• 한국항공우주학회지
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• 제31권9호
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• pp.32-37
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• 2003

소형화의 추세는 마이크로 로켓의 연구에도 적용되어 MEMS 공정으로 제작된 마이크로 로켓들이 시도되었다. 본 논문에서는 마이크로 밀링을 사용한 3차원 마이크로 로켓의 제작과 연소 및 발사시험의 결과를 다루고자 한다. 로켓의 동체는 알루미늄 6061 합금을 사용하였다. 3차원 마이크로 노즐은 황동을 직경 127${\mu}m$의 마이크로 엔드밀로 절삭하여 가공되었다. 두 가지 크기의 노즐이 제작되었는데 하나는 노즐목의 직경이 1mm이고 다른 하나는 0.5mm이다. 로켓의 질량은 7.32g이고 추진제의 질량은 0.65g이었다. 추력 대 무게비는 1.58에서 1.74로 계산되며 지면에서 45도 각도로 발사된 비행시험결과 약 46m~53m의 수평거리를 비행하였다.

• 한국분말재료학회지
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• 제20권4호
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• pp.269-274
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• 2013

The present work investigated the dispersion behavior of $Y_2O_3$ particles into AISI 316L SS manufactured using laser cladding technology. The starting particles were produced by high energy ball milling in 10 min for prealloying, which has a trapping effect and homogeneous dispersion of $Y_2O_3$ particles, followed by laser cladding using $CO_2$ laser source. The phase and crystal structures of the cladded alloys were examined by XRD, and the cross section was characterized using SEM. The detailed microstructure was also studied through FE-TEM. The results clearly indicated that as the amount of $Y_2O_3$ increased, micro-sized defects consisted of coarse $Y_2O_3$ were increased. It was also revealed that homogeneously distributed spherical precipitates were amorphous silicon oxides containing yttrium. This study represents much to a new technology for the manufacture and maintenance of ODS alloys.

• 한국자기학회지
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• 제14권5호
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• pp.174-179
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• 2004

고주파 회로에서 발생하는 전도 노이즈의 흡수율을 측정하는 방안의 하나로 50 $\Omega$ 특성 임피던스의 마이크로스트립 선로를 제작하고, 순철 압분체로 구성되는 자기손실재의 전력 흡수율 측정을 통하여 측정 및 해석 방법의 타당성을 제시하였다 제작된 마이크로스트립 선로는 S$_{11}$ < -60 dB, S$_{21}$=0 dB의 반사/투과 특성을 보여 전도 노이즈 흡수율 측정에 이상적인 전송특성을 보였다. Attrition milling에 의해 순철 압분체를 제작하고, 이를 고무와 혼합하여 두께 1mm정도의 복합재 sheet를 제작하였다. 이 재료를 마이크로스트립 선로에 장착한 결과 2～8 GHz대역에서 전력흡수율이 80% 이상인 대역저지 필터와 유사한 특성을 얻을 수 있었다. 주파수, 흡수 sheet 크기에 따른 노이즈 흡수율에 관한 분석을 통하여, 노이즈 흡수율에 주된 영향을 주는 인자는 자기손실임을 제안하였다.

• 한국재료학회지
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• 제12권8호
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• pp.600-607
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• 2002

The Ni-Zn synthetic ferrite were acquired from thermally decomposing the metal nitrates Fe(NO$_3$)$_3$.$9H_2$O, Zn($NO_3$)$_2$.$6H_2$O, Ni($NO_3$)$_2$. $6H_2$O, and Cu($NO_3$)$_2$. $3H_2$O at $150^{\circ}C$ for 24 hours and was calcined at $500^{\circ}C$. Each of those was pulverized for 3, 6, 9, and 12 hours in a steel ball mill and was sintered between $700^{\circ}C$ and $1,000^{\circ}C$ for 1 hour, and then their microstructures and electromagnetic properties were examined. We could make the initial specimens chemically bonded in liquid at the temperature as low as $150^{\circ}C$, by using the melting points less than $200^{\circ}C$ of the metal nitrates instead of the mechanical ball milling, then narrowed a distance between the particles into a molecular level, and thus lowed sintering temperature by at least $200^{\circ}C$ to$ 300^{\circ}C$. Their initial permeability was 50 to 400 and their saturation magnetic induction density and coercive force 2,400 G and 0.3 Oe to 0.5 Oe each, which were similar to those of Ni- Zn ferrite synthesized in the conventional process. In the graph of initial permeability vs frequencies, we could observe a $180^{\circ}C$rotation of the magnetic domain, which appears in a broad band of microwave near the resonance frequency.

• Journal of Electrochemical Science and Technology
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• 제4권3호
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• pp.113-118
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• 2013

Fluorophosphate, $Na_2MnPO_4F$ as new cathode material was synthesized by carbothermal treatment method. Prepared $Na_2MnPO_4F$ has particle size under 100 nm and residual carbon exists in surface of $Na_2MnPO_4F$. Additional carbon coating was performed in order to increase the electrochemical properties. Even capacity and overpotential were improved by carbon coating using mechanical ball milling, the reduced crystallinity limited the drastic improvement of the electrochemical properties. To solve this problem, re-heat treatment was involved to recover crystallinity and then notable improvement of electrochemical properties was obtained. Specific amount of $Li^+$ that participates in electrochemical $Li^+$ insertion / extraction reaction, was x = 1 in $Li_xNa_{2-x}MnPO_4F$ within the voltage range of 2.0 to 4.8 V. The doubled capacity by 2 electron reaction can be obtained when NMPF is charged to higher voltage over 4.8 V.

