• Title/Summary/Keyword: Mechanical testing

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Development of Pilot-Scale Manufacturing Process of SiC Fiber from Polycarbosilane Precursor with Excellent Mechanical Property at Highly Oxidation Condition and High Temperature (폴리카보실란 전구체로부터 고온 산화성분위기서 기계적물성이 우수한 파이롯-규모의 탄화규소섬유 제조공정 개발)

  • Yoon, B.I.;Choi, W.C.;Kim, J.I.;Kim, J.S.;Kang, H.G.;Kim, M.J.
    • Composites Research
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    • v.30 no.2
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    • pp.116-125
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    • 2017
  • The purpose of this study is to develop silicon carbide fiber showing an excellent mechanical properties under highly oxidative conditions at high temperature. Polycarbosilane(PCS) as a preceramic precursor was used for making the SiC fiber. PCS fiber was taken by melt spinning method followed by melting the PCS at $300{\sim}350^{\circ}C$ in N2 gas. The Curing of PCS fiber was carried out in air oxygen chamber, prior to high temperature pyrolysis. Degree of cure was calculated by characteristic peak's ratio of Si-H to $Si-CH_3$ in FT-IR spectra before and after curing of PCS fiber. The properties of SiC fiber was affected greatly by the degree of cure. The SiC fiber produced by controlling fiber tension during heat treatment showed good properties. The SiC fiber exposed to $1000^{\circ}C$ at air from 1 min. up to maximum 50 hrs showed around 60% reduction in tensile strength. We found that large amount of carbon content on the fiber surface after long-term exposure has resulted in lower tensile strength.

A Fundamental Study of Ferro Copper Slag for Concrete Aggregate (동슬래그의 콘크리트용 골재 활용에 관한 기본연구)

  • Song, Tae-Hyeob;Lee, Mun-Hwan;Lee, Sea-Hyun
    • Journal of the Korea Concrete Institute
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    • v.15 no.1
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    • pp.35-42
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    • 2003
  • To use ferro copper slag as aggregate in the construction, an evaluation upon the two kinds of ferro copper slag being produced was conducted to determine the basic physical, and mechanical properties, chemical component and environmental noxiousness. As a result of experiment, it was found that two kinds of ferro copper slag satisfies the physical and mechanical properties of aggregate, prescribed in KS F 2526, and that in the result of noxious heavy metal eruption test by single bach extraction, no eruption of noxious heavy metal was detected or the eruption was far below the reference value. And mortar test was conducted by replacing sand of 25, 50, 75, 100% and the performance level was presented upon reviewing the fluidity property and variable aspects of unit weight. The increase of strength in accordance with replacement rate of sand was found to be the below than the equivalent level compared to the testing specimens that did not use ferro copper slag, but those of 25% replacement rate was above than 0%. Thus, two kinds of ferro copper slag, produced in the domestic, were found to be possessing the enough physical properties to use as concrete aggregate assuming that used with sand and in particular, it was reviewed to be advantageous in manufacturing concrete or mortar that requires weight.

Synthesis of Aliphatic Ester-Carbonate Copolymer (지방족 에스터-카보네이트 공중합체의 합성)

  • Kim, Dong-Kook;Kim, Ki-Seab;Chang, Young-Wook
    • Applied Chemistry for Engineering
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    • v.7 no.5
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    • pp.970-976
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    • 1996
  • An ester-carbonate copolymer was synthesized, in which carbonate was inserted into a biodegradable aliphatic polyester, poly(butylene succinate) (PBS), to modify its mechanical properties. The synthesis was carried out by condensation reactions in two steps. In the first step, oligo(butylene succinate) was prepared by the reaction of succinic acid with 1,4-butanediol (BD). In the second step, it was reacted with oligohexamethylenecarbonate diol (OHMCG) to prepare the ester-carbonate copolymer. Titanium(IV) isopropoxide (TIP) was used as a catalyst for the reaction. The structure of the copolymer was confirmed by FT-IR and $^1H$-NMR and the thermal behavior and mechanical properties were investigated by differential scanning calorimetry (DSC) and universal testing machine (UTM), respectively. It was found that optimum amount of the catalyst for the formation of high molecular weight copolymer was 1wt% for succinic acid. When the BD:OHMCG is in the range 149:1~249:1, the copolymer with high viscosity was obtained. As the OHMCG content was increased, melting temperature ($T_m$) of the copolymer was decreased. When BD:OHMCG is 149:1, the copolymer showed a increase in ultimate strain by two times and the slight decrease in modulus compared to those of PBS.

