• 한국식품과학회지
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• 제23권1호
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• pp.19-24
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• 1991

고형 유지의 상승 융점 변화에 영향을 주는 여러 가지 조건들 중 처리 온도와 시간이 미치는 영향에 대하여 연구하였다. 실험결과 처리 온도가 $4^{\circ}C$ 이하인 경우는 시간에 의한 영향을 크게 받지는 않았다. 그러나 $10^{\circ}C$에서 처리한 경우는 저융점 트리글리세리드들이 미처 결정을 형성하지 못하였으므로 돈지 및 팜유에서는 비교적 낮은 온도에서 융점이 측정되었다. 그러므로 고형 유지의 융점을 측정하기위해서는 유지 내의 자유 에너지도를 낮춘 상태에서 충분한 결정을 형성 시킨 후 측정해야하므로 바람직한 전처리 조건은 $4^{\circ}C$에서 방치하여 고형화한 후 융점을 측정하는 것이다.

• 보존과학연구
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• 통권21호
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• pp.57-75
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• 2000

We performed the scientific analysis through composition analysis, micro-structure investigation, melting point and hardness test to the glass beads excavated at Naesanri in Gosung. Through this investigation, we could examine closely the characterization of raw materials and manufacture technique As a result of micro-structure investigation of glass beads, it appeared that the bubbles in glass beads have remained. Coloring agents of yellow glass bead was remained to the shape of inclusion. And on observing the transparent solid particle, we can know that these do not melt the raw materials because of low melting temperature of a crucible. The result of composition analysis of all glass beads using ICP, these were classified as $Na_2O_2$-$SiO_2$ type of glass. Also, these added to $AI_2O_3$ to improve the durability. The value of Vickers hardness of glass beads appeared the HV 490-530. The HV 1,440 of the transparent solid particle was much more than that of inner glass bead. This means that raw materials do not melt because of a low melting temperature of a crucible. The result of melting temperature analysis of glass beads using DSC/TGA, it was measured about $1,250^{\circ}C$.

• ETRI Journal
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• 제41권6호
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• pp.820-828
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• 2019

A highly reliable conductive adhesive obtained by transient liquid-phase sintering (TLPS) technologies is studied for use in high-power device packaging. TLPS involves the low-temperature reaction of a low-melting metal or alloy with a high-melting metal or alloy to form a reacted metal matrix. For a TLPS material (consisting of Ag-coated Cu, a Sn96.5-Ag3.0-Cu0.5 solder, and a volatile fluxing resin) used herein, the melting temperature of the metal matrix exceeds the bonding temperature. After bonding of the TLPS material, a unique melting peak of TLPS is observed at 356 ℃, consistent with the transient behavior of Ag₃Sn + Cu₆Sn₅ → liquid + Cu₃Sn reported by the National Institute of Standards and Technology. The TLPS material shows superior thermal conductivity as compared with other commercially available Ag pastes under the same specimen preparation conditions. In conclusion, the TLPS material can be a promising candidate for a highly reliable conductive adhesive in power device packaging because remelting of the SAC305 solder, which is widely used in conventional power modules, is not observed.

• Korean Chemical Engineering Research
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• 제46권2호
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• pp.340-347
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• 2008

용해공정의 경우, 용해물을 균일한 상태로 유지하고 용해로에 투입되는 연료의 연소상황을 분석하기 위해 폐가스 유속을 측정한다. 현재 시중에 많은 종류의 기체유속 측정장치들이 있지만, 용해공정에서 발생하는 폐가스는 고온이고, 저속이며, dust를 많이 갖고 있어 기존의 측정장치들은 이런 조건에 적합하지 않다. 따라서 저속에 반응할 만큼 충분히 정밀하고 고온에 견딜 수 있는 새로운 방식의 측정장치를 제작하였다. 현장테스트 결과, 제작된 측정 장치는 유속의 작은 변화에도 반응할 정도로 충분히 민감하고 온도변화를 빠르게 감지하기 때문에 용해로의 온도제어에 도움을 줄 것으로 기대된다.

• 한국재료학회지
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• 제15권9호
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• pp.598-603
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• 2005

To develope new lead-free solders with the melting temperature close to that of Sn-37Pb$(183^{\circ}C)$, Sn-0.7Cu-5Pb-1Ga, Sn-0.7Cu-5Pb-1Ag, Sn-0.7Cu-5Pb-5Bi-1Ag, and Sn-0.7Cu-SBi-1Ag alloys were composed by adding low-netting elements such as Ga, Bi, Pb, and Ag to Sn-0.7Cu. Then the melting temperatures, microstructures, wettability, and adhesion properties of these alloys were evaluated. DSC analysis showed that the melting temperature of Sn-0.7Cu-SPb-1Ga was $211^{\circ}C$, and those of other alloys was in the range of $192\~200^{\circ}C$. Microstructures of these alloys after heat-treatment at $150^{\circ}C$ for 24 hrs were basically composed of coarsely- grown $\beta-Sn$ grains, and $Cu_6Sn_5$ and $Ag_3Sn$ intermetallic precipitates. Sn-0.7Cu-5Pb-1Ga and Sn-0.7Cu-5Pb-5Bi-1Ag showed excellent wettability, while Sn-0.7Cu-5Bi-1Ag and Sn-0.7Cu-5Pb-5Bi-1Ag revealed good adhesion strength with the Cu substrates. Among 4 alloys, Sn-0.7Cu-5Pb-5Bi-1Ag with the lowest melting temperature $(192^{\circ}C)$ and relatively excellent wettability and adhesion strength was suggested to be the best candidate solder to replace Sn-37Pb.

