• Title/Summary/Keyword: Metal Surface Defects

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A Study on Ultrasonic for MoSi$_2$ (MoSi$_2$의 초음파에 관한 기초적 연구)

  • 김유철;남궁재관
    • Journal of the Korean Society of Safety
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    • v.9 no.1
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    • pp.28-30
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    • 1994
  • Ultrasonic for MoSi$_2$/Y. C. Kim, C. K. Namkoong/MoSi$_2$in the silicides has excellence in the oxidation and corrosion resistence. When the solid state bonding sintered-MoSi$_2$/metal or the thermal sprayed coating by powder-MoSi$_2$on the metal are carried out, the defects may be occured at the bonded surface. So, the method for evaluating the existence of the defects by non-destructive inspection is strongly desired. Here, the characteristics of ultrasonic for sintered-MoSi$_2$are elucidated and the possibility of the detection of defects using by ultrasonic is investigated.

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Characteristics of Slurry Filter for Reduction of CMP Slurry-induced Micro-scratch (CMP 공정에서 마이크로 스크래치 감소를 위한 슬러리 필터의 특성)

  • 김철복;김상용;서용진
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.14 no.7
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    • pp.557-561
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    • 2001
  • Chemical mechanical polishing (CMP) process has been widely used to planarize dielectric layers, which can be applied to the integraded circuits for sub-micron technology. Despite the increased use of CMP process, it is difficult to accomplish the global planarization of in the defect-free inter-level dielectrics (ILD). Especially, defects such as micro-scratch lead to severe circuit failure which affect yield. CMP slurries can contain particles exceeding 1㎛ in size, which could cause micro-scratch on the wafer surface. The large particles in these slurries may be caused by particles agglomeration in slurry supply line. To reduce these defects, slurry filtration method has been recommended in oxide CMP. In this work, we have studied the effects of filtration and the defect trend as a function of polished wafer count using various filters in inter-metal dielectrics(IMD)-CMP process. The filter installation in CMP polisher could reduce defects after IMD-CMP process. As a result of micro-scratch formation, it is shown that slurry filter plays an important role in determining consumable pad lifetime. The filter lifetime is dominated by the defects. We have concluded that slurry filter lifetime is fixed by the degree of generating defects.

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Prediction of Positions of Gas Defects Generated from Core (중자에서 발생한 가스 결함 위치 예측)

  • Matsushita, Makoto;Kosaka, Akira;Kanatani, Shigehiro
    • Journal of Korea Foundry Society
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    • v.42 no.1
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    • pp.61-66
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    • 2022
  • Hydraulic units are important components of agricultural and construction machinery, and thus require high-quality castings. However, gas defects occurring inside the sand cores of the castings due to the resin used is a problem. This study therefore aimed to develop a casting simulation method that can clarify the gas defect positions. Gas defects are thought to be caused by gas generated after the molten metal fills up the mold cavity. The gas constant is the most effective factor for simulating this gas generated from sand cores. It is calculated by gas generating temperature and analysis of composition in the inert gas atmosphere modified according to the mold filling conditions of molten metal. It is assumed that gases generated from the inside of castings remain if the following formula is established. [Time of occurrence of gas generation] + [Time of occurrence of gas floating] > [Time of occurrence of casting surface solidification] The possibility of gas defects is evaluated by the time of occurrence of gas generation and gas floating calculated using the gas constant. The residual position of generated gases is decided by the closed loops indicating the final solidification location in the casting simulation. The above procedure enables us to suggest suitable casting designs with zero gas defects, without the need to repeat casting tests.

A Study of the Formation of Binary Intermediate Layer on Pd-based Hydrogen Separation Membrane Using Various Types of Metal Oxides (다양한 형태의 금속 산화물을 이용한 Pd계 복합 수소분리막의 2원계 중간층 형성에 관한 연구)

  • Hwang, In-Hyuck;Kim, Sung Su
    • Applied Chemistry for Engineering
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    • v.29 no.2
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    • pp.196-200
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    • 2018
  • In this study, the intermediate layer in Pd-based hydrogen separation membrane was synthesized to minimize the surface roughness and defects using powder-type and sol-type metal oxides. The surface properties and gas permeation characteristics were analysed by SEM and $N_2$ gas permeation test. The coating layer composed of sol type metal oxides has smooth surface, especially the layer coated by $TiO_2$ sol has little pin holes, cracks and defects. The binary layer composed of powder type and sol type metal oxides has similar flux characteristics to a single sol type layer. The Pd-based composite membrane improved by the binary intermediate layer exhibited $0.32mol/m^2s$ of the hydrogen permeation flux with a selectivity ($H_2/N_2$) of ~10,890 at 672 K and a pressure difference of 1 bar.

Assessement of Forming Defects in Hot Backward Extruded Ti-6Al-4V Tube (열간 후방압출된 Ti-6Al-4V 튜브의 성형결함 해석)

  • 염종택;심인규;나영상;박노광;홍성석;심인옥
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.05a
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    • pp.347-350
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    • 2003
  • The metal forming behavior and defect formation in Ti-6Al-4V tube during hot backward extrusion were investigated. To predict the forming-defects such as shear band, inner cracks or surface cracks, dynamic material model(DMM) including Ziegler's instability criterion and modified Cockcroft-Latham fracture criterion(C-L model) were used. These models were coupled to the internal variables generated from FE analysis. The chilling effect and friction indicated a great influence on the deformation mode of the tube and the formation of surface cracks. The simulation results for the backward extrusion were compared with the experimental observations.

