• 소성∙가공
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• 제25권2호
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• pp.91-95
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• 2016

This paper is concerned with modeling of a ductile fracture criterion for sheet metal considering anisotropy to predict the sudden fracture of advanced high strength steel (AHSS) sheets during complicated forming processes. The Lou−Huh ductile fracture criterion is modified using the Hill’s 48 anisotropic plastic potential instead of the von Mises isotropic plastic potential to take account of the influence of anisotropy on the equivalent plastic strain at the onset of fracture. To determine the coefficients of the model proposed, a two dimensional digital image correlation (2D-DIC) method is utilized to measure the strain histories on the surface of three different types of specimens during deformation. For the derivation of an anisotropic ductile fracture model, principal stresses (𝜎₁,𝜎₂, 𝜎₃) are expressed in terms of the stress triaxiality, the Lode parameter, and the equivalent stress (𝜂_𝐻, 𝐿,) based on the Hill’s 48 anisotropic plastic potential. The proposed anisotropic ductile fracture criterion was quantitatively evaluated according to various directions of the maximum principal stress. Fracture forming limit diagrams were also constructed to evaluate the forming limit in sheet metal forming of AHSS sheets over a wide range of loading conditions.

• 한국생산제조학회지
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• 제21권6호
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• pp.932-937
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• 2012

In the presented study, SM45C carbon steel parts were joined by friction welding. The welding process was carried out under optimized conditions using statistical approach. The study of SM45C is conducted with various combinations of process parameters. Parameter optimization, microstructure and mechanical property correlation are the major contribution of the study. The welded joints were produced by varying spindle revolution speed, friction pressure, upset pressure and burn-off length. Tension tests were applied to welded parts to obtain the strength of the joints. Fracturs properties were additionally obtained experimentally under fluctuated tensile loads. Microstructures using microphotographs were examined in the weld interface and weld region and heat affected zone and base metal and flash zone of welded parts. Finally, Hardness variations in welding zone and base metal were also obtained. Through these tests, the optimum conditions of parameters for ${\phi}20$ SM45C in friction welding were obtained when the friction spindle revolution was 1,950 rpm, the friction pressures was 30 MPs, upset pressures was 50 MPs.

• 소성∙가공
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• 제22권7호
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• pp.383-388
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• 2013

Metal flow of the beam blank during H-beam rolling was examined in order to correlate the rolling defects with the beam blank configuration. For this purpose, H-beam rolling was performed on the beam blank where stainless steel bolts were inserted as the marker at the web and flange. The positional variation of the marker was monitored at each rolling pass, and the result was compared with the 3D FEM simulation employing the point tracking function. The simulation results were reasonably agreed with the experimental within the error of 0.5~1mm on both web and flange of the H-beam. It is anticipated that the 3D FEM simulation employing the point tracking function provides the guidance information on analyzing the correlation between the rolling defects and the beam blank configuration in H-beam rolling.

• 대한화학회지
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• 제31권1호
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• pp.79-83
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• 1987

Triphenylmetal(IVA) methoxide 또는 triphenylmetal(IVA) methoxide와 phenylisocyanate를 1 : 500mole비로 혼합하여 여러온도에서 반응시켰다. Methyltrimethylsilyl ether, methyltriphenylsilyl ether 및 triphenyltin methoxide는 100$^{\circ}C$에서도 phenylisocyanate의 cyclid dimer(N,N'-diphenyluretidine-2,4-dione)를 생성하였으나, 다른 화합물들은 주로 cyclic trimer(phenylisocyanate)만을 생성하였다. 또한 200$^{\circ}C$이상에서는 모든 화합물들이 상당량의 diphenylcarbodiimide를 생성하였다. 이와 같은 반응결과로부터 phenylisocyanate의 cyclic polymerization의 mechanism과 (p-d)$\pi$ overlap에 대한 금속의 치환기 효과를 고찰하였다.

• 한국기계가공학회지
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• 제11권6호
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• pp.42-47
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• 2012

Followed by a paper on the Pig and Bone orthopedic prosthetic, this experiment using Phantom and Bone MRI imaging I, II of orthopedic prosthetic metal effect combines magnetic resonance imaging on metal signal-to-noise ratio(Signal to noise : SNR) and CNR(Contrast to noise: CNR), fat signal suppression(Fat-suppression) images was compared. Specimen trees to measure the reliability of the experimental reproducibility tests and statistical analysis using the SPSS statistical package was applied program SPSS(IBM SPSS Statistice 19) by * P = 0.000 < significance level $({\alpha})$ = 0.01 as a significant there was a correlation(** P < 0.01). SNR and CNR results did not directly proportional to the Titanium, Stainless, Clip CNR and fat signal suppression of the order of images of blood specimens was found to be close to the image. The impact of orthopedic prosthetic metals on magnetic resonance imaging in the diagnostic value of Titanium is relatively high and are meant more.

