• 제목/요약/키워드: Micro sampling technique

검색결과 29건 처리시간 0.025초

불꽃원자 흡수 분광법의 Micro Sampling Technique 에 의한 미량 중금속의 분석에 관한 연구 (A Study on the Determination of Some Heavy Metals using Micro Sampling Technique in Flame Atomic Absorption Spectrophotometry)

  • 이원
    • 대한화학회지
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    • 제29권3호
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    • pp.220-225
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    • 1985
  • 불꽃 원자 흡수 분광법의 Micro Sampling Technique을 이용하여 염의 농도가 높고, 양이 제한된 시료중에 미량으로 함유된 Cu, Zn 및 Fe의 분석을 시도하였다. 최적기간 및 분석조건을 조사한 결과 측정시간 0.3초, 시료부피 100${\mu}l$, 시료의 흡입속도 7.5ml/min, 연료와 산화기체의 혼합비 2.0 및 버어너 높이는 Cu일때 6.0mm, Zn 및 Fe는 8.0mm이었다. 이 방법을 일반적인 불꽃 방법과 비교하여 보면 시료의 전처리 과정이 필요없이 간단하고, 비교적 정밀성과 정확성이 있으며, 특히 100${\mu}l$정도로 양이 제한된 시료와 약 20% 정도로 염의 농도가 높은 시료의 경우도 버어너 틈새가 막히지 않고 안정한 불꽃에서 분석이 가능하였다.

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단일입자재현법(單一粒子再現法)을 활용한 고고유물의 진위판별 연구 (Authentication Test of Archaeological Materials using Single Grain Regenerative Dose Method)

  • 김명진;윤민영;홍덕균
    • 보존과학회지
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    • 제23권
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    • pp.73-80
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    • 2008
  • 이 연구에서는 고고학 유물의 진위여부를 판단하기 위하여 미세시료채취법을 적용하여 시료를 채취한 후 화학적으로 분리된 세립 석영 입자의 고고선량을 산출하였다. 진위판별 연구에 앞서 미세시료채취법의 타당성은 백제무령왕릉 출토 전(塼)에서 산출된 고고선량 값들로부터 입증되었다. 이를 바탕으로 고구려 시대에 제작되었다고 주장되는 4점의 고고학 유물에 미세시료채취법을 적용하여 극소량의 시료를 채취한 후 단일입자재현법으로 고고선량을 산출하였다. 모든 유물에 대하여 고고선량 값은 0.2Gy 이하로 매우 낮았으며 단일시료재현법으로 산출된 값과 비교한 결과 매우 신뢰도가 높음을 알 수 있었다. 그러므로 유물의 고고학적 상황과 국내에서 고고선량은 평균적으로 1,000년 당 약 3.5Gy 내외의 값을 가진다는 점으로 미루어 판단하건데, 이 유물들은 고구려 시대에 제작된 유물이 아닐 가능성이 매우 높았다.

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증폭기 공유 기법을 이용한 저전력 저잡음 용량형 센서용 신호 처리 IC (Low Noise and Low Power IC Using Opamp Sharing Technique for Capacitive Micro-Sensor Sensing Platform)

  • 박윤종;김철영;정방철;유호영;고형호
    • 센서학회지
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    • 제26권1호
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    • pp.60-65
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    • 2017
  • This paper describes the low noise and low power IC using the opamp sharing technique for the capacitive micro-sensor sensing platform. The proposed IC reduces noise using correlated double sampling (CDS) and reduces power consumption using the opamp sharing technique. The IC is designed to be fully programmable, and can be digitally controlled by serial peripheral interface (SPI). The power consumption and the integrated input referred noise are 1.02 mW from a 3.3 V supply voltage and $0.164aF_{RMS}$ with a bandwidth of 400 Hz. The capacitive sensitivity, the input-output linearity and the figure of merits (FoM) are 2.5 mV/fF, 2.46 %FSO, and 8.4, respectively.

