• Title/Summary/Keyword: Melt temperature

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Quality Characteristics of Mixed Polysaccharide Gels with Various Kiwifruit Contents (키위 첨가량에 따른 다당류 혼합겔의 품질 특성)

  • 윤혜신;오명숙
    • Korean journal of food and cookery science
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    • v.19 no.4
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    • pp.511-520
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    • 2003
  • This study was carried out to determine the effects of various contents of kiwifruit contents on the quality characteristics of mixed polysaccharide gels made from $\kappa$-carrageenan and locust bean gum. The color value, gelling temperature, melting temperature, break down rate, syneresis, rupture properties, TPA properties and sensory properties of mixed polysaccharide gels with various contents of kiwifruit contents were measured. As the kiwifruit contents was increased, the lightness (L), yellowness (b) and greenness (-a) of the mixed polysaccharide gels increased. There were no differences in the color values of gels during storage. As the kiwifruit content was increased, the gelling and melting temperatures of the mixed polysaccharide gels also increased. The mixed polysaccharide gels with high kiwifruit contents were difficult to melt, and it seemed that the addition of kiwifruit to the mixed polysaccharide gels could improve the thennal stability of the gels. The syneresis of the gel increased with increasing storage time, whereas the addition of kiwifruit to the gel resulted in suppression of syneresis. With regard to the rupture properties, stress, energy and strain, they were all decreased with increasing kiwifruit contents. The TPA properties, adhesiveness, hardness and chewiness increased and cohesiveness decreased with increasing kiwifruit contents. The results showed that the gel became tough and adhesive, and could be easily broken under small deformation, with increasing kiwifruit contents. The sensory evaluation showed that the green color, aroma, sweetness and sourness increased with increasing kiwifruit contents. The texture, adhesiveness, springiness and cohesiveness decreased, and brittleness and hardness increased, with increasing kiwifruit contents. The overall acceptability of the gel with 30% kiwifruit content was the highest. Thus, mixed polysaccharide gels made from kiwifruits could be useful, as the addition of kiwifruit to a mixed polysaccharide gel results in a good aroma, taste and stability, despite a lowering of the textural properties.

Foaming of Poly(butylene succinate) with Supercritical Carbon Dioxide (초임계 이산화탄소를 이용한 Poly(butylene succinate) 발포)

  • Son, Jae-Myoung;Song, Kwon-Bin;Kang, Byong-Wook;Lee, Kwang-Hee
    • Polymer(Korea)
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    • v.36 no.1
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    • pp.34-40
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    • 2012
  • The foaming of poly(butylene succinate) (PBS) using supercritical $CO_2(scCO_2)$ was studied. In order to improve the melt strength, PBS was modified using the reactive compounding technique. Rapid decompression of $scCO_2$-saturated PBS at a temperature above the depressed $T_m$ yielded expanded microcellular foams. The resulting foam structure could be controlled by manipulating process conditions. Experiments varying the foaming temperature while holding other variables constant showed that higher temperatures produced larger cells and reduced cell densities. Higher saturated pressures led to higher nucleation densities and smaller cell sizes. Decreasing the rate of depressurization permitted a longer period of cell growth and therefore larger cells were obtained.

Joining Foil-typed Pd-Cu Membranes to Collect CO2 Gas (이산화탄소 포집용 극박형 Pd-Cu 멤브레인 접합)

  • Rhewy, Gyung-Woo;Wee, So-Young;Kim, Gyeom;Lee, Chang-Ha;Baik, Il-Hyun;Park, Jin-Woo
    • Korean Journal of Metals and Materials
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    • v.48 no.12
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    • pp.1056-1063
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    • 2010
  • We present a new joining method for Pd-Cu membrane foils used as permeation tubes to collect $CO_2$. Since foils have poor mechanical strength, joining should be done at low temperatures to reduce residual stresses and without joining pressure. This contradicts the well known conditions for good contact between base materials that determines joint qualities. We selected Sn-Ag-Cu alloys that are highly reactive with Pd and Cu as a filler metal. As the filler melts at joining temperatures as low as $220{\sim}280^{\circ}C$, Pd and Cu are dissolved into the melt and react with the filler elements, which raises the melting temperature of the filler based on eutectic structures among the elements. Then, isothermal solidification progresses for the rest of the joining time. Intermetallic compounds (IMC) in the joints, one of the main factors for brittle joints, are inevitably formed. However, by optimizing both joining time and temperature, we balanced the wettability with IMC. Sealing test results confirmed that the joints are mechanically reliable during operation.