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A Study on Design Automation of Cooling Channels in Hot Form Press Die Based on CATIA CAD System (CATIA CAD 시스템 기반 핫폼금형의 냉각수로 설계 자동화에 관한 연구)

  • Kim, Gang-Yeon;Park, Si-Hwan;Kim, Sang-Kwon;Park, Doo-Seob
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.3
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    • pp.147-154
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    • 2018
  • This paper focuses on the development of a support system that can rapidly generate the design data of a hot-form die with cooling channels, commonly known as hot stamping technology. We propose a new process for designing hot-form dies based on our (automated) system, whose main features are derived from the analysis of the design requirements and design process in the current industry. Our design support system consists of two modules, which allow for the generation of a 3D geometry model and its 2D drawings. The module for 3D modeling automation is implemented as a type of CATIA template model based on CATIA V5 Knowledgeware. This module automatically creates a 3D model of a hot-form die, including the cooling channels, that depends on the shape of the forming surface and the number of STEELs (subsets of die product) and cooling channels. It also allows for both the editing of the positions and orientations of the cooling channels and testing for the purpose of satisfying the constraints on the distance between the forming surface and cooling channels. Another module for the auto-generation of the 2D drawings is being developed as a plug-in using CAA (CATIA SDK) and Visual C++. Our system was evaluated using the S/W test based on a user defined scenario. As a result, it was shown that it can generate a 3D model of a hot form die and its 2D drawings with hole tables about 29 times faster than the conventional manual method without any design errors.

Mechanical Properties of Carbon Fiber/Si/SiC and Carbon Fiber/C/SiC Composites (탄소섬유/Si/SiC 및 탄소섬유/탄소/SiC 복합재의 기계적 물성)

  • 신동우;박삼식;김경도;오세민
    • Composites Research
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    • v.12 no.3
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    • pp.8-16
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    • 1999
  • Carbon woven fabric/C/SiC composites were fabricated by multiple impregnations of carbon woven fabric/carbon preform with the polymer precursor of SiC, i.e., polycarbosilane. In addition, two kinds of low density carbon/carbon preforms which had different fiber volume fraction and fiber orientation, i.e., a carbon woven fabric(${\thickapprox}$55 vol%)/carbon and a chopped carbon fiber${\thickapprox}$40 vol%)/carbon composites, were reaction-bonded with a silicon melt at 1$700^{\circ}C$ in a vacuum to fabricate dense carbon fiber/Si/SiC composites. The reaction-bonding process increased the density to ~2.1 g/$cm^3$ from 1.6 g/$cm^3$ and 1.15 g/$cm^3$ of a carbon woven and a chopped carbon preforms, respectively. All of the composites fractured with extensive fiber pull-out. The higher the density the higher the stiffness and proportional limit stress. The mechanical properties obtained from a three-point bend and tension tests were compared. The ratios of the peak tensile stresses to the bending strengths of a carbon woven and a chopped carbon composites were about one-third, respectively. The carbon woven fabric/Si/SiC composites with density of 2.06 g/$cm^3$ showed ~120 MPa of ultimate strength and ~80 MPa of proportional limit in bend testing.

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An Analysis of Running Stability of 1/5 Small Scaled Bogie on Small-Scaled Derailment Simulator (소형탈선시뮬레이터상에서의 1/5 축소대차 주행안정성 해석)

  • Eom, Beom-Gyu;Kang, Bu-Byoung;Lee, Hi-Sung;Song, Moon-Shuk
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.36 no.11
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    • pp.1413-1420
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    • 2012
  • To predict the dynamics behavior, running stability, etc. of a railway vehicle and to understand its physical characteristics, analytical methods are used for the testing and manufacturing of a scale model along with numerical simulations in developed countries (England, France, Japan, etc.). The test of the dynamics characteristics of full-scale models is problematic in that it is expensive and time-consuming because an entire large-scale test plant needs to be constructed, difficulties are involved in the test configuration, etc. To overcome these problems, an analytical study involving dynamics tests and computer simulations using a scaled bogie model that applies the laws of similarity was carried out. In this study, we performed stability analysis on a 1/5 small scaled bogie for parameters such as the running speed and carbody weight by using an analysis model. Furthermore, we verified the reliability by using a small-scaled derailment simulator and examined the dynamic characteristic of the 1/5 small scaled bogie.

An efficient approach for model updating of a large-scale cable-stayed bridge using ambient vibration measurements combined with a hybrid metaheuristic search algorithm

  • Hoa, Tran N.;Khatir, S.;De Roeck, G.;Long, Nguyen N.;Thanh, Bui T.;Wahab, M. Abdel
    • Smart Structures and Systems
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    • v.25 no.4
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    • pp.487-499
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    • 2020
  • This paper proposes a novel approach to model updating for a large-scale cable-stayed bridge based on ambient vibration tests coupled with a hybrid metaheuristic search algorithm. Vibration measurements are carried out under excitation sources of passing vehicles and wind. Based on the measured structural dynamic characteristics, a finite element (FE) model is updated. For long-span bridges, ambient vibration test (AVT) is the most effective vibration testing technique because ambient excitation is freely available, whereas a forced vibration test (FVT) requires considerable efforts to install actuators such as shakers to produce measurable responses. Particle swarm optimization (PSO) is a famous metaheuristic algorithm applied successfully in numerous fields over the last decades. However, PSO has big drawbacks that may decrease its efficiency in tackling the optimization problems. A possible drawback of PSO is premature convergence leading to low convergence level, particularly in complicated multi-peak search issues. On the other hand, PSO not only depends crucially on the quality of initial populations, but also it is impossible to improve the quality of new generations. If the positions of initial particles are far from the global best, it may be difficult to seek the best solution. To overcome the drawbacks of PSO, we propose a hybrid algorithm combining GA with an improved PSO (HGAIPSO). Two striking characteristics of HGAIPSO are briefly described as follows: (1) because of possessing crossover and mutation operators, GA is applied to generate the initial elite populations and (2) those populations are then employed to seek the best solution based on the global search capacity of IPSO that can tackle the problem of premature convergence of PSO. The results show that HGAIPSO not only identifies uncertain parameters of the considered bridge accurately, but also outperforms than PSO, improved PSO (IPSO), and a combination of GA and PSO (HGAPSO) in terms of convergence level and accuracy.

