• 제목/요약/키워드: Mg:Ag

검색결과 538건 처리시간 0.022초

PMN-PT-BT/Ag/MgO 나노복합체의 제조 및 유전 특성 (Preparation of PMN-PT-BT/Ag/MgO Nanocomposite and Dielectric Properties)

  • 정순용;임경란;남산
    • 한국세라믹학회지
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    • 제39권11호
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    • pp.1074-1082
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    • 2002
  • 소결온도가 $1200{\circ}C$인 PMN-PT-BT에 소량의 $AgNO_3$와 MgO 졸을 첨가하여 $950{\circ}C$ 소결로 PMN-PT-BT/Ag/MgO 나노복합체를 제조하였다. Modified mixed oxide 방법으로 제조된 저온 소결용 PMN-PT-BT/Ag 분말을 $600{\circ}C$/1h 하소한 다음 MgO 졸을 0-1.0wt% 첨가하여, 산소 분위기에서 $850-950{\circ}C$에서 4시간 소결하여 MgO 졸의 첨가량과 소결온도에 따른 미세구조의 발달과 유전특성을 조사하였다. MgO 졸이 0.5wt% 첨가되고, $950{\circ}C$에서 소결하여 얻은 PMN-PT-BT/Ag/MgO(0.5wt%) 소결체는 $1-3{\mu}m$의 입의 크기에 $0.1-0.3{\mu}m$의 MgO가 2차상을 입경, 삼중접, 입내에 분포되어 있음을 SEM으로 볼 수 있었으며, Ag는 SIMS로 << $1{\mu}m$로 분포되어 있음을 정성적으로 확인하였다. 상대소결밀도 99%, 실온유전율 17200, 유전손실 2.1%, 비저항 $5.46{\times}10^{12}{\Omega}{\cdot}cm$의 특성을 나타내었다. 그러나 MgO 졸이 첨가되지 않은 PMN-PT-BT/Ag/MgO(0 wt%)의 $950{\circ}C$ 소결체는 상대 소결밀도 99.5%, 상온유전율 19500, 유전손실 2.1%, 비저항 $7.30{\times}10^{12}{\Omega}{\cdot}cm$의 좀더 높은 특성을 나타내었다.

Enhancement of light reflectance and thermal stability in Ag-Mg alloy contacts on p-type GaN

  • 송양희;손준호;김범준;정관호;이종람
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2010년도 춘계학술회의 초록집
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    • pp.18-20
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    • 2010
  • 수조구조의 InGaN LED 소자에 적용이 가능하며 높은 열적안정성을 갖는 저저항 고반사율 p형 오믹 전극을 개발하였다. Ag에 Mg을 첨가하여 p형 전극을 이용하여 $400^{\circ}C$, 공기중에서 1분간 열처리 후 $2.2\;{\times}\;10^{-5}\;{\Omega}cm^2$의 낮은 접촉 저항을 얻을 수 있었고, 460 nm 파장에서 82.6%의 높은 반사율을 획득할 수 있었다. 이는 Mg가 첨가됨에 따라 Ag가 고온에서 집괴되는 원인인 산소-공공 결합을 줄여줌으로써 높은 열적 안정성을 얻게 되었다. Ag를 열처리 할 경우, 외부에 존재하는 산소가 공공 자리에 들어간 후, 산소와 공공의 강한 인력에 의해 산소가 침입형 자리에 들어가서면서 두개의 공공과 강하게 bonding을 갖는 diffusion center가 많이 존재하게 된다. 하지만 Mg가 첨가되었을 경우, Oxygen affinity가 강한 Mg에 산소가 먼저 결합을 이루면서 산소-공공결합을 줄여주게 되어 높은 온도에서도 diffusion이 이루어지지 않고 높은 열적 안정성을 갖게 된다.

