• Title/Summary/Keyword: Melting Range

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Material Characteristics of Ti-6Al-4V Alloy Manufactured by Electron Beam Melting for Orthopedic Implants (전자빔 용해 방법으로 제조된 정형외과 임플란트용 Ti-6Al-4V 합금의 재료 특성 분석)

  • Gang, Gwan-Su;Jeong, Yong-Hun;Jang, Tae-Gon;Yang, Jae-Ung;Jeong, Jae-Yeong;Park, Gwang-Min;U, Su-Heon;Park, Tae-Hyeon
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2018.06a
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    • pp.25-25
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    • 2018
  • Electron beam melting (EBM) is one of powder based additive manufacturing technology used to produce parts for high geometrical complexity and directly with three-dimensional computer aided design (CAD) model. It is kind of the most promising methods with additive manufacturing for a wide range of medical applications, such as orthopedic, dental implant, and etc. This research has been investigated the microstructure and mechanical properties of as fabricated and hot iso-static pressing (HIP) processed specimens, which are made by an Arcam A1 EBM system. The Ti-6Al-4V titanium alloy powder was used as a material for the 3 dimensional printing specimens. Mechanical properties were conducted with EBM manufacturing and computer numerical control (CNC) machining specimens, respectively. Surface morphological analysis was conducted by scanning electron microscopy (SEM) for their surface, dissected plan, and fractured surface after tensile test. The mechanical properties were included tensile stress-strain and nano-indentation test as a analysis level between nano and macro. As following highlighted results, the stress-strain curves on elastic region were almost similar between as fabricated and HIP processed while the ductile (plastic deformed region) properties were higher with HIP than that of as fabricated processed.

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Volcanism and Petrogenesis of Dodong Basaltic Rocks in the Ulleung Island, East Sea (울릉도 도동현무암질암류의 화산작용과 암석성인)

  • Hwang, Sang Koo;Kim, Jae Ho;Jang, Yundeuk
    • The Journal of the Petrological Society of Korea
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    • v.26 no.4
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    • pp.361-371
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    • 2017
  • We investigated geochemical characteristics of the Dodong Basaltic Rocks in the lower part of the Ulleung Island. They have lithological range of alkali basalt to trachybasalt, belonging to Na and K subseries of alkaline series. They mostly fall within the field of alkalline within-plate basalts on tectonic discrimination diagrams, and then plot in the field of oceanic island basalt (OIB). Geochemically, extension of lithospheric mantle and asthenospheric upwelling after East Sea under an Cenozoic extensional tectonic setting might be a heat source for partial melting of the enriched lithospheric mantle, which might generate the basaltic magma. But we cannot exclude that mantle plume might also be a heat source for melting of the lithospheric mantle.

Electrical Characteristics of the Ag Past with addition of Low-melting Alloy of Bi58Sn42 for Metal Mesh Touch Sensors (저융점 합금(Bi58Sn42)을 이용한 Metal Mesh Touch Sensor용 Ag 페이스트의 전기적 특성)

  • Kim, Tae-Hyung;Heo, Young-Woo;Kim, Jeong-Joo;Lee, Joon-Hyung
    • Journal of the Korean institute of surface engineering
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    • v.50 no.6
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    • pp.510-515
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    • 2017
  • In this study, a transient liquid phase sintering (TLPS) process of Ag pastes mixed with a fusible metal alloy of Bi58Sn42 with the melting temperature of $138^{\circ}C$, was examined. After screen printing of the Ag pastes with and without Bi58Sn42 powders on polyimide (PI) substrates, the electrodes were heat-treated at different temperatures in the range between 150 and $300^{\circ}C$ for 60 min in air. Comparing the electrical conductivity of the Ag pastes with and without Bi58Sn42 alloy powder after the heat treatment, it was manifested that the low melting temperature alloy definitely played a major role in an increased conductivity when it is added into the Ag pastes by providing more electrical conduction paths between Ag particles. This can be explained by the fact that capillary force of the melts of Bi58Sn42 can contribute to the rearrangement of the Ag particles during the heat-treatment inducing better connectivity between the Ag particles.

