을 통한 Sn-xAg-0.5Cu 무연 솔더의 기계적 물성평가 (Estimation of Mechanical Properties of Sn-xAg-0.5Cu Lead-free Solder by Tensile Test)

  • 정종설;신기훈;김종형
    • Journal of Welding and Joining
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    • 제29권1호
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    • pp.41-45
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    • 2011
  • SnAgCu lead-free solder alloy is considered as the best alternative to eutectic tin-lead solder. However, the detailed material properties of SnAgCu solder are not available in public. Hence, this paper presents an estimation of mechanical properties of SnAgCu lead-free solder. In particular, the weight percent of Ag was varied as 1.0wt%, 2.5wt%, 3.0wt%, and 4.5wt% in order to estimate the effect of Ag in the Sn-xAg-0.5Cu ternary alloy system. For this purpose, four types of SnAgCu bars were first molded by casting and then standard specimens were cut out of molded bars. Micro-Vickers hardness, tensile tests were finally performed to estimate the variations in mechanical properties according to the weight percent of Ag. Test results reveal that the higher the weight percent of Ag is, the higher the hardness, yield strength, and ultimate tensile strength become. More material properties will be further investigated in the future work.

MFC 센서를 이용한 응력 확대 계수 측정에 관한 연구 (A Study of Stress Intensity Factors using Micro Fiber Composite Sensors)

  • 오동진;김명현
    • Journal of Welding and Joining
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    • 제29권3호
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    • pp.76-81
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    • 2011
  • Recently, the structural failures due to fatigue occur frequently with the increase of size of ships and offshore structures. In this respect, the assessment of fatigue life and the residual strength are very important. Currently, the smart materials technology has demonstrated a variety of possibilities for a diagnosis of structural strength and structural health condition for large structures. The benefits and feature of the MFC sensor are more flexible, durable and reliable than conventional smart material. In this study, Micro Fiber Composite (MFC) sensor for the measurement of stress intensity factor (SIF) of two dimensional cracks induced in a structure is developed. Two MFC sensors are placed in the vicinity of the crack tip close to each other with the crack tip in between them. The SIFs of Mode I($K_I$) as well as of Mode II($K_{II}$) based on the piezoelectric constitutive law and fracture mechanics are calculated. In this study, the SIF values measured by MFC sensors are compared with the theoretical results and measured value.

고강도 구상흑연주철의 피로한도에 미치는 2상 기지조직의 영향 (Effects of 2-Phase Matrix Structure on Fatigue Limit of High Strength Ductile Iron)

  • 김진학;지정근;김민건
    • 산업기술연구
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    • 제19권
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    • pp.75-79
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    • 1999
  • Rotary bending fatigue tests were performed to investigate the effects of 2-phase matrix structure on fatigue limit with prepared specimens in high strength ductile irons. Two types of the specimens with different microstructures have been used. Series A has sorbite and series B has bainite. Fatigue limits of both specimens are improved comparing with as cast specimen. The fatigue limit is higher in series B than in series A. The reason why the fatigue limit of series A shows inferiority to that of series B is due to the transition of micro fatigue cracks to mesocrack occurs very rapidly, so increased stress intensity factor drives the fatigue crack growth. The higher fatigue limit of series B which has bainite is caused by the ${\gamma}$ layer contained in microstructure impede the rapid growth of micro fatigue crack to mesocrack and ${\alpha}$ layer around graphite has the higher capacity for the absorption of plastic deformation energy than sorbite.

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점熔接材 의 破壞擧動 과 應力分布 (A Study on Behavior of Fracture and Stress Distribution in Spot Welds)

  • 송삼홍;김부동
    • 대한기계학회논문집
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    • 제8권3호
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    • pp.224-231
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    • 1984
  • 본 연구에서는 이상과 같은 점을 고려하고, 인장시험을 통해 최대용접강도를 나타내는 최적용접조건을 구한 다음, 최적조건하에서 박강판을 1점 점용접한 재료의 너깃주위에 관찰되는 파괴거동을 광탄성 응력분포거동과 관련시켜 고찰하였다.