• 태양에너지
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• 제16권2호
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• pp.113-122
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• 1996

본 연구는 수직원통형 빙축열조 내에 상변화물질로서 순수한 물을 $-10^{\circ}C$의 초기 과냉온도로 응고시킨 후, 작동유체의 입구온도를 $7^{\circ}C,\;4^{\circ}C,\;1^{\circ}C$로, 작동유체의 유입방향을 상향과 하향으로 각각 변화시키면서 외향용융시켰을 경우, 시간경과에 따른 축열매질의 온도분포, 상경계면의 형상, 용융율, 용융에너지를 실험적으로 구하여 이를 비교 검토한 것이다. 작동유체의 입구온도가 $7^{\circ}C,\;4^{\circ}C$의 경우에는 작동유체의 유입방향이 상 하향 모두 물의 최대 밀도점인 $4^{\circ}C$ 부근에서 일시적으로 온도가 상승하지 않고 일정 시간동안 정체하는 온도정체구간이 나타났다. 또한, 용융이 진행됨에 따라 물이 축열조의 하부에 적체되고, 이에 따라 하부에서의 용융이 활발히 진행됨으로써 상경계면 형상은 전체적으로 종모양 형태의 곡선을 나타낸다. 작동 유체의 입구온도가 $7^{\circ}C$인 경우, 용융율(Vl/Vtot)과 용융에너지는 작동유체의 유입방향이 상향인 경우가 하향인 경우에서보다 크게 나타난 반면, 작동유체의 입구온도가 $4^{\circ}C,\;1^{\circ}C$인 경우는 $7^{\circ}C$의 경우와는 달리 하향인 경우가 상향인 경우에서보다 큰 것으로 나타났다.

• Fibers and Polymers
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• 제5권3호
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• pp.245-251
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• 2004

Poly(trimethylene terephthalate-co-trimethylene 2,6-naphthalate)s (P(TT-co-TN)s) with various copolymer composition were synthesized, and their chain structure, thermal property and crystalline structure were investigated by using $^1$H-NMR spectroscopy, differential scanning calorimetry (DSC) and wide-angle X-ray diffraction (WAXD), respectively. It was found from sequence analysis that all the P(TT-co-TN) copolymers synthesized have a statistical random distribution of TT and TN units. It was also observed from DSC thermograms that the glass transition temperature increases linearly with increasing the TN comonomer content, whereas the melting temperature of copolymer decreases with increasing the corresponding comonomer content in respective PTT- and PTN-based copolymer, showing pseudo-eutectic melting behavior. All the samples melt-crystallized isothermally except for P(TT-co-66 mol % TN) exhibit multiple melting endotherms and clear X-ray diffraction patterns. The multiple melting behavior originates from the dual lamellar population and/or the melting-recrystallization-remelting. The X-ray diffraction patterns are largely divided into two classes depending on the copolymer composition, i.e., PTT and PTN $\beta$-form diffraction patterns, without exhibiting cocrystallization.

• Journal of Astronomy and Space Sciences
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• 제33권4호
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• pp.305-311
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• 2016

The spatial size and variation of Arctic sea ice play an important role in Earth's climate system. These are affected by conditions in the polar atmosphere and Arctic sea temperatures. The Arctic sea ice concentration is calculated from brightness temperature data derived from the Defense Meteorological Satellite program (DMSP) F13 Special Sensor Microwave/Imagers (SSMI) and the DMSP F17 Special Sensor Microwave Imager/Sounder (SSMIS) sensors. Many previous studies point to significant reductions in sea ice and their causes. We investigated the variability of Arctic sea ice using the daily sea ice concentration data from passive microwave observations to identify the sea ice melting regions near the Arctic polar ice cap. We discovered the abnormal melting of the Arctic sea ice near the North Pole during the summer and the winter. This phenomenon is hard to explain only surface air temperature or solar heating as suggested by recent studies. We propose a hypothesis explaining this phenomenon. The heat from the deep sea in Arctic Ocean ridges and/or the hydrothermal vents might be contributing to the melting of Arctic sea ice. This hypothesis could be verified by the observation of warm water column structure below the melting or thinning arctic sea ice through the project such as Coriolis dataset for reanalysis (CORA).

• 한국가시화정보학회지
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• 제1권2호
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• pp.52-57
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• 2003

The present paper investigated the effect of ultrasonic vibrations on the melting process of a phase-change material (PCM). The melting process in the square cavity with a heated vertical wall has been studied in terms of acoustic streaming. In the present study, applying with ultrasonic vibrations to the liquid were found to induce acoustic streaming which was clearly observed using by a particle image velocimetry (PIV) and a thermal infrared camera. The experimental results revealed that acoustic streaming could accelerate the melting process as much as 2.5 times, compared to the rate of natural melting (i. e., the melting without acoustic streaming). In addition, temperature and Nusselt numbers over time provided conclusive evidence of the important role of the acoustic streaming on the melting phenomena of the PCM.

• 한국자원리싸이클링학회:학술대회논문집
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• 한국자원리싸이클링학회 2001년도 정기총회 특별강연 및 춘계학술연구발표회(2)
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• pp.19-22
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• 2001

In recent years, the creation of waste recycling society has been required to cope with the traditional ways of waste treatments. In accordance with the package recycling law in force, calls for the developments of new waste treatment techniques suitable for 21st century are growing higher. A new ash melting furnace system named Eco Burner Ash Melting Furnace System has been developed. It is a burner type ash melting system in which the fluffs made of the plastics segregated from municipal solid wastes are directly fired at high temperature in the furnace. This system provides an economical ash melting system because plastic wastes or paper scraps that have heretofore been considered hard to recycle are used in compensation for fossil fuel. In this paper, we describe the ash melting test results obtained from a substantiative facility.