• 제목/요약/키워드: Mean grain size

검색결과 313건 처리시간 0.028초

강소성압연법으로 제조된 초미세립 마그네슘 재료의 마이크로 성형능 (Micro-forming Ability of Ultrafine-Grained Magnesium Alloy Prepared by High-ratio Differential Speed Rolling)

  • 유성진;김우진
    • 대한금속재료학회지
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    • 제49권2호
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    • pp.104-111
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    • 2011
  • An ultrafine grained Mg-9Al-1Zn magnesium alloy with the mean grain size less than $1{\mu}m$ was produced by using high-ratio differential speed rolling. The processed alloy exhibited excellent superplasticity at relatively low temperatures. The micro-forming tests were carried out using a micro-forging apparatus with micro V-grooved shaped dies made of silicon and the micro-formability was evaluated by means of micro-formability index, $R_f$ ($=A_f/A_g$, $A_f$: formed and inflowed area into the V-groove, $A_g$: area of the V-groove). The $R_f$ value increased with temperature up to $280^{\circ}C$ and then decreased beyond $300^{\circ}C$. The decrease of the $R_f$ value at $300^{\circ}C$ was attributed to the accelerated grain coarsening. Increasing the micro-forging pressure increased the $R_f$ values. At a given die geometry, die filling ability decreased as the die position moved away from the die center to the end. FEM simulation predicted this behavior and a method of improving this problem was proposed.

유기산염 열분해법으로 합성한 Cu-Ni-Zn 페라이트분말의 특성과 하소조건 (Calcined Condition and Characteristic of Cu-Ni-Zn Ferrite Powder Made by Thermal Decomposition of Organic Acid Salt)

  • 정재우
    • 한국분말재료학회지
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    • 제2권1호
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    • pp.29-35
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    • 1995
  • In this study the calcined condition and characteristic of Cu-Ni-Zn ferrite powder were investigated. The Cu-Ni-Zn ferrite powder has been synthesized by the thermal decomposition of the organic acid salt. This process did not require a strict pH control and provided the uniform composition and fine powder with about 0.3 $\mu\textrm{m}$. The XRD diffraction pattern of this powder showed about 50% spinel phase. The optimum calcination was found to be done at $700^{\circ}C$ for one hour. After the calcination, the amount of spinel increased to 90%. The distribution of the particle size showed bimodal peaks, one was about 0.5 $\mu\textrm{m}$ and the other was about 20 $\mu\textrm{m}$. The large particles of 20 $\mu\textrm{m}$ were the agglomeration of fine Particles. The mean Particle size of the powder was about 0.4 $\mu\textrm{m}$. The powder was compacted under 100 MPa pressure and sintered at 1100~ $1250^{\circ}C$ for one hour in air. The density of ferrites specimen was a function of the sintering temperature. The higher the temperature, the denser the ferrite. The maximum relative density of the sintered ferrite was about 93% at $1250^{\circ}C$. The grain size of sintered specimen at $1200^{\circ}C$ was 5 $\mu\textrm{m}$ and homogeneous.

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16mol% CaO-84mol% $ZrO_2$ 고용체의 소결특성에 관한 연구 (A Study on Sintering Behavior of 16 mol% CaO-84mol% $ZrO_2$ Solid Solution)

  • 박금철;최영섭
    • 한국세라믹학회지
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    • 제20권4호
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    • pp.347-355
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    • 1983
  • A batch mixture was prepared as 16mol% CaO-84mol% $ZrO_2$ of regeant-grade powder. The monoclinic Zirconia powder had an average particle size of $9.24 \mu\textrm{m}$ and calcium carbonate powder had a reported purity of 99.7 weight percent and mean particle size of TEX>$24, 37<\mu\textrm{m}$. The specimens were fired at 1400, 1500, 1650 and $1750^{\circ}C$ for 0. 3, 5 and 7 hours respectively. After fired the specimens were investigated using Scaning electron microscopy. Density Porosity Compressive strength Modulus of rupture and Thermal expansion were measured X-ray diffration analysis was also carried out. The results are as follows ; 1) As the firing temperature or soaking time was increased firing linear shrinkage apparent density compressive strength and modulus of rupture increased but apparent porosity decreased, 2) Cubic and monoclinic Zirconia was found at $1400^{\circ}C$ and cubic Ziconia found above $1500^{\circ}C$ 3) The specimens fired at 140$0^{\circ}C$ without soaking display thermal expansion curves by monoclinic〓tetragonal transformation and no tranformation was found at $1400^{\circ}C$ for 5hrs and above $1500^{\circ}C$. 4) The lattice parameter had constant value of 5.1345 $\AA$ through all the ranges of firing temperature 5) The higher the firing temperature was or the longer the soaking time was the larger the grain size was.

