• Title/Summary/Keyword: Mechanical ball milling

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Improvement in Microstructure Homogeneity of Sintered Compacts through Powder Treatments and Alloy Designs

  • Hwang, K.S.;Wu, M.W.;Yen, F.C.;Sun, C.C.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.824-825
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    • 2006
  • Homogeneous microstructures of the PM compacts are difficult to attain when mixed elemental powders are used. This study examined the microstructures of pressed-and-sintered and MIM products that contain Ni and Mo.Ni-rich areas, which were lean in carbon and were soft and were found easily in regular specimens. Gaps or cracks near the Ni-rich or Mo-rich areas were also frequently observed. This problem worsened when Ni and Mo particles were large and were irregular in shape. By using ball milling treatment and ferroalloy powders, the microstructure homogeneity and mechanical properties were improved. The addition of 0.5wt%Cr further improved the distribution of Ni because Cr reduced the repulsion effect between nickel and carbon. With the elimination of Ni-rich areas, more bainites and martensites were formed and mechanical properties were significantly improved.

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Off-line Control of Machining Error in a Flexible Ball End Milling System (유연 볼 엔드밀에 의한 가공오차의 Off-line 제어)

  • 심충건;양민양
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.16 no.3
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    • pp.468-484
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    • 1992
  • 본 연구에서는 기존의 유연 볼 엔드밀의 절삭력 모델을 바탕으로 자유 곡면의 정삭 가공에서 발생할 수 있는 과대 또는 과소 절삭을 방지하면서 그 가공의 효율성을 높이기 위한 볼 엔드밀의 이송 속도 결정법을 제시하고자 한다. 먼저, 자유 곡면의 가공에서 발생될 수 있는 공구의 처짐에 따른 가공오차에 대하여 볼 엔드밀 공구의 처 짐벡터와 공작물의 공구 접촉점에서의 법선벡터로 표현되는 가공오차(machining error ) 예측 모델식을 유도하였다. 본 가공오차 예측 모델식은 다시 절삭날당 가지는 이 송량의 함수로 전개되어 그 곡면의 주어진 가공 공차(machining tolerance)를 만족시 키는 이송속도를 결정하게 된다.

Analysis of the Characteristic Lines on Geometrical Texture by Ball end Milling (볼엔드밀 가공면의 기하학적 특징선 해석)

  • Jung, Tae-Sung;Choi, In-Hugh;Yang, Min-Yang
    • Proceedings of the KSME Conference
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    • 2003.04a
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    • pp.1148-1153
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    • 2003
  • An adequate method for the prediction of machining errors is essential to improve productivity and product quality. But it is known that there is a remarkable difference between values calculated by conventional roughness model and measured values of actual machined surfaces under high efficient cutting condition. This paper introduces the theoretical analysis of characteristic lines of cut remainder to evaluate a geometrical surface roughness accurately. In this study, analytic equations of the characteristic lines are derived from the surface generation mechanism of ball end milling considering the actual trochoidal trajectories of cutting edges. The predicted results are compared with the results of conventional roughness model.

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Fabrication of $TiH_2$ Powders from Titanium Tuning Chip by Mechanical Milling

  • Jang, Jin-Man;Lee, Won-Sik;Ko, Se-Hyun
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.969-970
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    • 2006
  • In present work, manufacturing technologies of titanium hydride powder were studied for recycling of titanium tuning chip and for this, attrition ball milling was carried out under $H_2$ pressure of 0.5 MPa. Ti chips were completely transformed into $TiH_2$ within several hundred seconds. Dehydrogenation process $TiH_2$ powders is consist of two reactions: one is reaction of $TiH_2$ to $TiH_x$ and the other decomposition of $TiH_x$ to Ti and $H_2$. The former reaction shows relatively low activation energy and it is suggested that the reaction is caused by introduction of defects due to milling.

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Fabrication Process and Mechanical Properties of Co-based Metal Bond in Diamond Impregnated Tools (다이아몬드 공구용 코발트계 합금 결합제의 제조 및 기계적 성질)

  • Lee, Gi-Seon;Jeong, Seung-Bu
    • Korean Journal of Materials Research
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    • v.10 no.8
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    • pp.532-539
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    • 2000
  • Co-0.5C-(15~20)Cr-20Ni-8W-(2~7)Fe alloy bond in diamond-impregnated abrasive tool was synthesized by ball-milling and mechanical alloying process. When the powders were mechanical alloyed for 6h, micro-welding in most metal powders was observed irrespective of addition of stearic acid. Without stearic acid in metal powders, partial-ly coarse powders were obtained, which could be unfaverable to the densification of composite of composite powders. The hot-pressed compacts showed rupture strength of 1100MPa and hardness of about $46H_{RC}$, respectively.

