• 융복합기술연구소 논문집
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• 제6권2호
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• pp.35-40
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• 2016

Ignitor tip is a component of burner to start the burning process in power plant. This is used to ignite the coal to a constant operating state by fuel mixed with air and kerosene. This component is composed of three components so that air and kerosene are mixed in the proper ratio and injected uniformly. Because the parts with the designed shape are manufactured in the machining process, they have to be made of three parts. These parts are designed to have various functions in each part. The mixing part mixes the supplied air and kerosene through the six holes and sends it to the injecting part at the proper ratio. The inject part injects mixed fuel, which is led to have a constant rotational direction in the connecting part, to the burner. And the connecting plate that the mixed fuel could rotate and spray is assembled so that the flame can be injected uniformly. But this part causes problems that are worn by vibration and rotation because it is mechanically assembled between the mixing part and the inject part. In this study, 3D printing method is used to integrate a connecting plate and an inject part to solve this wear problem. The 3D printing method could make this integrated part because the process is carried out layer by layer using a metal powder material. The part manufactured by 3D printing process should perform the post process such as support removal and surface treatment. However, while performing the 3D printing process, the material properties of the metal powders are changed by the laser sintering process. This change in material properties makes the post process difficult. In consideration of these variables, we have studied the optimization of manufacturing process using 3D printing method.

• 한국재료학회지
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• 제5권7호
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• pp.888-896
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• 1995

Al 금속분말을 zircon sand (ZrSiO$_4$)와 A1$_2$O$_3$혼합체에 첨가하여 반응소결시킴으로써 무수축 Mullite-ZrO$_2$, 요업체를 얻고자 하였다. 반응식, 3(Al+Al$_2$O$_3$)+2ZrSiO$_4$$\longrightarrow$3A1$_2$O$_3$ .2SiO$_2$+2ZrO$_2$에 의하여 ZrO$_2$-강화 Mullite 요업체를 제조하였다. Al 분말은 A1$_2$O$_3$에 대해 0-30 무게 퍼센트까지 대체하였다. 평량한 분말을 볼밀하여 혼합 분쇄한 후, 정수압 성형하여 시편을 제조하고, 온도범위 1450-1$600^{\circ}C$에서 3시간 반응소결시켰다. Al의 충분한 산화를 위해, 한편으로는 125$0^{\circ}C$에서 5시간동안 열처리를 거친후 소성온도로 올리기도 했다. Al을 첨가함으로서 반응은 촉진되었으며, 소성수축도 산화한 Al의 부피팽창에 의해 상쇄되어, 무수축요업체 제조의 가능성을 보였다. 박편모양을 한 비교적 큰 Al분말이 잘 분쇄되지 않음으로 해서, Al이 자리했던 곳에 큰 기공을 남겼다.

• 한국산학기술학회논문지
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• 제15권1호
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• pp.21-26
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• 2014

치과에서 사용되는 구강 치료용 요오드 용기는 개폐 시 용기의 캡에 부착되어 있는 칼날에 의해 치료용 실은 절단이 된다. 금속의 칼날은 요오드 용액과 반응하여 단기간에 부식이 되는 문제로 인해 환자의 위생에도 영향을 준다. 이러한 문제를 해결하기 위해 최근 세라믹 칼날로 대체되어진 제품들도 개발되어 생산되는데, 이때 세라믹 칼날은 수작업과 기계가공을 통해 만들어 진다. 본 연구에서는 세라믹 칼날을 분말사출성형공정으로 대량 생산할 수 있도록 20Cavity의 균일 충전을 위한 유동 시스템을 제안하였다. Moldflow를 이용하여 20cavity 유동성에 대한 시뮬레이션을 진행하였고, 금형제작과 수정을 통해 금형을 완성하였다. 사출성형 후 탈지와 소결공정을 통해 완성하고, 금형에 세라믹 칼날을 인서트 사출하여 캡 제품을 완성하였다. 본 연구를 통해 유효한 절단 성능을 갖는 세라믹칼날 대량생산 가능성을 검증하였다.

