• Title/Summary/Keyword: Measurement standards

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Measurement of Cortisol in Human Serum by Isotope Dilution Liquid Chromatography/Mass Spectrometry and a Comparison through a Proficiency Testing

  • Lee, Hwa-Shim;Shin, Hye-Sun;Park, Sang-Ryoul;Park, Chang-Joon
    • Bulletin of the Korean Chemical Society
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    • v.31 no.5
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    • pp.1149-1154
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    • 2010
  • Liquid chromatography/mass spectrometry using isotope dilution method has been established as a primary method for the measurement of cortisol in human serum. Verification of this method was accomplished by the participation in Consultative Committee for Amount of Substance-Metrology in Chemistry (CCQM) pilot study. Two levels of cortisol certified reference materials were prepared and certified by the established method. They were used as sample materials for the proficiency testing. The expanded uncertainty in the measurement of cortisol in human serum was approximately 1.2% at 95% confidence level. The results of the proficiency testing showed a good precision among the participants, but some bias to the certified values. This means that commercial field laboratories should keep traceability chain to SI unit through available reference measurement procedures and/or available reference materials.

Estimation of Measurement Uncertainty in Evaluation of Tensile Properties (인장 물성 측정 불확도 평가)

  • Huh, Y.H.;Lee, H.M.;Kim, D.J.;Park, J.S.
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.1
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    • pp.73-78
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    • 2010
  • Estimation of tensile properties measurement uncertainty of material was carried out. Sources of uncertainty affecting the measurement of tensile properties were classified and analyzed. The models for uncertainty evaluation of measurands to be determined from tensile test, such as elastic modulus, yield strength and tensile strength, were suggested and derived from the mathematical relations, corresponding to the respective measurands, and the measuring quantities by calculating each sensitivity coefficient of the quantities. Based on these models, the uncertainty of the tensile properties was evaluated from the experimental data of SUS316LN determined according to ISO 6892.

Infrared Thermography Characterization of Defects in Seamless Pipes Using an Infrared Reflector

  • Park, Hee-Sang;Choi, Man-Yong;Park, Jeong-Hak;Lee, Jea-Jung;Kim, Won-Tae;Lee, Bo-Young
    • Journal of the Korean Society for Nondestructive Testing
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    • v.32 no.3
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    • pp.284-290
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    • 2012
  • Infrared thermography uses infrared energy radiated from any objects above absolute zero temperature, and the range of its application has been constantly broadened. As one of the active test techniques detecting radiant energy generated when energy is applied to an object, ultrasound infrared thermography is a method of detecting defects through hot spots occurring at a defect area when 15~100 kHz of ultrasound is excited to an object. This technique is effective in detecting a wide range affected by ultrasound and vibration in real time. Especially, it is really effective when a defect area is minute. Therefore, this study conducted thermography through lock-in signal processing when an actual defect exists inside the austenite STS304 seamless pipe, which simulates thermal fatigue cracks in a nuclear power plant pipe. With ultrasound excited, this study could detect defects on the rear of a pipe by using an aluminium reflector. Besides, by regulating the angle of the aluminium reflector, this study could detect both front and rear defects as a single infrared thermography image.

Study on the Defects Detection in Composites by Using Optical Position and Infrared Thermography

  • Kwon, Koo-Ahn;Park, Hee-Sang;Choi, Man-Yong;Park, Jeong-Hak;Choi, Won Jae
    • Journal of the Korean Society for Nondestructive Testing
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    • v.36 no.2
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    • pp.130-137
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    • 2016
  • Non-destructive testing methods for composite materials (e.g., carbon fiber-reinforced and glass fiber-reinforced plastic) have been widely used to detect damage in the overall industry. This study detects defects using optical infrared thermography. The transient heat transport in a solid body is characterized by two dynamic quantities, namely, thermal diffusivity and thermal effusivity. The first quantity describes the speed with thermal energy diffuses through a material, whereas the second one represents a type of thermal inertia. The defect detection rate is increased by utilizing a lock-in method and performing a comparison of the defect detection rates. The comparison is conducted by dividing the irradiation method into reflection and transmission methods and the irradiation time into 50 mHz and 100 mHz. The experimental results show that detecting defects at 50 mHz is easy using the transmission method. This result implies that low-frequency thermal waves penetrate a material deeper than the high-frequency waves.

Development of the Near/Far Absolute Gain Measurement System Using an Extrapolation Technique (외삽기법을 이용한 안테나의 원 ${\cdot}$ 근역장 절대이득 측정시스템 개발)

  • Shin, Joon;Kang, Chan-Koo;Kim, Jeong-Hwan;Chung, Nak-Sam
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.27 no.2
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    • pp.31-38
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    • 1990
  • An antenna gain measurement system using an extrapolation technique is described. The technique is similar to the usual two-antenna method for absolute gain measurement system, but involves the measurement of the received signal as a function of seperation in short distances, and the signal-versus-seperation data is processed in a way that allows an extrapolation of the signal to "infinite" seperation. In this technique it is possible to obtain the near field gain as function of distance by combining the far field gain and a proximity correction factor. The results of gain measurements of standard gain horn antennas and OEG (open ended waveguide) antennas are also presented.

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Uncertainty Analysis of 1 GHz Band Impulse Spectrum Amplitude (1 GHz 대역 임펄스의 스펙트럼 진폭 불확도 평가)

  • Lee, Dong-Joon;Lee, Joo-Gwang;Kwon, Jae-Yong;Kang, Tae-Weon
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.23 no.12
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    • pp.1365-1372
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    • 2012
  • This paper presents a methodology to accurately evaluate the spectral components of impulse signals which are delivered from an impulse generator through the measurement system. The complicated terms for uncertainty measurement of impulse spectrum amplitude and their analysis methods and experimental results are discussed. The expanded uncertainty of the impulse spectrum measurement is 0.015, which is believed to be the best domestic measurement capability and comparable to those of world class.