혈당검사를 위한 진공자동채혈기법사용시 채혈부위와 바늘침투깊이에 따른 통증과 채혈량 분석 (Pain and Blood Volume with Different Sampling Sites and Puncture Depths in Vacuum Assisted Auto Lancing Technique for Blood Glucose Test)

  • 박미숙;박경순;김경아;차영주;전명희;김태임;;차은종
    • 한국간호교육학회지
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    • 제12권2호
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    • pp.265-271
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    • 2006
  • Purpose: To analyze the newly developed vacuum assisted auto-lancing technique applied to the forearm for the purpose of obtaining an adequate blood sample for glucose test with minimal pain. Methods: Visual and facial pain measures were introduced to compare lancing pain between the forearm and fingertip in 58 normal females. Sampled blood volumes were accurately measured by computer scanning technique. Results: Visual pain measure demonstrated significant pain reduction effect of the forearm sampling compared with the traditional fingertip sampling, which was also consistent with facial pain measure results. Blood volume more than $0.5{\mu}L$, enough for blood glucose testing with modern glucometers, was collected in 399(86%) of 464 forearm samples. Conclusions: Capillary blood sampling could be performed with minimal pain on the forearm by the newly developed vacuum assisted auto-lancing technique. With some resampling when necessary, the forearm sampling seemed very useful, considering almost no pain felt by the patients.

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마이크로 EDM공정을 이용한 마이크로 바늘의 제조 (Manufacturing of Micro-needle Using Micro-EDM Process)

  • 리춘미;권원태
    • 한국생산제조학회지
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    • 제26권3호
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    • pp.285-291
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    • 2017
  • Micro-needles are used as transferring devices for sampling of tiny constitute substances from biological bodies. Typically, nickel is used as a coating to improve the rigidity of micro-needles. This study introduces the methodology to manufacture a WC needle with very high hardness and toughness. Micro-EDM technology was used to manufacture micro-needles with holes $130{\mu}m$ in diameter and $2300{\mu}m$ in length. A micro-needle was aligned to the micro-EDM electrode using a custom two degree-of-freedom alignment system. A three-step manufacturing technique was developed to drill a micro-hole using a WC electrode. In the first process, an electrode $105{\mu}m$ in diameter was used to make a hole. Electrodes of 90 and $105{\mu}m$ diameters were used in the second and third process, respectively. Consequently, a WC micro-needle with an inner hole of $135{\mu}m$ diameter, length of $2300{\mu}m$, and outer diameter of $300{\mu}m$ was developed.

차동 델타 샘플링 기법을 이용한 비냉각형 적외선 검출회로의 설계에 관한 연구 (A Study on the Design of a ROIC for Uncooled Infrared Ray Detector Using Differential Delta Sampling Technique)

  • 정은식;권오성;이포;정세진;성만영
    • 한국전기전자재료학회논문지
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    • 제24권5호
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    • pp.387-391
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    • 2011
  • A uncooled infrared ray sensor used in an infrared thermal imaging detector has many advantages. But because the uncooled infrared ray sensor is made by MEMS (micro-electro-mechanical system) process variation of offset is large. In this paper, to solve process variation of offset a ROIC for uncooled infrared ray sensor that has process variation of offset compensation technique using differential delta sampling and reference signal compensation circuit was proposed. As a result of simulation that uses the proposed ROIC, it was possible to acquire compensated output characteristics without process variation of offsets.

A Site Specific Characterization Technique and Its Application

  • Kamino, T.;Yaguchi, T.;Ueki, Y.;Ohnish, T.;Umemura, K.;Asayama, K.
    • 한국전자현미경학회:학술대회논문집
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    • 한국현미경학회 2001년도 제32차 추계학술대회
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    • pp.18-22
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    • 2001
  • A technique to characterize specific site of materials using a combination of a dedicated focused ion beam system(FIB), and Intermediate-voltage scanning transmission electron microscope(STEM) or transmission electron microscope(TEM) equipped with a scanning electron microscope(SEM) unit has been developed. The FIB system is used for preparation of electron transparent thin samples, while STEM or TEM is used for localization of a specific site to be milled in the FIB system. An FIB-STEM(TEM) compatible sample holder has been developed to facilitate thin sample preparation with high positional accuracy Positional accuracy of $0.1{\mu}m$ or better can be achieved by the technique. In addition, an FIB micro-sampling technique has been developed to extract a small sample directly from a bulk sample in a FIB system These newly developed techniques were applied for the analysis of specific failure in Si devices and also for characterization of a specific precipitate In a metal sample.