Evaluation of Granite Melting Technique for Deep Borehole Sealing (심부시추공 밀봉을 위한 화강암 용융거동 평가)

  • Lee, Minsoo;Lee, Jongyoul;Ji, Sung-Hoon
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.16 no.4
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    • pp.479-490
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    • 2018
  • The granite melting concept, which was suggested by Gibb's group for the closing of a deep borehole, was experimentally checked for KURT granite. The granite melting experiments were performed in two pressure conditions of atmospheric melting with certain inorganic additives and high pressure melting formed by water vaporization. The results of atmospheric tests showed that KURT granite started to melt at a lower temperature of $1,000^{\circ}C$ with NaOH addition and that needle shaped crystals were formed around partially melted crystals. In high pressure tests, vapor pressure was increased by adding water with maximum pressure of about 400 bars. KURT granite was partially melted at $1,000^{\circ}C$ when vapor pressure was low. However, it was not melted at vapor pressures higher than 200 bars. Therefore, it was determined that high pressure with a small amount of water vapor more effectively decreased the melting point of granite. Meanwhile, high temperature and high pressure vapor caused severe corrosion of the reactor wall.

Glacier Change in the Yigong Zangbo Basin, Tibetan Plateau, China

  • Ke, Chang-Qing;Lee, Hoonyol;Han, Yan-Fei
    • Korean Journal of Remote Sensing
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    • v.35 no.4
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    • pp.491-502
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    • 2019
  • Distinguishing debris-covered glaciers from debris-free glaciers is difficult when using only optical remote sensing images to extract glacier boundaries.According to the features that the surface temperature of debris-covered glacier is lower than surrounding objects, and higher than clean glaciers, glacial changes in the Yigong Zangbo basin was analyzed on the basis of visible, near-infrared and thermal-infrared band images of Landsat TM and OLI/TIRS in the support of ancillary digital elevation model (DEM). The results indicated that glacier area gradually declined from $928.76km^2$ in 1990 to $918.46km^2$ in 2000 and $901.51km^2$ in 2015. However, debris-covered glacier area showed a slight increase from $63.39km^2$ in 1990 to $66.24km^2$ in 2000 and $71.16km^2$ in 2015. During 25 years, the glacier length became shorter continuously with terminus elevation rising up. The area of moraine lakes in 1990 was $1.43km^2$, which increased to $1.98km^2$ in 2000 and $3.41km^2$ in 2015. In other words, the total area of the moraine lakes in 2015 is 2.38 times of that in 1990. This increase in moraine lake area could be the result of accelerated glacier melt and retreat, which is consistent with the significant warming trend in recent decades in the basin.

Characteristics of Heavy Metal Oxide Glasses in BaO-GeO2-La2O3-ZnO-Sb2O3 System for Infrared Lens (적외선 렌즈용 BaO-GeO2-La2O3-ZnO-Sb2O3계 중금속 산화물 유리의 특성)

  • Sang-Jin Park;Bok-Hyun Oh;Sang-Jin Lee
    • Korean Journal of Materials Research
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    • v.33 no.10
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    • pp.414-421
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    • 2023
  • Infrared radiation (IR) refers to the region of the electromagnetic radiation spectrum where wavelengths range from about 700 nm to 1 mm. Any object with a temperature above absolute zero (0 K) radiates in the infrared region, and a material that transmits radiant energy in the range of 0.74 to 1.4 um is referred to as a near-infrared optical material. Germanate-based glass is attracting attention as a glass material for infrared optical lenses because of its simple manufacturing process. With the recent development of the glass molding press (GMP) process, thermal imaging cameras using oxide-based infrared lenses can be easily mass-produced, expanding their uses. To improve the mechanical and optical properties of commercial materials consisting of ternary systems, germanate-based heavy metal oxide glasses were prepared using a melt-cooling method. The fabricated samples were evaluated for thermal, structural, and optical properties using DSC, XRD, and XRF, respectively. To derive a composition with high glass stability for lens applications, ZnO and Sb2O3 were substituted at 0, 1, 2, 3, and 4 mol%. The glass with 1 mol% added Sb2O3 was confirmed to have the optimal conditions, with an optical transmittance of 80 % or more, a glass transition temperature of 660 ℃, a refractive index of 1.810, and a Vickers hardness of 558. The possibility of its application as an alternative infrared lens material to existing commercial materials capable of GMP processing was confirmed.

Microstructure and EDM Processing of $MoSi_2$ Intermetallic Composite ($MoSi_2$ 금속간화합물 복합재료의 미세구조와 방전가공특성)

  • Yoon, Han-Ki;Lee, Sang-Pill;Yoon, Kyong-Wok;Kim, Dong-Hyun
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2002.05a
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    • pp.23-28
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    • 2002
  • This paper describes the machining characteristics of the $MoSi_2$ based composites by electric discharge drilling with various tubular electrodes, besides, Hardness characteristics and microstructures of $Nb/MoSi_2$ laminate composites were evaluated from the variation of fabricating conditions such as preparation temperature, applied pressure and pressure holding time. $MoSi_2$ -based composites has been developed in new materials for jet engine of supersonic-speed airplanes and gas turbine for high- temperature generator. Achieving this objective may require new hard materials with high strength and high temperature-resistance. However, With the exception of grinding, traditional machining methods are not applicable to these new materials. Electric discharge machining (EDM) is a thermal process that utilizes a spark discharge to melt a conductive material, the tool electrode being almost non-unloaded, because there is no direct contact between the tool electrode and the workpiece. By combining a nonconducting ceramics with more conducting ceramic it was possible to raise the electrical conductivity. From experimental results, it was found that the lamination from Nb sheet and $MoSi_2$ powder was an excellent strategy to improve hardness characteristics of monolithic $MoSi_2$. However, interfacial reaction products like (Nb, Mo)$SiO_2$ and $Nb_2Si_3$ formed at the interface of $Nb/MoSi_2$ and increased with fabricating temperature. $MoSi_2$ composites which a hole drilling was not possible by the conventional machining process, enhanced the capacity of ED-drilling by adding $NbSi_2$ relative to that of SiC or $ZrO_2$ reinforcements.