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퇴적물 이동경로 식별을 위한 입도경향 분석법의 가능성과 한계 (Grain-Size Trend Analysis for Identifying Net Sediment Transport Pathways: Potentials and Limitations)

  • 김성환;류호상;유근배
    • 대한지리학회지
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    • 제42권4호
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    • pp.469-487
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    • 2007
  • 입도경향 분석법은 파이척도로 표현된 평균입도, 분급, 왜도 등 퇴적물 입도조직변수가 퇴적물의 이동경로를 따라 특정한 경향을 보이는 성질을 이용한 퇴적물 이동경로 식별 방법론이다. 적용이 간편하고 저렴하여 지형학 연구에 널리 응용될 수 있는 가능성을 지니고 있으나 방법론상의 한계도 몇 가지 측면에서 지적되고 있어 주의가 필요하다. 이 연구는 McLaren과 Bowles의 1차원 경로분석법, Gao와 Collins, Le Roux의 2차원 이동벡터법 등 현재까지 정립된 입도경향 분석의 대표적인 세 가지 기법을 비교 평가하여 적절한 활용법을 도출하고, 입도경향 분석의 추후 연구과제를 제안한 것이다. McLaren-Bowles의 1차원 경로분석법은 연구자의 현장경험을 분석에 효과적으로 결합시킬 수 있고 X-분포를 통해 퇴적환경에 대한 해석을 제공해주며 장기적인 퇴적물 순이동 패턴을 파악하는데 효과적이나 연구자의 주관적 해석에 의존해야 한다는 점, 식별할 수 있는 시간 해상도가 낮다는 점등이 단점이다. Gao-Collins의 2차원 이동벡터법은 명확한 절차, 2차원적인 시각화, 세밀한 시간 해상도 등이 장점이지만, 임계거리 선정, 잡벡터 제거과정 등이 문제를 유발할 수 있으므로 분석 시 주의를 요한다. 셋째, Le Roux의 2차원 이동벡터법은 확장된 경험규칙과 조직변수 간의 구배를 고려하고 시간해상도도 세밀하지만, 분석개념이 모호하고 복잡하다. 입도경향 분석은 현장에 대한 연구자의 이해도, 조사하고자 하는 퇴적물 순이동 패턴의 시간적 스케일, 초점을 맞추고자 하는 정보 등에 따라 적절한 기법을 선택하고, 거기에 부합되는 시료채취방안을 기획하는 것이 중요하다. 또한 입도경향 분석이 지형학 연구에 기여하기 위해서는 시료채취 깊이, 교란층의 두께 등 시료채취 과정의 요소들과 퇴적물 순이동 패턴이 지시하는 시간스케일 간의 관계가 체계적으로 규명되어야 한다고 판단된다.

한국 서해남부 조간대 표층 퇴적물의 지화학적 특성 (Geochemical Characteristics of Intertidal Surface Sediments along the Southwestern Coast of Korea)

  • 황동운;류상옥;김성길;최옥인;김성수;고병설
    • 한국수산과학회지
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    • 제43권2호
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    • pp.146-158
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    • 2010
  • In order to evaluate the characteristics of sediments and pollution by organic matter and metallic elements in intertidal sediments along the southwestern coast of Korea, we measured various geochemical parameters, including the mean grain size (Mz), water content (WC), ignition loss (IL), chemical oxygen demand (COD), acid volatile sulfide (AVS), and metallic elements (Al, Fe, Cu, Pb, Zn, Cd, Cr, Mn, Hg, As), in intertidal surface sediments. The Mz of the surface sediments ranged from 2.1 to 8.3$\phi$, indicating that the surface sediments consist of various sedimentary facies, such as sand, slightly gravelly mud, sandy mud, and silt. The IL and COD in surface sediment ranged from 0.8 to 5.5% (mean $2.9\pm1.2%$) and from 3.9 to $13.8\;mgO_2/g{\cdot}dry$ (mean $8.5\pm2.6\;mgO_2/g{\cdot}dry$), respectively, which were lower than the values for surface sediment in areas near fish and shellfish farms or industrial complexes. No AVS was detected at any sampling station, despite various sedimentary facies. Most of metallic elements in surface sediments showed relatively good positive correlations with Mz and IL, which imply that the concentrations of metallic elements are mainly controlled by grain size and the organic matter content. The concentrations of metallic elements, except As, at some stations were considerably lower than those in the Sediment Quality Guideline (Effect Range Low, ERL) proposed by the National Oceanic and Atmospheric Administration (NOAA) in the United States. Similarly, the geoaccumulation index (Igeo) class indicated that pollution by metallic elements in intertidal surface sediment, except As, was moderate or non-existent. Our results imply that the intertidal surface sediments along the southwestern coast of Korea are not polluted by organic matter and metallic elements and are healthy for benthic organisms.