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차량용 임베디드 프로세서에서 저전력 반응적 제어를 위한 이기종 멀티코어 협력적 스트리밍 온-칩 소프트웨어 구조 (Collaborative Streamlined On-Chip Software Architecture on Heterogenous Multi-Cores for Low-Power Reactive Control in Automotive Embedded Processors)

  • 권지수;박대진
    • 대한임베디드공학회논문지
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    • 제17권6호
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    • pp.375-382
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    • 2022
  • This paper proposes a multi-core cooperative computing structure considering the heterogeneous features of automotive embedded on-chip software. The automotive embedded software has the heterogeneous execution flow properties for various hardware drives. Software developed with a homogeneous execution flow without considering these properties will incur inefficient overhead due to core latency and load. The proposed method was evaluated on an target board on which a automotive MCU (micro-controller unit) with built-in multi-cores was mounted. We demonstrate an overhead reduction when software including common embedded system tasks, such as ADC sampling, DSP operations, and communication interfaces, are implemented in a heterogeneous execution flow. When we used the proposed method, embedded software was able to take advantage of idle states that occur between heterogeneous tasks to make efficient use of the resources on the board. As a result of the experiments, the power consumption of the board decreased by 42.11% compared to the baseline. Furthermore, the time required to process the same amount of sampling data was reduced by 27.09%. Experimental results validate the efficiency of the proposed multi-core cooperative heterogeneous embedded software execution technique.

Real-Time All-Optical Three-Dimensional Image Projector

  • Jang, Ju-Seog;Javidi, Bahram
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2002년도 International Meeting on Information Display
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    • pp.285-288
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    • 2002
  • We propose the use of synchronously moving micro-optics (lenslet arrays) for image pickup and display in three-dimensional integral imaging to overcome the upper resolution limit imposed by the Nyquist sampling theorem. With the proposed technique, we present an all-optical three-dimensional integral imaging projector. An optically addressed spatial light modulator is used, which potentially provides better image resolution than the conventional CCD and liquid crystal display pair. We present experimental results using a liquid crystal light valve.

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Perceived Usefulness of Business Coaching on the Relationship between Entrepreneurial Competencies and Business Success

  • IDRIS, Mohd Mahfudz bin;ABU BAKAR, Saridan bin
    • The Journal of Asian Finance, Economics and Business
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    • 제7권10호
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    • pp.329-338
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    • 2020
  • The present study aims to investigate the perceived usefulness of business coaching as a moderator between the association of entrepreneurial competencies and business success of women micro-entrepreneurs. This study employs a stratified random sampling technique to collect data from women micro-entrepreneurs who attended business coaching sessions. In total, 261 questionnaires were distributed and collected. This study has divided the moderator (i.e., perceived usefulness of business coaching) into two groups, namely, group 1 (with a low mean) and group 2 (with a high mean) for moderation analysis. By using a comparative analysis of the path coefficient for groups 1 and 2, the path is moderated by the perceived usefulness of business coaching if the beta value for group 1 is significant, and the beta value for group 2 is non-significant. The results show that eight out of a total of sixteen hypotheses were supported, while the remaining hypotheses were rejected. The findings of the study suggest that the domains of entrepreneurial competencies for women micro-entrepreneurs, including strategic, commitment, conceptual, opportunity, and relationship competencies, together with the perceived usefulness of business coaching, are vital for the business success and should remain the principal focus of future research in women entrepreneurship.