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MgO(100) 기판 위에 증착된 Ag/CoFeB 박막의 스퍼터링 조건에 따른 미세성장구조 변화 연구 (Effects of Sputtering Conditions on the Growth of Ag/CoFeB Layer on MgO(100) Substrate)

  • 전보건;정종율
    • 한국자기학회지
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    • 제21권6호
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    • pp.214-218
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    • 2011
  • 본 연구에서는 DC 마그네트론 스퍼터링을 이용해 MgO 단결정 기판 위에 성장된 Ag/CoFeB 박막의 스퍼터링 조건에 따른 박막 미세구조의 변화를 연구하였다. Ag 박막의 결정성 및 표면 거칠기는 인가전력(sputtering power) 및 증착온도의 변화에 따라 증착온도가 증가하는 경우 (200) 방향의 결정성이 향상되는 것을 확인하였으며, 인가전력이 증가되는 경우 표면 거칠기가 감소하는 것을 확인하였다. 또한 고분해능 TEM(transmission electron microscopy) 및 XRR(X-ray reflectivity) 측정을 통해 MgO 기판 위 Ag층의 켜쌓기 성장 및 MgO 기판과 Ag층 사이에 산화층에 해당하는 계면층이 존재하는 것을 알 수 있었으며, 증착온도의 증가에 따른 Ag의 섬상구조 형성 및 intermixing 효과에 의한 Ag/CoFeB 계면층의 변화 및 자기적 특성의 변화를 연구하였다.

국화 '오블랑'의 재생 효율 증진을 위한 식물생장조절제와 AgNO3 적정 농도 선별 (Optimal concentrations of plant growth regulators and AgNO3 for the improvement of regeneration efficiency in Chrysanthemum morifolium 'Ohblang')

  • 윤여진;양용준
    • Journal of Plant Biotechnology
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    • 제50권
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    • pp.169-175
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    • 2023
  • 국화 '오블랑'의 기내 배양 잎 절편체로부터 신초 기관형성을 통한 식물체 재생 시스템을 확립하는데 있어 효율적인 신초 재생 및 갈변억제를 위한 식물생장조절제와 AgNO3의 농도를 선정하고자 실험을 수행하였다. 잎 절편체를 식물생장조절제인 BA 0.5, 1.0, 2.0 mg/L와 NAA 0.2, 0.5, 1.0, 2.0 mg/L를 조합 처리한 12가지 조성의 배지에 치상하여 암조건에서 6주간, 명조건에서 6주간 배양하였을 때, BA 1.0 mg/L, NAA 1.0 mg/L를 첨가한 배지를 사용하는 것이 가장 효과적이었다. 이 결과를 기반으로 잎 절편체로부터 갈변 감소를 위해 MS 염류와 비타민, BA 1.0 mg/L, NAA 1.0 mg/L, sucrose 30 g/L, agar 6 g/L를 포함한 신초유도배지에 AgNO3 0, 1, 3, 5, 7, 10 mg/L를 각각 첨가하여 실험을 실시하였다. AgNO3 처리는 잎 절편체로부터의 갈변을 감소시키는 효과를 보였으나, 처리 농도가 증가됨에 따라 신초로의 발달은 원활하게 이루어지지 않았다. 결과적으로 AgNO3 1 mg/L를 포함한 신초유도배지(MS 염류와 비타민, BA 1.0 mg/L, NAA 1.0 mg/L)에 잎 절편체를 치상하였을 때, 갈변지수 0.7, 절편체당 신초 수가 2.6개로 '오블랑' 재생에 있어 가장 적합한 농도임을 확인하였다.