• Composites Research
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• 제29권6호
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• pp.353-357
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• 2016

B-stage 레진 필름에 탄소나노튜브(CNT) 등을 균일하게 분포시킨 뒤에 기타의 보강섬유 층과 함께 여러 겹으로 적층하여 하이브리드 형태의 복합재료를 만드는 방법은 유용하다. 본 연구에서는 CNT가 포함된 에폭시 레진으로부터 shear mixing 및 Three-roll mill 공정을 이용하여 B-stage 레진 필름을 제작하였다. 두 공정을 통해 형성된 CNT/레진 복합재 필름의분산도를 파단면의 SEM 관찰을통해분석하였다. 보다 효율적인 공정을 위해 Calendering pass 횟수에 따른 분산도를 평가하였다. Pass의 횟수에 따른 샘플을 제조하고 CNT 분산도는 SEM 이미지를 통해 확인하고, 전기 전도도 측정을 통해 분석하였다. 추가적으로 gap mode, force mode를 통해 제작한 각각의 샘플의 전기 전도도를 측정하여 CNT 분산도를 분석하였고 이를 통해 최적공정을 도출하였다.

• 한국정밀공학회지
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• 제32권5호
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• pp.431-439
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• 2015

One of common challenges in designing modern production machines is realizing high speed motion without sacrificing accuracy. To address this challenge it is necessary to maximize the stiffness of the mechanical structure and the control system with consideration on the main disturbance input, cutting forces. This paper presents analysis technologies for realizing high stiffness in production machines. First, CAE analysis techniques to evaluate the dynamic stiffness of a machine structure and a new method to construct the physical machine model for servo controller simulations are demonstrated. Second, cutting forces generated in milling processes are analyzed to evaluate their effects on the mechatronics system. In the effort to investigate the interaction among the structure, controller, and process, a flexible multi-body dynamics simulation method is implemented on a magnetic bearing stage as an example. The presented technologies can provide better understandings on the mechatronics system and help realizing high stiffness production machines.

• Korea-Australia Rheology Journal
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• 제14권3호
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• pp.107-114
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• 2002

Residual stress distribution in injection molded short fiber composites is determined by using the layer-removal method. Polystyrene is mixed with carbon fibers of 3% volume fraction (4.5% weight fraction) in an extruder and the tensile specimen is injection-molded. The layer-removal process, in which removing successive thin uniform layers of the material from the surface of the specimen by a milling machine, is employed and the resulting curvature is acquired by means of an image processing. The isotropic elastic analysis proposed by Treuting and Read which assumes a constant Yaung’s modulus in the thickness direction is one of the most frequently used methods to determine residual stresses. However, injection molded short fiber composites experience complex fiber orientation during molding and variation of Yaung’s modulus distribution occurs in the specimen. In this study, variation of Yaung’s modulus with respect to the thickness direction is considered for calculation of the residual stresses as proposed by White and the result is compared with that by assuming constant modulus. Residual stress distribution obtained from this study shows a typical stress profile of injection-molded products as reported in many literatures. Young’s modulus distribution is predicted by using numerical methods instead of experimental results. For the numerical analysis of injection molding process, a hybrid FEM/FDM method is used in order to predict velocity, temperature field, fiber orientation, and resulting mechanical properties of the specimen at the end of molding.

• 한국미생물·생명공학회지
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• 제18권3호
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• pp.260-267
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• 1990

분쇄마찰매체 함유 효소반응계에서 순수분리된 glucoamylase 또는 $\alpha$-amylase에 의한 옥수수 생전분의 효소당화 mechanism을 규명코자, 생성된 당조성, SEM을 이용한 전분입자의 구조, 효소흡착량 그리고 amylose 함량 등의 변화를 관찰하였다. 생성당 조성은 분쇄마찰매체 효소반응계에서도 큰 변화없이 glucoamylase의 경우 반응초기부터 glucose가 주로 생성되었고, $\alpha$-amylase의 경우에는 maltopentaose (G5)를 포함한 oligosaccharide(G2-G8)가 주고 생성되었고 약간의 glucose가 포함되었으며, 당조성은 경시적으로 크게 변하지 않았다. SEM으로 전분입자의 구조를 관찰한 결과, 효소를 첨가하지 않을 경우 분쇄마찰매체의 기계적 충격은 전분입자의 구조변화에 큰 영향을 미치지는 못하였고 다만 전분입자를 균열시켰다.

• 한국분말재료학회지
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• 제20권6호
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• pp.474-478
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• 2013

The most general photocatalyst, $TiO_2$ and $WO_3$, are acknowledged to be ineffective in range of visible light. Therefore, many efforts have been directed at improving their activity such as: band-gap narrowing with non-metal element doping and making composites with high specific surface area to effectively separate electrons and holes. In this paper, the method was introduced to prepare a photo-active catalyst to visible irradiation by making a mixture with $TiO_2$ and $WO_3$. In the $TiO_2-WO_3$ composite, $WO_3$ absorbs visible light creating excited electrons and holes while some of the excited electrons move to $TiO_2$ and the holes remain in $WO_3$. This charge separation reduces electron-hole recombination resulting in an enhancement of photocatalytic activity. Added Ag plays the role of electron acceptor, retarding the recombination rate of excited electrons and holes. In making a mixture of $TiO_2-WO_3$ composite, the mixing route affects the photocatalytic activity. The planetary ball-mill method is more effective than magnetic stirring route, owing to a more effective dispersion of aggregated powders. The volume ratio of $TiO_2(4)$ and $WO_3(6)$ shows the most effective photocatalytic activity in the range of visible light in the view point of effective separation of electrons and holes.