• Journal of the Korean Crystal Growth and Crystal Technology
• /
• v.25 no.3
• /
• pp.93-97
• /
• 2015

To synthesis of high purity micro silver particle, we extracted the silver from the waste by liquid-liquid extraction and used the rapid firing-liquid phase precursor (RF-LPP) method. The silver micro particle was synthesized at $500^{\circ}C$ for 3 hr in air atmosphere by RF-LPP method. As a result of the research, micro silver particle is measured X-ray diffraction (XRD), the main peak is nearly corresponded to the same as JCPDS card (No.87-0719). With using the RF-LPP method, the fine Ag micro particle indicated due to the control of nucleation site and the oxygen contents was decreased by reducing treatment. We expect this research contribute to advance in field of the recycling technology.

• Transactions of the Korean Society of Mechanical Engineers B
• /
• v.24 no.6
• /
• pp.753-759
• /
• 2000

Photoelectric charging is a very efficient way of charging small particles. This method can be applied to combustion measurement, electrostatic precipitator, metal separation and control of micro-contamination. To understand the photoelectric charging mechanism, particle charging of silver by exposure to ultraviolet is investigated in this study. Average charges and charge distributions are measured at various conditions, using two differential mobility analyzers, a condensation nucleus counter, and an aerosol electrometer. The silver particles are generated in a spark discharge aerosol generator. After that process, the generated particles are charged in the photoelectric charger using low-pressure mercury lamp that emits ultraviolet having wavelength 253.7 nm. The results show that ultra-fine particles are highly charged by the photoelectric charging. The average charges linearly increase with increasing particle size and the charge distribution change with particle size. These results are discussed by comparison with previous experiments and proposed equations. It is assumed that the coefficient of electron emission probability is affected by initial charge. The results also show that the charge distribution of a particle is dependent on initial charge. Single changed particle, uncharged particle and neutralized particle are compared. The differences of charge distribution in each case increase with increasing particle size.

• 한국정보디스플레이학회:학술대회논문집
• /
• 2009.10a
• /
• pp.1118-1121
• /
• 2009

We have fabricated inverted staggered pentacene Thin Film Transistor (TFT) with 1-${\mu}m$ channel length by micro contact printing (${\mu}$-CP) method. Patterning of micro-scale source/drain electrodes without etching was successfully achieved using silver nano particle ink, Polydimethylsiloxane (PDMS) stamp and FC-150 flip chip aligner-bonder. Sheet resistance of the printed Ag nano particle films were effectively reduced by two step annealing at $180^{\circ}C$.

• Proceedings of the Materials Research Society of Korea Conference
• /
• 2011.05a
• /
• pp.238.1-238.1
• /
• 2011

본 연구에서는 non-contact deposition method의 일환인 ESD (electroctatic deposition)의 박막공정을 이용하여 Conductive layer 위에 Gold nanoparticles 및 Silver nanoparticles 등 organic/inorganic nano particle conductive ink system의 단분산 2D 박막을 제조를 연구하였다. ESD head를 통해 여러가지 organic / inorganic nano particle conductive ink system을 Deposition하였으며 분산도가 높고 균일한 단분산의 2차원 박막 구조를 얻을 수 있었으며, 전도성 PEDOT과의 Hybridization을 통해 균일상의 표면 Morphology를 갖는 고 전도성 투명 필름을 제작하였다. ESD technique를 이용하는 박막공정 기술은 나노입자 및 나노구조물의 박막화 패턴화를 포함하는 새로운 Deposition 기술로써 이를 응용하여 금속 나노입자의 2차원의 패턴화된 박막 구현을 통해 유기반도체 및 전자소자에의 응용성을 증거할 수 있었다.

• 한국정보디스플레이학회:학술대회논문집
• /
• 2005.07b
• /
• pp.913-918
• /
• 2005

It is expected that the inkjet technology offers prospect for reliable and low cost manufacturing of FPD (Flat Panel Display). This inkjet technology also offers a more simplified manufacturing process for various part of the FPD than conventional process. For example, recently the novel manufacturing processes of color filter (C/F) in LCD, or RGB patterning in OLED by inkjet printing method have been developed. This elaborates will be considered as the precious point of manufacturing process for the mass production of enlarged-display panel with a low price. On this point of view, we would like to review the status of inkjet technology in FPD, with some results on forming micro line by inkjet patterning of suspension type silver nano ink as below. We have studied the inkjet patterning of synthesized aqueous silver nano-sol on interface-controlled ITO glass substrate. Furthermore, we designed the conductive ink for direct inkjet patterning on bare ITO glass substrate. The first, the highly concentrated polymeric dispersant-assisted silver nano sol was prepared. The high concentration of batch-synthesized silver nano sol was possible to 40 wt%. At the same time the particle size of silver nanoparticles was below $10{\sim}20nm$. The second, the synthesized silver nano sol was inkjet - patterned on ITO glass substrate. The connectivity and width of fine line depended largely on the wettability of silver nano sol on ITO glass substrate, which was controlled by surfactant. The relationship was understood by wetting angle. The line of silver electrode as fine as $50{\sim}100\;{\mu}m$ was successfully formed on ITO glass substrate. The last, the direct inkjet-patternable silver nano sol on bare ITO glass substrate was designed also.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2007.06a
• /
• pp.550-550
• /
• 2007

Inkjet printed silver films were fabricated using nano particles with the size of ~ 20 nm. We can obtain very good conducting silver films with the resistivity of $7.3\;{\mu}{\Omega}{\cdot}cm$ even though they were sintered at the very low temperature of $200^{\circ}C$. The electrical and mechanical properties of inkjet printed silver lines were measured with the sintering time and analyzed with the micro-structural development. The measured resistivity of inkjet printed Ag films were $57.4\;{\sim}\;7.3\;{\mu}{\Omega}{\cdot}cm$. And their hardness and Young's modulus were 0.98 ~ 1.72 GPa and 32 ~ 71 GPa, respectively.