Study on the Reduction of Molten EAF Slag (용융 전기로 슬래그의 환원반응에 관한 연구)

  • Joo, Seong-Woong;Shin, Jong-Dae;Shin, Dong-Kyung;Hong, Seong-Hun;Ki, Jun-Sung;Hwang, Jin-Il;You, Byung-Don
    • Korean Journal of Metals and Materials
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    • v.50 no.10
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    • pp.753-761
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    • 2012
  • The reduction behavior of low level oxides such as (T.Fe), (MnO) and ($P_2O_5$) in molten EAF slag was investigated using commercial reductants. In an air atmosphere, the slag volume increased and the reduction rate of the slag was very low due to the oxidation loss of reductants by oxygen in the air. The reduction rate of the slag was also low when a commercial reductant was used alone in an Ar gas atmosphere. The reason is probably because the material transfer through the interface between the slag and reductant is difficult due to the formation of high melting point oxide. When reductants were mixed with burnt lime in order to form low melting point reaction products, the reduction rate of the slag increased up to the range of 45-70%. By using the mixtures of reductants and burnt lime so as to form a low melting point slag at the reaction end, the reduction rate of the slag was improved up to 60-85%.

Evaluation of marginal and internal fit of metal copings fabricated by selective laser melting (SLM 방식으로 제작한 도재관 금속하부구조물의 변연 및 내면 적합도 평가)

  • Sung-Ryung Bae;Ha-Bin Lee;Mi-Jun Noh;Ji-Hwan Kim
    • Journal of Technologic Dentistry
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    • v.45 no.1
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    • pp.1-7
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    • 2023
  • Purpose: To evaluate the marginal and internal fit of metal coping fabricated by a metal three-dimensional (3D) printer that uses selective laser melting (SLM). Methods: An extraoral scanner was used to scan a die of the prepared maxillary right first molar, and the coping was designed using computer-aided design software and saved as an stereo lithography (STL) file. Ten specimens were printed with an SLM-type metal 3D printer (SLM group), and 10 more specimens were fabricated by casting the castable patterns output generated by a digital light processing-type resin 3D printer (casting the 3D printed resin patterns [CRP] group). The fit was measured using the silicon replica technique, and 8 points (A to H) were set per specimen to measure the marginal (points A, H) and internal (points B~G) gaps. The differences among the groups were compared using the Mann-Whitney U-test (α=0.05). Results: The mean of marginal fit in the SLM group was 69.67±18.04 ㎛, while in the CRP group was 117.10±41.95 ㎛. The internal fit of the SLM group was 95.18±41.20 ㎛, and that of the CRP group was 86.35±32 ㎛. As a result of statistical analysis, there was a significant difference in marginal fit between the SLM and CRP groups (p<0.05); however, there was no significant difference in internal fit between the SLM group and the CRP group (p>0.05). Conclusion: The marginal and internal fit of SLM is within the clinically acceptable range, and it seems to be applicable in terms of fit.

Effect of Sn Doping on the Thermoelectric Properties of P-Type Mg3Sb2 Synthesized by Controlled Melting, Pulverizing Followed by Vacuum Hot Pressing

  • Rahman, Md. Mahmudur;Kim, Il-Ho;Ur, Soon-Chul
    • Korean Journal of Materials Research
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    • v.32 no.3
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    • pp.132-138
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    • 2022
  • Zintl phase Mg3Sb2 is a promising thermoelectric material in medium to high temperature range due to its low band gap energy and characteristic electron-crystal phonon-glass behavior. P-type Mg3Sb2 has conventionally exhibited lower thermoelectric properties compared to its n-type counterparts, which have poor electrical conductivity. To address these problems, a small amount of Sn doping was considered in this alloy system. P-type Mg3Sb2 was synthesized by controlled melting, pulverizing, and subsequent vacuum hot pressing (VHP) method. X-ray diffraction (XRD) and scanning electron microscopy (SEM) were used to investigate phases and microstructure development during the process. Single phase Mg3Sb2 was successfully formed when 16 at.% of Mg was excessively added to the system. Nominal compositions of Mg3.8Sb2-xSnx (0 ≤ x ≤ 0.008) were considered in this study. Thermoelectric properties were evaluated in terms of Seebeck coefficient, electrical conductivity, and thermal conductivity. A peak ZT value ≈ 0.32 was found for the specimen Mg3.8Sb1.994Sn0.006 at 873 K, showing an improved ZT value compared to intrinsic one. Transport properties were also evaluated and discussed.