영암호 저서동물군집에 미친 하구둑 건설의 영향 (Ecological Impact of the Dyke Construction on the Marine Benthos Community of the Oligohaline Youngam Lake)

  • 임현식;최진우
    • 한국수산과학회지
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    • 제38권3호
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    • pp.172-183
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    • 2005
  • To assess the macrobenthic community of oligohaline Youngam Lake, which is located at the Youngsan Watershed on the southwest part of Korea, macrobenthic fauna were collected at 45 stations during May, 2002. A total of 16 species of macrofauna were recorded with a mean density of 240 individuals per $m^2$ and a mean biomass of 7.07 g wet weight per $m^2$. Major dominant faunal groups were crustacean arthropods in terms of the number of species and abundance, and polychaete annelids in terms of biomass. The mean grain size was $5.7\;{\phi}$ which was dominated by silt fraction. The hydrological environment of the lake was characterised as an oligohaline environment with a mean surface water temperature of $17.8^{\circ}C$ and a mean salinity of 2.08 psu. The major dominant species were amphipods, Corophium sp. ($31\%$) and Jesogammarus sp. ($25\%$). Lowe. values of species diversity (H') with a mean of 0.81 (less than 1.0 from most stations) reflected the overall poor faunal diversity in this area. Multivariate analysis suggested that this benthic faunal community could be divided into four sub-regions such as the area from lake proper to water channel to the south, the stations located at the entrance and northern water channel, the stations near the dike, and the lake proper area. Freshwater and brackish water species which occurred in each station group were corresponded to the oligohaline salinity regime. Bottom hypoxia appeared in the entrance part of the lake between dyke and lake proper on May, which was resulted from stratification from spring season. These facts imply that marine macrobenthos were severely impacted by low salinity and a consequent hypoxia after embankment of the lake due to the restriction of water circulation.

강화도 남단 조간대에 도래하는 마도요류의 환경수용능력 예측 (Bird-Days Carrying Capacity Estimation of the Curlews Stopping Over in the Southern Intertidal Zone of Kanghwa Island)

  • 문영민;김관목;유정칠
    • 한국습지학회지
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    • 제15권2호
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    • pp.281-288
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    • 2013
  • 본 연구는 현재 강화도 남단 조간대의 마도요류(알락꼬리마도요 Numenius madagascariensis와 마도요 Numenius arquata) 서식지로서의 질을 평가하고자 환경수용능력(Carrying capacity)을 추정하였다. 저서무척추동물(칠게 Macrophthalmus japonicus)의 생물량 추산에 있어 토양 입도(Sediment grain size)의 공간 분포를 고려하였으며, GIS의 공간 분석 기법을 이용하였다. 추정 결과 2012년 봄철은 약 153일 동안 11,767개체가 이용할 수 있는 수준이었으며, 가을철은 약 122일 동안 16,275개체가 이용할 수 있는 수준이었다. 환경수용능력 대비 평균 도래 개체군의 차지 비율은 봄철 9.4%, 가을철 5.9%의 수준이었으며, 이는 분석 방법이 달라 직접 비교는 어려우나 1993-94년 선행 연구 대비 2.8-6.3% 수준이 감소한 수치였다. 과거에 비해 환경 수용 능력이 감소한 현재의 상황에서 향후 서식지 보전을 위한 지속적인 연구와 관리가 매우 시급하다고 판단되며, 나아가 향후 조간대의 다양한 서식지 특성을 반영한 공간 분석을 통해 더욱 정교한 예측이 필요하다.

Wet/dry Repetitions of Centennial Scale Reconstructed by Inorganic Chemistry of the Mid-Holocene Hwayang Wetland in the West Coast of Korea

  • Yang, Dong-Yoon;Kim, Ju-Yong;Nahm, Wook-Hyun;Yi, Sang-Heon;Kim, Jin-Kwan;Kim, Jeong-Chan;Lee, Jin-Young
    • 한국제4기학회지
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    • 제21권2호
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    • pp.69-73
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    • 2007
  • Inorganic geochemical and mineralogical analyses from the trench sediments of the Hwayang wetland were carried out to verify the wet/dry conditions during 6000 - 5000 yr BP and abnormal event of 6300 yr BP of Korean west coast. Lithostratigraphy, mineralogy and major element concentrations of the sediments of the trench indicate that during 6000 - 5000 yr BP, a wet/dry conditions might be repeated at an interval of 200 years. Carbonate minerals precipitated with the decrease of water depth in the lake or wetland after about 6000 yr BP. On the other hand, the sediments coarser in mean grain size and larger in standard deviation were corresponded with periods of 6300 yr BP and 6230 yr BP. Especially, such a feature of grain size distribution of 6300 yr BP appears in other wetlands situated in the west coast, e.g., Hwangsan wetland and Cheollipo coastal wetland. During the period, the coarse sediments seem to have been delivered by a high energy like storming.

