• Title/Summary/Keyword: Mg Powders

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Thermal Sprayed AlSiMg/TiC Composite Coatings : Fabrication of Powder and Characteristics of Coatings (I) (AlSiMg/TiC 복합 용사 피막 : 분말제조 및 피막 특성(I))

  • 양병모;변응선;박경채
    • Journal of Welding and Joining
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    • v.18 no.5
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    • pp.98-104
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    • 2000
  • Aluminum alloys are being employed in automobile parts as strive to reduce overall vehicle weight to meet demands for improved fuel economy and reduction in vehicle emissions. Al-based composites reinforced with ceramic ($Al_2O_3,\;SiC,\;TiC\;and\;B_4C$) applications in a variety of components in automotive engines, such as liners, where the tribological properties of the material are important. In this study, Al-base composites reinforced with TiC particle powders has been developed for producing plasma spray coatings. The composite plasma spray powders were prepared Al-13Si-3Mg(wt%) alloy with TiC(40, 60 and 80wt%) particles ($0.2~5{\mu}textrm{m}$) by drum type ball milling. The composite powders ($36~76{\mu}textrm{m}$) were sprayed with plasma torch. Plasma sprayed coatings were heat-treated at $500^{\circ}C$ for 3 hours. The wear resistances of the plasma sprayed coatings were found to decrease with increasing TiC content and improved with heat treatment. AlSiMg-40% TiC heat-treated coatings were showed the best wear resistance in this study.

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The Photoluminescence and Decay time of the Green Phosphor $Zn_2$$SiO_4$:Mn, Mg (Mg와 Mn이 도핑된 $Zn_2$$SiO_4$ : Mn, Mg 녹색 형광체의 빛 발광과 잔광시간 특성)

  • 조봉현;황택성;손기선;박희동;장현주
    • Journal of the Korean Ceramic Society
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    • v.35 no.10
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    • pp.1101-1106
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    • 1998
  • Various $Zn_{2-x}SiO_4$:xMn based green phosphors were investigated in association with a co-dopant. The co-dopant incorporated into the phosphors are believed to alter the internal energy state of $Zn_{2-x}SiO_4$ : xMn So that the improvement in their intensity could be expected. Phosphor samples were prepared using the solid state reaction therein raw powders are mixed in the acetone and successively fired at $1300^{\circ}C$ for 4 hour. The fired powders are also heated up to $900^{\circ}C$ for 2 hour in the reduced atmoshpere and thereby giving The fired powders are also heated up to $900^{\circ}C$ for 2 hour in the reduced atmosphere and thereby giving rise to conspicuous enhancement of radiative efficiency. Basically the 0.08 mole ratio of the Mn con-centrations has the maximum value of the intensity so that a co-dopant are added to this Mn con-centration. When the Mg is co-doped with Mn luminescent intensity is proven to be promoted significantly.

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Synthesis of $MgB_2$ powders by ultrasonic spray pyrolysis (초음파 분무열분해를 이용한 $MgB_2$ 분말 합성)

  • Park, S.C.;Lim, Y.J.;Kang, S.G.;Chung, J.K.;Kim, C.J.;Kim, C.J.
    • Progress in Superconductivity and Cryogenics
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    • v.10 no.1
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    • pp.19-23
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    • 2008
  • Spherical $MgB_2$ powders was synthesized with the ultrasonic spray pyrolysis(USP) process using aqueous solutions of boron and magnesium ion. The properties of synthesized $MgB_2$ powder were characterized by XRD, SEM and EDS. A small amount of MgO was detected as the secondary phase out of the synthesized powder and the ratios of $MgB_2$ to MgO increased with increasing furnace temperature. The particle size and morphology of $MgB_2$ powder were investigated with varying molar concentration of the boron and magnesium solution and furnace temperature between $600^{\circ}C$ and $1000^{\circ}C$ in $Ar/H_2$. The average particle size of $MgB_2$ showed narrow distribution ranging from 300nm to 400nm. The morphology of particles exhibited mostly spherical shapes and uniform distribution.