• 한국재료학회지
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• 제23권12호
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• pp.722-726
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• 2013

Freeze drying of a porous Cu-Sn alloy with unidirectionally aligned pore channels was accomplished by using a composite powder of CuO-$SnO_2$ and camphene. Camphene slurries with CuO-$SnO_2$ content of 3, 5 and 10 vol% were prepared by mixing with a small amount of dispersant at $50^{\circ}C$. Freezing of a slurry was done at $-25^{\circ}C$ while the growth direction of the camphene was unidirectionally controlled. Pores were generated subsequently by sublimation of the camphene during drying in air for 48 h. The green bodies were hydrogen-reduced at $650^{\circ}C$ and then were sintered at $650^{\circ}C$ and $750^{\circ}C$ for 1 h. XRD analysis revealed that the CuO-$SnO_2$ powder was completely converted to Cu-Sn alloy without any reaction phases. The sintered samples showed large pores with an average size of above $100{\mu}m$ which were aligned parallel to the camphene growth direction. Also, the internal walls of the large pores had relatively small pores. The size of the large pores decreased with increasing CuO-$SnO_2$ content due to the change of the degree of powder rearrangement in the slurry. The size of the small pores decreased with increase of the sintering temperature from $650^{\circ}C$ to $750^{\circ}C$, while that of the large pores was unchanged. These results suggest that a porous alloy body with aligned large pores can be fabricated by a freeze-drying and hydrogen reduction process using oxide powders.

• 한국세라믹학회지
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• 제35권4호
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• pp.311-318
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• 1998

The reaction bonded alumina ceramics with reinforced particles which have low shrinkage were pro-duced by blending of SiC or TiC or ZrO2 powders to the mixture of Al metal and Al2O3 powder. The powd-ers were attrition milled isostantically pressed and preheated tio 110$0^{\circ}C$ with a heating rate of $1.5^{\circ}C$/min The specimens were then sintered at the temperature range 1500 to 1$600^{\circ}C$ for 5 hours with a heating rate of 5$^{\circ}C$/min. The specimens showed 5-9% weight gain and 2-9% dimensional expansion through the complete oxidation of Al after preheating up to 11--$^{\circ}C$ the overall dimensional change of the specimens after the reaction sintering at 1500-1$600^{\circ}C$ was 6-12% The maximum densities were 92% theoretical. The fine grain-ed(average grain size :0.4 ${\mu}{\textrm}{m}$) microstructure were observed in the specimen with ZrO2 and SiC. But the microstructure of specimen with TiC was relatively coarse.(average grain size : 2.1 ${\mu}{\textrm}{m}$) The mullite phase was formed by the reaction of Al2O3 and SiO2 in a specimen with SiC. In the TiC contained specimen TiC was oxidized into TiO2 and finally reacted with Al2O3 to form Al2TiO5 during sintering.

• 구강회복응용과학지
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• 제37권1호
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• pp.1-15
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• 2021

치과용 재료의 적층가공제작은 기존 제작방식에 비해 복잡한 형태까지 제작할 수 있으며 절삭가공에 비해서도 기구나 재료의 소모가 적어 지속가능성이 장점으로 대두되고 있다. 적층가공 제작은 7가지 방식으로 분류할 수 있는데, 폴리머는 적층가공에 가장 적합한 재료로 용기중합방식으로 제작하며 기존 자가중합방식에 비해 높은 물성과 적합도를 가져 상용화에 더 적합하지만 상대적으로 낮은 강도로 인해 임시수복물로 주로 이용된다. 금속은 PBF (powder bed fusion) 방식을 주로 이용하며 주조방식에 비해 파괴인성과 밀도가 높지만 잔류응력이 높아 이를 제거하기 위한 후처리방식에 대한 연구가 필요하다. 세라믹은 분말과 레진폴리머를 혼합한 재료를 용기중합하는 방식이 일반적이다. 제작 후 폴리머제거나 소결과 같은 후처리 과정이 복잡하다. 상용화되려면 세라믹 적층가공에 의한 결과물의 낮은 강도와 체적정확성이 개선되어야 한다. 적층가공은 어떤 재료이건 공정조건에 따라 물성과 표면환경이 달라지므로 가장 적합한 공정조건을 찾기 위한 연구가 더 많이 필요하다고 사료된다.