Fire at an Indoor Shooting Range in Busan I. Fire Reconstruction (부산 실내사격장 화재 I. 화재재현)

  • Park, Woe-Chul
    • Fire Science and Engineering
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    • v.24 no.2
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    • pp.114-119
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    • 2010
  • The fire at a Busan indoor shooting range on November 14, 2009 was reconstructed by using a computational fluid dynamics model for fire simulations, in order to investigate the cause of the heavy death toll in a short period of time. Spread of the flame and smoke, and temperature distribution obtained by fire simulation were compared with the results of fire investigation based on the CCTV recordings. The flame and smoke flew out violently through the door into the cafeteria from the shooting range, and the cafeteria was filled with smoke just within 3 seconds followed by the onset of fire. This is consistent with the CCTV recordings. It was confirmed, as a result, that people in the cafeteria did not have enough evacuation time. The computed temperature at the door knob reached about $1400^{\circ}C$, near its melting point.

Film Properties of TiO2 Made by Activated Reactive Evaporation (활성화 반응으로 제작된 TiO2의 박막특성)

  • Park, Yong-Gwon;Choi, Jae-Ha
    • Journal of the Korean Society for Heat Treatment
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    • v.14 no.3
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    • pp.151-154
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    • 2001
  • $TiO_2$ thin film has wide application because of its high capacitanca, reflection, and good transmissivity in visible range. $TiO_2$ thin film can be made by thermal deposition method, reactive evaporation method, activated reactive evaporation(ARE) method. In the case of thermal deposition, the oxygen deficiency can occur because the melting point of Ti is very high. While in the case of reactive evaporation, high density $TiO_2$ can not be made, because reactive gas($O_2$) and evaporated material(Ti) are not fully combined, activated reactive evaporation, $TiO_2$ is easily deposited at lower gas pressure compared with reactive evaporation because the ionized reactive gas is made by plasma. Therefore, activated reactive evaporation is very useful to deposit the material having the high melting point. In this work, we formed $TiO_2$ thin film by activated reactive evaporation method. The surface of $TiO_2$ thin film was analyzed by X-ray photoelectron spectroscopy. The surface morphology which was analyzed by atomic force microscopy(AFM) shows that feature of the film surface is uniform. The dielectric capacitance, withstanding voltage were $600{\mu}F/cm^2$, 0.4V respectively. In further work, we can increase the withstanding voltage by improving the deposition parameter of substrates.

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Thermal Characteristic Simulation and Property Evaluation of High Melting Point Materials by Pulsed Current Activated Sintering Process (PCAS공정에 의한 고융점 소결체 열전달 해석 및 특성분석)

  • Nam, Hyo-Eun;Jang, Jun-Ho;Park, Hyun-Kuk;Oh, Ik-Hyun
    • Journal of Sensor Science and Technology
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    • v.26 no.3
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    • pp.214-222
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    • 2017
  • In this study, the effects of internal heat treatment associated sintering temperatures were simulated by the Finite Element Method (FEM). The sintering mechanism of pulsed current activated sintering process (PCAS) is still unclear because of some unexplainable heat transfer phenomena in coupled multi-physical fields, as well as the difficulty in measuring the interior temperatures of metal powder. We have carried out simulation study to find out thermal distributions between graphite mold and Ruthenium powder prior to PCAS process. For PCAS process, heating rate was maintained at $100^{\circ}C/min$ the simulation indicates that the sintering temperature range was between $1000^{\circ}C$ to $1300^{\circ}C$ under 60 MPa. The heat transfer inside the Ruthenium sintered-body sample was modelled through the whole process in order to predict the minimum interior temperature. Thermal simulation shows that the interior temperature gradient decreased by graphite punch length and calculation results well agreed with the PCAS field test results.

Predicting Micro-Thickness of Phase Fronts in Propellants (추진제의 마이크로 스케일 상면 두께 예측)

  • Yoh Jai-Ick
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2005.11a
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    • pp.13-21
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    • 2005
  • I consider the structure of steady wave system which is admitted by the continuum equations for materials that undergo phase transformations with exothermic chemical reaction. In particular, the dynamic phase front structures between liquid and gas phases, and solid and liquid phases are computationally investigated. Based on the one-dimensional continuum shock structure analysis, the present approach can estimate the nano-width of waves that are present in combustion. For illustration purpose, n-heptane is used in the evaporation and condensation analysis and HMX is used in the melting and freezing analysis of energetic materials of interest. On-going effort includes extension of this idea to include broad range of liquid and solid fuels, such as rocket propellants.

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