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전남 남부 도서갯벌 퇴적물의 유기물 및 미량금속 오염 평가 (Evaluation of Organic Matter and Trace Metal Contaminations of Intertidal Sediments from Coastal Islands in the Southern Region of Jeollanam Province)

  • 황동운;김평중
    • 한국수산과학회지
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    • 제46권5호
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    • pp.626-637
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    • 2013
  • We measured the grain size, ignition loss (IL), chemical oxygen demand (COD), acid volatile sulfide (AVS) and trace metals (Al, Fe, Cu, Pb, Zn, Cd, Cr, Mn, Hg, and As) of intertidal surface sediment collected from 11 islands (62 stations) in the southern region of Jeollanam Province. The objective of this research was to evaluate the organic matter and trace metals contaminations of sediments from coastal island tidal flats. Surface sediment texture was characterized as follows: mud, sandy silt, muddy sand, and slightly gravelly sand facies. The finer sediments are mainly dominated in the northern part of each island. The concentrations of IL, COD, AVS and some trace metals (Al, Fe, Zn, Cr, Cu, and Hg) were higher in the northwestern part of Wan Island and the area between Gogeum and Sinji Islands, and were associated with relatively finer sediment, as compared to other locations. The concentrations of Mn, Pb, Cd, and As were higher in the northwestern and southeastern parts of Geoguem and Pyungil Islands, but were not correlated with mean grain size. Based on sediment quality guidelines (SQGs), the concentrations of trace metals were lower than the values of effect range low (ERL), used in United States, and threshold effects level (TEL), used in Korea, with exception of As. Similarly, the intertidal sediments were moderately contaminated with As, based on the the enrichment factor (EF) and the geoaccumulation index ($I_{geo}$). The high concentration of As in intertidal sediments from this study region may be due to the input of naturally or artificially contaminated submarine groundwater, contaminated waste from seaweed aquaculture operations and/or land-based seaweed processing facilities. Further studies are needed to identify the sources of As in this study region, and to determine the effects of As contamination on coastal ecosystem.

Depositional Processes of Fine-Grained Sediments and Foraminiferal Imprint of Estuarine Circulation by Summer Floods in Yoja Bay, Southern Coast of Korea

  • Lee, Yeon-Gyu;Jung, Kyu-Kui;Woo, Han-Jun;Chu, Yong-Shik
    • Journal of the korean society of oceanography
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    • 제35권2호
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    • pp.109-123
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    • 2000
  • Depositional processes of fine-grained sediments were investigated on the basis of sediment transport vector analysis and identification of benthic foraminiferal assemblages in Yoja Bay, southern coast of Korea. The bay is a semi-enclosed embayment where extensive mud flats occur with a width up to about 4 km. Most surface sediments are poorly sorted (sorting values: 1.9-3.0 ${\phi}$) mud and silt (mean grain size: 6.0-8.7 ${\phi}$), except for the tidal inlets with basement rocks locally exposed. Grain-size distribution shows a fining tendency toward the basin center near the Yoja Island, implying a possible existence of turbidity maximum and relatively rapid settling of fine-grained sediments. The agglutinated foraminiferal taxa are dominant in the inner bay and decrease in abundance toward the mouth of the bay. Species diversities are higher in the outer bay, due to mixing of the offshore faunas with those of the bay. Four groups of benthic foraminiferal assemblages, identified by cluster analysis, represent the bay. Biofacies I and ll with relatively lower diversities are dominated by Ammobaculites exiguus and Ammonia beccarii, suggestive of influx of fresh water. In contrast, biofacies III and IV with relatively higher diversities include increased amounts of calcareous genus Elphidium and Quinquelocuzina, accounting for strong influence of sea water from the offshore. The fluvial discharge in summer floods appears to develop a bay-wide, clockwise lateral circulation in Yoja Bay, a typical of well-mixed estuaries. Accordingly, the foraminiferal assemblages of the surface sediments well show a sign of this circulation. The dominant inflow of the offshore water into the western part of the bay has resulted in more extensive muddy tidal flats compared to the eastern narrower counterpart.

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