The development of the Ionizer using clean room (청정환경용 정전기 제거장치 개발)

  • Jeong, Jong-Hyeog;Woo, Dong Sik
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.1
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    • pp.603-608
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    • 2018
  • Although the voltage-applied discharge method is most widely used in the semiconductor and display industries, periodic management costs are incurred because the method causes defects due to the absorption of ambient fine dust and causes emitter tip contamination due to the discharge. The emitter tip contamination problem is caused by the accumulation of fine particles in ambient air due to the corona discharge of the ionizer. Fuzzy ball generation accelerates the wear of the emitter tip and deteriorates the performance of the ionizer. Although a mechanical cleaning method using a manual brush or an automatic brush is effective for contaminant removal, it requires management of additional mechanical parts by the user. In some cases, contaminants accumulated in the emitter may be transferred to the wafer or product. In order to solve this problem, we developed an ionizer for a clean environment that can remove the pencil-type emitter tip and directly ionize the surrounding gas molecules using the tungsten wire located inside the ion tank. As a result of testing and certification by the Korea Institute of Machinery and Materials, the average concentration was $0.7572particles/ft^3$, the decay time was less than two seconds, and the ion valance was 7.6 V, which is satisfactory.

A Study for Optimization of Armed Flight Test Ammunition Requirement for the Development of Attack Helicopter (공격헬기 개발을 위한 무장 비행시험 탄약발수 최적화 연구)

  • Lee, Myeong-Seok;Hur, Jang-Wook
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.8
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    • pp.147-153
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    • 2020
  • Developments in aircraft require safety verification through flight testing for many hours with prototype design and production. The test evaluation step of performing flight tests was an important process that determines the success in the development of the system. In particular, safety development through flight tests in the armed flight test is important for the development of attack helicopters. In the development of attack helicopters, the evaluation period and cost related to the armed flight test are closely related to the required ammunition requirement. Therefore, this paper presents the amount of ammunition required for the military flight test between attack helicopter developments through an analysis of the AH-1 helicopter in a similar case and ADS-44-HDBK of military specification. The AH-1 can be used to calculate the ammunition demand by considering the exclusion of redundant firing tests and configuration differences. In the case of the machine gun-equipped configuration, approximately 10,500R was required, and approximately 324R was required in the case of a rocket-mounted configuration. In addition, if the armed integrated bench is used properly, it is expected to promote efficiently the flight test in the armed flight by identifying the possible risk factors with armed flight tests and excluding them.

Effects on Bond Strength between Zirconia and Porcelain according to Etching Treatment and Low Temperature Degradation (지르코니아 표면에칭처리와 저온열화현상이 지르코니아와 전장도재의 결합강도에 미치는 영향)

  • Park, Jin-Young;Kim, Jae-Hong;Kim, Woong-Chul;Kim, Ji-Hwan;Kim, Hae-Young
    • Journal of dental hygiene science
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    • v.14 no.2
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    • pp.140-149
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    • 2014
  • The purpose of this study was to investigate the influence of etching surface treatment and aging treatment of zirconia on the shear bond strength between zirconia core and veneered ceramic. Four groups of zirconia-ceramic specimens were prepared; 1) NEZ group (no etching zirconia), 2) EZ group (etching zirconia), 3) ANEZ group (aging and no etching zirconia), 4) AEZ group (aging and etching zirconia). The shear bond strength between zirconia and porcelain was measured using Instron Universal Testing Machine. Surface texture with crystalline structure of zirconia surface was examined by the field emission scanning electron microscopy (FE-SEM) with ingredient analysis. The fractured surfaces of specimens were examined to determine the failure pattern by a digital microscope. The mean${\pm}$standard deviation of shear bond strengths were $23.47{\pm}3.47$ Mpa in NEZ, $28.30{\pm}4.34$ Mpa in EZ, $21.85{\pm}4.65$ Mpa in ANEZ, $24.65{\pm}3.65$ Mpa in AEZ group, respectively, and were significantly different (p<0.05). The average shear bond strength was largest in EZ group, followed by AEZ, NEZ, and ANEZ groups. Most specimens in NEZ group showed adhesive failure and most specimens in EZ, AEZ, and ANEZ group showed mixed failure. Surface of etching treatment group (EZ and AEZ) showed complex micro-structure and irregular surface texture which may facilitate mechanical interlocking, while untreated zirconia surface presented simpler micro-structure. In conclusion, an etching treatment improved bonding strength between zirconia and porcelain by forming mechanical interlocking.