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An Experimental Study on the Turning Property of Welded Material (용접부의 선삭특성에 관한 실험적 연구)

  • Jang, Bok-Deuk
    • Journal of the Korean Society for Precision Engineering
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    • v.3 no.3
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    • pp.13-21
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    • 1986
  • Turning property of metal is affected by the cutting condition, tool geome- try and cutting material. But the turning property of welded material is not welknown. Welded structures usually contain nonhomogeneity, defects and resi- dual stresses due to differential contraction between welded metal and base metal. In this paper, authors conducted the experimental test on the turning property, by changing turning condition and welding electrodes of the welded specimens. The results obtained in these experimental tests are as follows; (1) Within the limit of this experimental test, the cutting force of the weld zone is bigger than that of base metal, and this phenomena is caused by the different mechanical property of the weld zone. The range of the variation of cutting force in the weld zone is caused by the nonhomogeneity of the weld zone, respectively. (2) The surface roughness follows the general characteristic of the effect of cutting condition on the surface roughness and the surface roughness of the weld zone shows coarse surface comparing with that of the base metal. (3) The specimen welded by the electrode E4301, shows worse cutting property than that of E4361 and E4313.

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The Effect of Oxide Layer Thickness to the Scale Defects Generation during Hot finish Rolling (열연사상 압연시 스케일 결함발생에 미치는 산화피막 두께의 영향)

  • 민경준
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1999.08a
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    • pp.412-422
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    • 1999
  • Scale defects generated on the strip surface in a tandem finishing mill line are collected from the strip trapped among the production mills by freezing the growing scale on the strip by the melt glass coating and shutting down the line simultaneously. The samples observed of its cross sectional figure showed the process of scale defect formation where the defects are formed at the base metal surface by thicker oxidized scale during each rolling passes. The properties of the oxidized layer growth both at rolling and inter-rolling are detected down sized rolling test simulating carefully the rolling condition of the production line. The thickness of the oxidized layer at each rolling pass are simulated numerically. The critical scale thickness to avoid the defect formation is determined through the expression of mutual relation between oxidized layer thickness and the lanks of the strip called quality for the scale defects. The scale growth of scale less than the critical thickness and also to keep the bulk temperature tuning the water flow rate and cooling time appropriately. Two units of Inerstand Cooler are designed and settled among the first three stands in the production line. Two units of scale defect is counted from the recoiled strip and the results showed distinct decrease of the defects comparing to the conventionaly rolled products.

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Microstructure, Defects and Mechanical Properties of DED Metal Deposited Heat-Resistant Mold Steel (내열 금형강 DED 금속적층재의 조직, 결함 및 기계적 물성 평가)

  • Choi, Sung-Jong;Kim, Ho-Chan
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.21 no.3
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    • pp.12-21
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    • 2022
  • Directed energy deposition (DED) was adopted as a metal additive manufacturing method to develop a mold for the hot stamping process. The test piece was machined from Heatvar laminate material, and results were obtained through microstructure and defect observations, as well as hardness, tensile strength, and joint strength tests. 1) Spherical pores and irregular-shaped cavities were observed as lamination defects, and columnar dendrites formed in the structure, which tended to become coarse upon heat treatment. 2) The hardness of the heat-treated material (480HV) was slightly lower than that of the non-heat-treated material (500HV). 3) In the tensile test, the maximum tensile stress and strain of the heat-treated material were 1392 MPa and 15%, respectively, which were slightly higher than the values of 1381 MPa and 13%, respectively, for the non-heat-treated material. 4) In the case of the early final fracture in the tensile test, in most cases, pores or irregularly shaped cavities were observed at the fracture surface or near the surface. 5) In the joint strength test, most of the specimens finally fractured in the laminated metal area, and the fracture surface was intragranular. In addition, dimples formed over the entire area on the fracture surface of the fractured specimen after sufficient elongation.

Metal Surface Defect Detection and Classification using EfficientNetV2 and YOLOv5 (EfficientNetV2 및 YOLOv5를 사용한 금속 표면 결함 검출 및 분류)

  • Alibek, Esanov;Kim, Kang-Chul
    • The Journal of the Korea institute of electronic communication sciences
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    • v.17 no.4
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    • pp.577-586
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    • 2022
  • Detection and classification of steel surface defects are critical for product quality control in the steel industry. However, due to its low accuracy and slow speed, the traditional approach cannot be effectively used in a production line. The current, widely used algorithm (based on deep learning) has an accuracy problem, and there are still rooms for development. This paper proposes a method of steel surface defect detection combining EfficientNetV2 for image classification and YOLOv5 as an object detector. Shorter training time and high accuracy are advantages of this model. Firstly, the image input into EfficientNetV2 model classifies defect classes and predicts probability of having defects. If the probability of having a defect is less than 0.25, the algorithm directly recognizes that the sample has no defects. Otherwise, the samples are further input into YOLOv5 to accomplish the defect detection process on the metal surface. Experiments show that proposed model has good performance on the NEU dataset with an accuracy of 98.3%. Simultaneously, the average training speed is shorter than other models.

Investigation on DHF Application at Metal CMP Cleaning Process (Metal CMP 세정 공정에서 DHF 적용에 관한 연구)

  • 김남훈;김상용;김인표;장의구
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.7
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    • pp.569-572
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    • 2003
  • In this study, we evaluated the dilute HF cleaning to reduce residual defects made by metal CMP process. The purpose of this test is to observe the existence of barrier metal damage during DHF cleaning on condition that it should not affect metal thin film reliability, so we will get rid of slurry residual particles as a main defect of the metal CMP process for the better yield. In-line defect data showed us that slurry residual particles were removed by DHF application. The HF rinse significantly reduced metal contamination levels and surface roughness. The best effect by additional oxide loss was discovered when Dilute HF condition is 10".