Synthesis and characterization of soft magnetic composite in Fe2O3-Mg system by mechanical alloying (기계적합금화에 의한 Fe2O3-Mg계 연자성 콤포지트의 합성 및 평가)

  • Lee, Chung-Hyo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.25 no.6
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    • pp.245-251
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    • 2015
  • We have applied mechanical alloying (MA) to produce soft magnetic composite material using a mixture of elemental $Fe_2O_3$-Mg powders. An optimal milling and heat treatment conditions to obtain soft magnetic ${\alpha}$-Fe/MgO composite with fine microstructure were investigated by X-ray diffraction, differential scanning calorimetry (DSC) and vibrating sample magnetometer (VSM) measurement. It is found that ${\alpha}$-Fe/MgO composite powders in which MgO is dispersed in ${\alpha}$-Fe matrix are obtained by MA of $Fe_2O_3$ with Mg for 30 min. The saturation magnetization of ball-milled powders increases with increasing milling time and reaches to a maximum value of 69.5 emu/g after 5 h MA. The magnetic hardening due to the reduction of the ${\alpha}$-Fe grain size by MA was also observed. Densification of the MA powders was performed in a spark plasma sintering (SPS) machine at $800{\sim}1000^{\circ}C$ under 60 MPa. X-ray diffraction result shows that the average grain size of ${\alpha}$-Fe in ${\alpha}$-Fe/MgO nanocomposite sintered at $800^{\circ}C$ is in the range of 110 nm.

Effects of Nano FexC Addition on Superconducting Properties of MgB2 (MgB2 초전도 특성에 대한 나노 FexC 첨가 효과)

  • Lee, Dong-Gun;Lee, Ji-Hyun;Jun, Byung-Hyuk;Park, Soon-Dong;Uhm, Young-Rang;Park, Hai-Woong;Kim, Chan-Joong
    • Journal of Powder Materials
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    • v.19 no.2
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    • pp.146-150
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    • 2012
  • The effects of nano $Fe_xC$ addition to superconducting properties of $in$ $situ$ processed $MgB_2$ superconductors was examined. 0.1 wt.% and 1 wt.% nano $Fe_xC$ powders were mixed with boron and magnesium powders by ball milling. The powder mixtures were made into pellets by uniaxial pressing. The pellets were heat-treated at $700^{\circ}C-900^{\circ}C$ in argon atmosphere for $MgB_2$ formation. It was found by powder X-ray diffraction that the raw powders were completely converted into $MgB_2$ after the heat treatment. The superconducting transition temperature ($T_c$) and critical current density ($J_c$), estimated from susceptibility-temperature and $M-H$ curves, were decreased by nano $Fe_xC$ addition. The $T_c$ and $J_c$ decrease by nano $Fe_xC$ addition are attributed to the incorporation of iron and carbon with $MgB_2$ lattices (Fe substitution for Mg and C substitution for B) due to the high reactivity of the nano $Fe_xC$ powder.

Studies for Component Analysis and Antioxidative Evaluation in Acorn Powders (도토리 가루의 성분분석과 항산화능 평가)

  • Shim, Tae-Heum;Jin, Ying-Shan;Sa, Jae-Hoon;Shin, In-Cheol;Heo, Seong-Il;Wang, Myeong-Hyeon
    • Korean Journal of Food Science and Technology
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    • v.36 no.5
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    • pp.800-803
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    • 2004
  • Chemical components and physiological activities of acorn powders were investigated to develop functional food. Proximate components were 87.29% crude fiber, 1.18% crude fat, 0.84% crude protein, and 0.12% crude ash. Potassium was most predominant mineral, followed by phosphorus, calcium, magnesium, and sodium. Contents of unsaturated fatty acids, such as oleic, linoleic, and linolenic acids, were higher than those of saturated fatty acids. Water and 75% ethanol extracts of acorn powders showed higher absorbency at 285 nm. Water and 75% ethanol extracts exhibited antioxidative activity with $IC_{50}$ of 19.0 and $21.4\;{\mu}g/mL$, respectively, indicating they are the major biological component in acorn powders. Results suggest water extract of acorn can be used as new material for natural antioxidant and functional food.