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Ferromagnetic Resonance Study of a Nanocrystalline $Fe_{76}Cu_{1}Nb_{3}Si_{14}B_{6}$ Alloy (초미세결정합금 $Fe_{76}Cu_{1}Nb_{3}Si_{14}B_{6}$의 강자성공명 연구)

  • 이수형;김원태;장평우;김약연;임우영
    • Journal of the Korean Magnetics Society
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    • v.4 no.1
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    • pp.7-11
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    • 1994
  • Ferromagnetic resonance experiment was performed to study the variations of micromagnetic structure with heat treatment of melt spun $Fe_{76}Cu_{1}Nb_{3}Si_{14}B_{6}$ alloy for 1h at every $50^{\circ}C$ in the temperature range of $400^{\circ}C-700^{\circ}C$. The variations of micromagnetic structure was discussed qualitatively in terms of the variations of line width ${\Delta}H_{p-p}$ and resonance magnetic field $H_{res}$. With increasing armealing temperature to $400^{\circ}C$, ${\Delta}H_{p-p}$ decreases and $H_{res}$ increases due to the decrease in magnetic anisotropy resulting from structural relaxation during heat treatment. With increasing annealing temperature from 400 to $500^{\circ}C$, ${\Delta}H_{p-p}$ increases and $H_{res}$ decreases due to the increase in magnetic anisotropy resulting from the formation of nanocrystalline particles embedded in an amorphous matrix. With increasing armealing temperature from 500 to $550^{\circ}C$, ${\Delta}H_{p-p}$ decreases and $H_{res}$ increases due to the decrease in magnetic anisotropy resulting from the formation of homogeneous nanocrystalline structure with a minor amorphous phase. Further increase in armealing temperature above $550^{\circ}C$ C causes ${\Delta}H_{p-p}$ to increase and $H_{res}$ to decrease due to the increase in magnetic anisotropy due to the formation of inhomogeneous grain structure and intermetallic compounds.

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Process design for solution growth of SiC single crystal based on multiphysics modeling (다중물리 유한요소해석에 의한 SiC 단결정의 용액성장 공정 설계)

  • Yoon, Ji-Young;Lee, Myung-Hyun;Seo, Won-Seon;Shul, Yong-Gun;Jeong, Seong-Min
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.26 no.1
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    • pp.8-13
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    • 2016
  • A top-seeded solution growth (TSSG) is a method of growing SiC single crystal from the Si melt dissolved the carbon. In this study, multiphysics modeling was conducted using COMSOL Multiphysics, a commercialized finite element analysis package, to get analytic results about electromagnetic analysis, heat transfer and fluid flow in the Si melt. Experimental results showed good agreements with simulation data, which supports the validity of the simulation model. Based on the understanding about solution growth of SiC and our set-up, crystal growth was conducted on off-axis 4H-SiC seed crystal in the temperature range of $1600{\sim}1800^{\circ}C$. The grown layer showed good crystal quality confirmed with optical microscopy and high resolution X-ray diffraction, which also demonstrates the effectiveness of the multiphysics model to find a process condition of solution growth of SiC single crystal.

Study on Analysis Technique Comparison and Evaluation of High Thermal Conductivity Concrete with Magnetite Aggregates and Steel Powder (자철광 및 철분말을 혼입한 고열전도 콘크리트의 열전도 평가 및 해석기법 비교에 대한 연구)

  • Lee, Hack-Soo;Kim, Min-Kyu;Kwon, Seung-Jun
    • Journal of the Korea Concrete Institute
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    • v.26 no.3
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    • pp.315-321
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    • 2014
  • Concrete as a construction material is widely used in nuclear vessel and plant for excellent radiation shielding. However the isolation characteristics in concrete may affect adversely in the case of fire and melt-down in nuclear vessel since temperature cooling down is very difficult from outside. This study is for development of high thermal conductive concrete, and its mechanical and thermal properties are evaluated. Magnetite aggregates with volume ratio of 42.3% (maximum) and steel powder of 1.5% are replaced with normal aggregates and thermal properties are evaluated. Thermal conductivity little increases by 30% addition of magnetite but rapidly increases afterwards. Finally thermal conductivity is magnified to 2.5 times in the case of 42.3% addition of magnetite. Steel powder has a positive effect on high thermal conduction to 106~113%. Several models for thermal conduction like ACI, DEMM, and MEM are compared with test results and they are verified to reasonably predict the thermal conductivity with increasing addition of magnetite aggregates and steel powder.