카본블랙이 도핑 된 $MgB_2$ 초전도체의 Ag 첨가의 영향 (Influence of Ag Addition on Superconducting Property of Carbon-black Doped $MgB_2$ Superconductor)

  • 김효진;김현지;김찬중;박해웅
    • Progress in Superconductivity
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    • 제12권1호
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    • pp.1-5
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    • 2010
  • In this work we synthesized both MgB2 and Carbon doped MgB2 superconductor with Ag addition via high energy milling and substituent heat treatment. Heat treatments were performed at $900\;^{\circ}C$ for 30 min in flowing Ar gas. We varied amount of Ag powder. In a range of Ag powder was 0~5wt%. The effect of Ag was correlated with superconducting properties. The results show a slight decrease in critical temperature ($T_c$) and a reduction of critical current density ($J_c$) at high fields for the Ag-doped samples as compared to the un-doped samples. Reduction of $J_c$ may be due to the formation of MgAg compound.

새로운 항암제 AG 60의 일반약리작용 (General Pharmacology of AG 60, a New Anticancer Drug)

  • 성연희;안희열;김선돈;이선애;조순옥;한영복
    • Biomolecules & Therapeutics
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    • 제5권4호
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    • pp.412-418
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    • 1997
  • General pharmacological properties of AG 60 (mixture of acriflavine and guanosine (1:1, w/w)), which has anticancer effect, following intramuscular administration were examined in terms of effects on central nervous system, gastrointestinal system, cardiovascular system, respiratory system and autonomic nervous system in mice, rats, guinea-pigs and rabbits. AG 60 at the dose of 15 mgtg had no influences on pentobarbital sleeping time, spontaneous motor activity, chemoshock produced by pentylenetetrazole solution, writhing syndromes induced by 0.8% acetic acid solution, and motor coordination of mice. However, AG 60 at the dose of 7.5 and 15 mg/kg caused significant decrease of normal body temperature 1 and/or 2 h after the administration. No influence on body temperature was observed at 3.75 mg/kg in mice. Gastric secretion of rat and intestinal motility of mice were not influenced by the dose of 15 mg/kg. In terms of autonomic nervous system, AG 60 did not show direct effect and inhibitory or augmentative action of histamine- or acetylcholine-induced contractions at the concentration of 5 mg/L in the isolated ileum of guinea-pig. The administration of 15 mg/kg of AG 60 did not affect mean arterial blood pressure and heart rate in rat. AG 60 (15 mg/kg) given to anesthetized rabbits showed no effect on respiratory rate.

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The Effect of Acori Graminei Rhizoma Pharmacopuncture at GV20 on Dementia in a Focal Cerebral Ischemia Mice Model

  • Jang, Yeo jin;Kwak, Min Kyung;Jeong, Sang Jun;Kim, Hye Hwa;Kim, Tae Gwang;Kim, Jae Hong
    • Journal of Acupuncture Research
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    • 제34권3호
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    • pp.1-11
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    • 2017
  • Objectives : The purpose of this study was to examine the effects of Acori Graminie Rhizoma Pharmacopuncture (PA-AG) at GV20 on cerebral ischemia-induced dementia in Mice. Methods : Mice were divided into the five following groups: normal, control, acupuncture, PA-AG (17 mg/kg), and PA-AG (34 mg/kg). All groups, except the normal group, had cerebral ischemia induced by occlusion of middle cerebral artery. The control group was not treated. The acupuncture, PA-AG (17 mg/kg), and PA-GA (34 mg/kg) groups were treated every other day with a total of 6 treatments. The effect of treatment was observed by Bax, Bcl-2, Bax/Bcl-2 ratio, cytochrome c, cresyl violet, and choline acetyltransferase staining. Results : In the PA-AG (34 mg/kg) group, the intensity of Bax was decreased and the intensity of Bcl-2 was increased. The Bax/Bcl-2 ratio also decreased in the PA-AG (34 mg/kg) group. The intensity of cytochrome c protein stain was decreased in the PA-AG (17 mg/kg) group. The density of neurons stained by cresyl violet and choline acetyltransferase (ChAT) was increased in the AT, PA-AG (17 mg/kg), and PA-AG (34 mg/kg) groups when compared with that of the control group. Conclusion : PA-AG at GV20 was effective on cerebral ischemia-induced dementia in mice.