$MgB_2$ Sheets using Mixture of Mg and B Powders by Powder Roll Compaction (Mg과 B 혼합분말을 이용하여 분말압연 공정으로 제조된 $MgB_2$ 초전도 판재연구)

  • Chung, K.C.;Chang, S.H.;Sinha, B.B.;Kim, J.H.;Dou, S.X.
    • Progress in Superconductivity
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    • v.13 no.3
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    • pp.184-188
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    • 2012
  • $MgB_2$ superconducting sheets have been fabricated by powder rolling method using mixture of Mg and B powders. Sheet-type $MgB_2$ bulk samples of ~10 mm width and 50-100 mm long were squeezed out after compacted by two rotating rolls of 130 mm diameter with gap distance of 0.5 mm and speed of ~40 cm/min (~1 rpm). The nominal composition of Mg, which is ductile metal, was added up to 30% to facilitate forming the $MgB_2$ sheets. The annealed samples at $900^{\circ}C$ and 3 hrs showed superconducting transition temperature of ~32 K and critical current densities at zero fields were ${\sim}10^5A/cm^2$ at 5 K and ${\sim}5{\times}10^4A/cm^2$ at 20 K.

Influence of Magnesium Powder and Heat Treatment on the Superconducting Properties of $MgB_2/Fe$ Wires ($MgB_2/Fe$ 선재의 초전도성에 대한 열처리 조건과 Mg 분말의 영향)

  • Tan, Tan Kai;Kim, N.K.;Kim, Y.I.;Jun, B.H.;Kim, C.J.
    • Progress in Superconductivity
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    • v.9 no.1
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    • pp.1-4
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    • 2007
  • The most common technique to fabricate $MgB_2$ superconducting wire is by powder-in-tube (PIT) technique. Therefore, the starting powder for the processing of $MgB_2$ superconductors is an important factor influencing the superconducting properties and performance of the conductors. In this study, the influence of magnesium precursor powders and annealing temperatures on the transition temperatures ($T_c$) and critical current densities ($J_c$) of $MgB_2/Fe$ wires was investigated. All the $MgB_2/Fe$ wires were fabricated by in situ PIT process. It was found that higher $J_c$ was obtained for $MgB_2$ wires with smaller particle size of magnesium precursor powders. The $J_c$ also increases with decreasing annealing temperatures.

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Dielectric properties of $xPb (Fe_{1/2}Nb_{1/2}) O_3 - (1-x) Pb (Mg_{1/3}Nb_{2/3}) O_3$ ceramics prepared by the molten salt synthesis method (용융염 합성법에 의해 제조된 $xPb (Fe_{1/2}Nb_{1/2}) O_3 - (1-x) Pb (Mg_{1/3} Nb_{2/3}) O_3$ 계 세라믹스의 유전성)

  • 박경봉;김태희
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.5 no.2
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    • pp.152-164
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    • 1995
  • $xPb(Fe_{1/2}Nb_{1/2})O_3 - (1 - x)Pb(Mg_{1/3}Nb_{2/3})O_3$ powders were synthesized by the molten salt synthesis method using the NaC!- KCI flux with 1 : 1 molar ratio, and their powders and dielectric properties were investigated. The synthesized powders showed less agglomerated shape with the average particle size of less than $2 \mu\textrm{m}$. The composition $x0.3Pb(Fe_{1/2}Nb_{1/2})O_3-0.7Pb(Mg_{1/3}Nb_{2/3})O_3$ could be sintered at $1000{\times}C$ and its dielectric constnat was over 11, 000.

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Formation of Ni layer onto alumina powders by hydrogen reduction technique (가압수소환원법에 의한 알루미나 분말상의 니켈 코팅층 형성에 관한 연구)

  • 김동진;정헌생;유케닝
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.6 no.3
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    • pp.415-423
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    • 1996
  • Hydrogen reduction technique was used to form the nickel layer onto alumina powders in nickel sulfate solutions. The reduction rate and precipitation states of nickel ions were investigated at various experimental conditions such as hydrogen pressure, temperature, $PdCl_{2}$ addition, particle size, and so on. Uniformly nickel coated alumina composite powders were obtained at such condition as reduction temperature of $165^{\circ}C$, hydrogen pressure of 300 psi, and $PdCl_{2}$ amount of $2\;mg/\ell$.

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