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Development of molybdenum silicides for hydrogen fueled combustion turbine by mechanical alloying (기계적 합금화에 의한 수소연소 터어빈용 Mo-Si계 금속간화합물의 개발에 관한 연구)

  • 이충효
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.7 no.4
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    • pp.665-672
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    • 1997
  • We applied mechanical alloying process by ball milling to produce molybdenum silicides $MoSi_2$ and $Mo_5Si_3$ using a mixture of elemental molybdenum and silicon powders at room temperature. The intermetallic compound MoSi$_3$ have been obtained by ball milling of $Mo_{33}Si_{67}$ mixture powders for 100 h, which is transformed to single $MoSi_2$ phase by subsequent heat treatment up to $725^{\circ}C$. The grain size of the $MoSi_2$ powders thus obtained was 19 nm, being approximately four times smaller than that of the commercial alloy. The intermetallic compound $MoSi_2$ with grain size of 30 nm have been also obtained by ball milling of $Mo_{62}Si_{38}$ mixture powders for 500 h, which is transformed to single $MoSi_2$ phase by heating up to $1000^{\circ}C$. We believe that the retarded ball milling time for the formation of $MoSi_2$ phase is attributed to its complicated crystal structure and large unit cell. The finer grain size in the ball-milled molybdenum silicides powders is expected to improve room-temperature mechanical properties for high-temperature structural materials.

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Mechanical Milling of Lithium with Metal Oxide and its Reactivity with Gases

  • Yokoi, Tomomichi;Yamasue, Eiji;Okumura, Hideyuki;Ishihara, Keiichi N.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.959-960
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    • 2006
  • Li reacts with $N_2$ at room temperature. In order to activate Li, the mechanical milling of Li with stable metal oxide, namely, $Al_2O_3$ and MgO, using a high energy vibrating ball mill was performed. In the case of Li-MgO system, it reacts with $N_2$, but hardly reacts with $O_2$. The reaction with $N_2$ generally produces $Li_3N$, while for some vigorous reactions the $Mg_3N_2$ is produced as the major phases. In the case of $Li-Al_2O_3$ system, reactivities with both $N_2$ and $O_2$ are high. The difference is explained in terms of the reaction mechanism and the Li state.

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Method and mechanism of dispersing agent free dispersion of short carbon fibers in silicon carbide powder

  • Raunija, Thakur Sudesh Kumar;Mathew, Mariamma;Sharma, Sharad Chandra
    • Carbon letters
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    • v.15 no.3
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    • pp.180-186
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    • 2014
  • This study highlights a novel method and mechanism for the rapid and effective milling of carbon fibers (CFs) in silicon carbide (SiC) powder, and also the dispersion of CFs in SiC powder. The composite powders were prepared by chopping and exfoliation of CFs, and ball milling of CFs and SiC powder in isopropyl alcohol. A wide range of CFs loading, from 10 to 50 vol%, was studied. The milling of CFs and SiC powder was checked by measuring the average particle size of the composite powders. The dispersivity of CFs in SiC powder was checked through scanning electron microscope. The results show that the usage of exfoliated CF tows resulted in a rapid and effective milling of CFs and SiC powder. The results further show an excellent dispersion of CFs in SiC powder for all CFs loading without any dispersing agent.

Fabrication of the Fine Magnetic Abrasives by using Mechanical Alloying Process and Its Polishing Characteristics (기계적 합금화 공정을 이용한 초미세 자성연마입자의 제조 및 특성 평가)

  • Park Sung-Jun;Lee Sang-Jo
    • Journal of the Korean Society for Precision Engineering
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    • v.21 no.10
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    • pp.34-41
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    • 2004
  • A new method to fabricate the fine magnetic abrasives by using mechanical alloying is proposed. The mechanical alloying process is a solid powder process where the powder particles are subjected to high energetic impact by the balls in a vial. As the powder particles in the vial are continuously impacted by the balls, cold welding between particles and fracturing of the particles take place repeatedly during the ball milling process using a planetary mill. After the manufacturing process, fine magnetic abrasives which the guest abrasive particles c lung to the base metal matrix without bonding material can be obtained. The shape of the newly fabricated fine magnetic abrasives was investigated using SEM and its polishing performance was verified by experiment. It is very helpful to finishing the injection mold steel in final polishing stage. The areal ms surface roughness of the workpiece after several polishing processes has decreased to a few nanometer scales.

Solid State Reduction of Haematite by Mechanical Alloying Process (기계적 합금화법에 의한 헤마타이트의 고상환원)

  • 이충효;홍대석;이만승;권영순
    • Journal of Powder Materials
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    • v.9 no.1
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    • pp.25-31
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    • 2002
  • The efects of mechanical aloying conditions and the type of reducing agent on the solid state reductionof haematite $Fe_2O_3$ have been investigated at room temperature. Aluminium titanium zinc and copper were used as reducing agent. Nanocomposites of metal-oxide in which oxide particles with nano size were dispersed in Fe matrix were obtained by mechanical alloying of $Fe_2O_3$ with aluminium and titanium respectively However the reduction of $Fe_2O_3$ by coppe was not occurred Composite materials of iron with $Al_2O_3$ and $TiO_2$ were obtained from the system of $Fe_2O_3-Al$ and $Fe_2O_3-Ti$ after ball milling for 20 hrs and 30 hrs respectively. And the system of $Fe_2O_3-Zn$ resulted in the formationof FeO with ZnO after ball milling of 120 hrs. The final grain sizes of iron estimated by X-ray diffraction line-width measurement were in the ranges of 24~33 nm.