다공성 칼슘포스파이트에 대한 파괴분석 (Numerical analysis of fracture mechanisms for porous calcium phosphate)

  • 박진홍;배지용;심재범;전인수
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2008년도 추계학술대회A
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    • pp.1301-1302
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    • 2008
  • In this study, the fracture strength for fracture mechanism porous calcium phosphate made from sintered with ${\beta}$-tricalcium phosphate obtained by wet precipitation procedure is analyzed using finite element method and experiment measurement. First, three $3{\times}3{\times}3mm^3$ and $5{\times}5{\times}5mm^3$ specimens are prepared and tomographic images of one $5{\times}5{\times}5mm^3$ specimen are obtained by micro focus X-ray CT. The compression tests using the specimens are carried out to measure the elastic modulus and fracture strength to analyze the fracture mechanism of porous calcium phosphate specimen. The tomographic images are reconstructed by 3D reconstruction program. The finite elements are directly built up in the reconstructed specimen. The numerical simulation for the compression tests is performed using the element. The mechanism of calcium phosphate of simulation are obtained by the compression tests using there cylindric specimen of height 19.5 mm and diameter 10 mm. From the results, the applicability of porous calcium phosphate is evaluated to care fracture and vacant bone of a patient as the reinforcement material.

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ESPI 기법을 이용한 미소 인장 특성 추정 (Measurement of Micro-Tensile Properties using ESPI technique)

  • 허용학;김동일;윤경진;김경석;오충석
    • 한국정밀공학회지
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    • 제18권5호
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    • pp.90-97
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    • 2001
  • An electronic speckle pattern interferometry (ESPI) system for measuring tensile properties under micro-tensile testing has been developed. The system consists of an optical system and an image processing system. In the optical system, optical components for measurement of in-plane deformation are arranged on the path of He-Ne laser. In the image processing system, the window-based program for acquiring speckle pattern interferometric image was developed and deformation in a small specimen is continuously evaluated during the test. Using this system, tensile strain of copper foil was measured during tensile testing. Tensile specimen had the thickness and width of 22 and 500 ${\mu}{\textrm}{m}$, respectively. Tensile properties, including the elastic modulus, yielding strength and tensile strength, of the copper were evaluated and also plastic exponent and coefficient in the Ramberg-Osgood relationship were evaluated from the stress-strain curve.

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브레이징을 이용한 Ti/STS321L 접합체의 미세조직과 기계적 특성의 변화 (Variations of Micro-Structures and Mechanical Properties of Ti/STS321L Joint Using Brazing Method)

  • 구자명;정우주;한범석;권상철;정승부
    • Journal of Welding and Joining
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    • 제20권6호
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    • pp.106-106
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    • 2002
  • This study investigated variations of micro-structures and mechanical properties of Ti / STS321L joint with various bonding temperature and time using brazing method. According to increasing bonding temperature and time, it was observed that the thickness of their reaction layer increased due So increasing diffusion rate and time. From the EPMA results, Ti diffused to the STS321L substrate according to increasing bending time to 30min. Hardness of bonded interface increased with increasing bonding temperature and time due to increasing their oxides and intermetallic compounds. XRD data indicated that Ag, Ag-Ti intermetallic compounds, TiAg and Ti₃Ag and titanium oxide, TiO₂were formed in interface. In tensile test, it was found that the tensile strength had a maximum value at the bonding temperature of 900℃ and time of 5min, and tensile strength decreased over bonding time of 5min. The critical thickness of intermetallic compounds was observed to about 30㎛, because of brittleness from their excessive intermetallic compounds and titanium oxide, and weakness from void.

PROPERTIES OF LOW-PH CEMENT GROUT AS A SEALING MATERIAL FOR THE GEOLOGICAL DISPOSAL OF RADIOACTIVE WASTE

  • Kim, Jin-Seop;Kwon, S.;Choi, Jong-Won;Cho, Gye-Chun
    • Nuclear Engineering and Technology
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    • 제43권5호
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    • pp.459-468
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    • 2011
  • The current solution to the problem of using cementitious material for sealing purposes in a final radioactive waste repository is to develop a low-pH cement grout. In this study, the material properties of a low-pH cement grout based on a recipe used at ONKALO are investigated by considering such factors as pH variation, compressive strength, dynamic modulus, and hydraulic conductivity by using silica fume and micro-cement. From the pH measurements of the hardened cement grout, the required pH (< pH 11) is obtained after 130 days of curing. Although the engineering properties of the low-pH cement grout used in this study are inferior to those of conventional high-pH cement grout, the utilization of silica fume and micro-cement effectively meets the long-term environmental and durability requirements for cement grout in a radioactive waste repository.