Ag첨가 마그네슘 합금의 이중열처리에 따른 미세조직 및 기계적 특성변화 (Effect of Double Aging on Microstructure and Mechanical Properties of Ag Added magnesium Alloys)

  • 이병덕;백의현;장경수;한정환;손현택
    • 대한금속재료학회지
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    • 제49권6호
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    • pp.440-447
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    • 2011
  • To improving the mechanical properties of Mg alloys at high temperature, we investigated the mechanical properties at high temperature and the change of microstructure of Mg-6 wt%Zn-0.4 wt%Mn and Mg-6 wt%Zn-0.4 wt%Mn-1 wt%Ag alloys on age treatment that have a stable MgZn phase at high temperature and $AgMg_4$ improving yield stress. In order to predict thermodynamic data of Mg alloys, a phase diagram and precipitation phase were calculated using a thermodynamic program, and it was confirmed that the MgZn and $AgMg_4$ phase existed as main precipitation in this alloys. The experimental data examined using DSC and XRD were comparable with the calculated data for reliability. In order to analysis the microstructure and precipitate phase during aging treatment, it was measured by SEM/EDS and TEM. Lastly, mechanical properties of the MgZn and $AgMg_4$ phase were measured by a tensile test at high temperature.

Influence of Ag nano-powder additions on the superconducting properties of Mg $B_2$ materials

  • K. J. Song;Park, S. J.;Kim, S. W.;Park, C.;J. H. Joo;Kim, H. J.;J. K. Chung;R. K. Ko;H. S. Ha
    • 한국초전도ㆍ저온공학회논문지
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    • 제5권3호
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    • pp.6-10
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    • 2003
  • Silver nano-powder was added to Ma $B_2$ to make (Ag)$_{(x)wt.%}$(Mg $B_2$)$_{(l00-x)wt.%}$ (A $g_{x}$-Mg $B_2$) (10 $\leq$ x $\leq$ 50) composite superconductors to investigate the effect of the Ag nano-powder on the vortex pinning. Pellets made out of the mixed powder were put inside stainless steel tubes, which were sintered at 85$0^{\circ}C$ in Ar atmosphere. No impurity phase was identified for as-rolled samples. However, both the Mg $B_2$ and the A $g_{x}$-Mg $B_2$ composite pellets, when sintered, contain small amount of Mg $B_4$ and MgAg impurity phases. From the magnetization study, it was found that the flux pinning was improved in the high magnetic field region (> 3 T) only when 10w/o Ag was added to Mg $B_2$. The "two step" structures in ZFC M(T) curve gradually increased as the amount of Ag added increased. Pinning centers can be created by adding a suitable amount of Ag nano-powder which is not too large to increase the decoupling between the Mg $B_2$ grains.crease the decoupling between the Mg $B_2$ grains.

Cu-Mg-P 합금의 기계적 성질과 전기전도도에 미치는 Ag첨가의 영향 (Influence of Ag Addition on the Mechanical Properties and Electrical Conductivity of Cu-Mg-P Alloys)

  • 김정민;박준식;김기태
    • 열처리공학회지
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    • 제23권1호
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    • pp.10-16
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    • 2010
  • The microstructure of Cu-Mg-P alloy sheet consisted of Cu matrix and very fine MgP precipitate, and it has been observed that the microstructure remains virtually unchanged by Ag additions up to 2%. Ag solutes were dissolved into the matrix and hardly found in the precipitates. The hardness increased with increase of the Ag content, while the conductivity slightly decreased. Strain hardening through cold rolling was found to be effective in improving the hardness, especially in high-Ag alloys. Aging treatment was conducted either before the first cold rolling or between the first and the final cold rolling, and the conductivity was significantly higher at the former case, regardless of the Ag content. Softening of Cu-Mg-P alloy sheet was remarkable above $400^{\circ}C$ and the Ag content did not show any significant effect on it.