• 소성∙가공
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• 제24권4호
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• pp.287-292
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• 2015

The possibility of chemical precipitation for recycled ammonium paratungstate (APT) was studied. WO₃ particles were synthesized by chemical precipitation method using a 1:2 weight ratio of APT:DI-water. At the 500℃ sintering temperature, the X-ray diffraction results showed that APT completely decomposed to WO₃. For the granulated powder WC-Co, vacuum heat treatment at proper temperatures increases tap density and flow-ability. Hardness of the WC-Co thermal spray coating layer was measured in the range HV 831~1266. Spray conditions for the best characteristic values were an oxygen flow rate=1500 scfh, a fuel flow rate = 5.25gph and a gun distance = 320mm.

• 한국세라믹학회지
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• 제33권11호
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• pp.1267-1275
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• 1996

Green sheet was prepared by tape casting in the composition of (1-x)Pb(Mg1/3Nb2/3)O3-PbTiO3 system using Pb(Mg1/3Nb2/3)O3 and PbTiO3 synthesized with PbO, Nb2O5 MgO and TiO2 The densest green sheet was obtained in the weight ratio 70:30 of powder to binder. Green sheet wasmultilayered in metal mould and formed into lamination at 7$0^{\circ}C$, 300kg/cm2 The lamination was sintered at 110$0^{\circ}C$ 2hr, Dielectric constant and Curie temperature of disc type sintered body was highered with increasing the amount of PbTiO3 and was in the range of 19000-21000, -7~45$^{\circ}C$ respectively. Green and sintered relative density of lamination was 61% and 95% respectively.

• 한국세라믹학회지
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• 제31권9호
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• pp.1069-1075
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• 1994

When ceramics are used as the parts of an engine and a machine, the tribological properties are very important. For the preparation of the resistance material for wear applications by the method of Reaction-Bonded Sintering, metal silicon and carbon black are mixed up into SiC powder, and Al2O3 and Fe2O3 are put as an additive. As the general properties, the bending strength and water absortion are measured in the normal temperature and the phase changies are investigated with XRD. The property of the resistance for wear applications is measured with the amount of friction and wear, friction coefficient and maximum asperties. And, the surface of wear is observed with SEM. With the results of this study, the optimal mol ratio of Si : C and the suitable quantity of the mixture of SiC are 7 : 3 and 40 wt%, respectively. In the case of the addition of Al2O3 (2 wt%), the resistance for friction and wear applications is prominent. The bending strength showed the highest peak when Al2O3 (4 wt%) and Fe2O3 (4 wt%) were added. The properties of friction and wear were related with the propagation velocity of crack rather than the bending strength.

• 한국세라믹학회지
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• 제34권6호
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• pp.591-600
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• 1997

Al2O3/Al composites were produced by displacement reaction method, which was carried out by immersing the sintered silica preform, which was prepared from fused silica powder, in molten aluminum. Because the molten aluminum did not penetrate into the silica preform with higher than 20% of porosity when the displacement reaction was accomplished at 100$0^{\circ}C$ for 10 hours in air atmosphere, the optimum range of sintering temperature of silica preform was from 135$0^{\circ}C$ to 140$0^{\circ}C$. The microstructure of this Al2O3/Al composites showed three-dimentionally co-continuous alumina, which provides wear resistance and high stiffness, and aluminium which acts as a toughnening phase. The grain size of the alumina in composites did not change with the particle size of the silica preform. The exact shape of the preform was retained and a net-shaped composite was produced. The representative Al2O3/Al composite prepared in this study showed 3.30mg/㎤ of bulk density, 350-430 MPa of flexural strength, 7.0 MPa.m1/2 of fracture toughness, and good machinability.