• 한국지반환경공학회 논문집
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• 제11권2호
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• pp.5-11
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• 2010

폐광산 주변의 광미장, 폐석더미로 인해 주변 지역의 토양 및 농작물들은 중금속으로 오염 될 수 있다. 본 연구는 주변토양 용도별, 농작물 재배품목별, 광산과의 이격거리별로 분류하여 광산 주변 중금속 오염실태조사를 수행하였다. 갱구인근 지역에서 Zn와 Pb이 토양오염기준치를 초과하였으며 다른 지역에 비해 광미장 지역과 논 경작지 토양의 중금속농도가 비교적 높은 것으로 나타났다. 광산과의 이격거리에 따른 중금속 농도는 갱구에서 거리가 멀어질수록 점차 감소하였다. 토양과 쌀 시료의 중금속 상관관계는 As와 Cd이 상관관계성이 있는 것으로 나타났으나 다른 중금속들은 관계성이 없는 것으로 조사되었다.

• 한국수처리학회지
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• 제26권6호
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• pp.43-51
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• 2018

In order to systematically and scientifically manage the organic and heavy metals against sediment at Daecheon Port, this study conducted particle composition, organic materials and heavy metals irradiation studies of sediments. Analysis of the grain size composition of sediments in the target study area showed the distribution characteristics of the mix of sand, silt and clay. That is, Station C (Stn. C) showed superior by fine-grained sediment, Station A and B (Stn. A and B) showed superior by coarse-grained sediment. The organic matter(COD, TOC, and IL) of Stn. C was appeared to be heavily polluted more than Stn. A and B. These data for the spatial properties in sediment showed that organic matter was related positively to the sediment silt-clay content. Also, in the case of heavy metals contamination in surface sediments, Stn. C was higher than Stn. A and B. Particularly, at the Stn. C, high organic matter concentration and C/N ratio value( >10) indicated that the sediment was composed highly of land-derived organic matter. From these results, it considered that the correlation analysis among to silt-clay, organic matter and heavy metal was found to have a good interrelationship.

• 센서학회지
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• 제33권3호
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• pp.125-133
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• 2024

Gas chromatography (GC) separation technology and metal oxide semiconductor (MOS) gas sensors have been integrated for the effective analysis of volatile sulfur compounds (VSCs) such as H₂S, CH₃SH, (CH₃)₂S, and (CH₃)₂S₂. The separation and detection characteristics of the GC/MOS system using diluted standard gases were investigated for the qualitative and quantitative analysis of VSCs. The typical concentrations of the standard gases were 0.1, 0.5, 1.0, 5.0, and 10.0 ppm. The GC/MOS system successfully separated H₂S, CH₃SH, (CH₃)₂S, and (CH₃)₂S₂ using a celite-filled column. The reproducibility of the retention time measurements was at a 3% relative standard deviation level, and the correlation coefficient (R²) for the VSC concentration was greater than 0.99. In addition, the chromatograms of single and mixed gases were almost identical.

• 환경위생공학
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• 제14권3호
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• pp.80-89
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• 1999

The ion exchange resins have been synthesized from chlormethyl styrene-1,4-divinyl benzene(DVB) with 1%, 5%, and 10%-crosslinking and macrocyclic ligand of cryptand type by copolymerization method and the adsorption characteristics of uranium(VI), lead(II) and holmium(III) ions have been investigated in various experimental conditions. The correlation between the adsorption characteristics of rare earths and transition metal on the resins and stability constants of complexes with macrocyclic ligand have been examined. The $UO_2^{2+}$ aqueous solutions are not adsorbed on the resins below pH 3.0, but the power of adsorption of $UO_2^{2+}$ increased rapidly above pH 4.0. The adsorption power was in the order of 1%, 10%, and 5%-crosslinked resin, but adsorptive characteristics of resins decreased in proportion to the order of dielectric constants of solvents.

• 대한화학회지
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• 제44권3호
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• pp.194-199
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• 2000

The chemical behavior for Mo(0) and W(0) complexes, [M(CO)$_2$(PPh$_3$)$_4$] (M=Mo and W),has been investigated by UV-vis spectroscopic, magnetic, and electrochemical methods. Three absorption bands are observed in the UV-spectra. The crystal-field-splitti ng energy, spin-pairing energy, and bond strengths were deduced from the spectra. The metal d electrons in both complexes seemed to be delocalized in low-spin state.Metal ligand correlation appeared to strongly depend on bond strengths and diamagnetic properties. In electrochemical processes, both complexes exhibit an irreversible reduction wave.