• Title/Summary/Keyword: Materials characterization

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A Study on Material Characterization of Semi-Solid Materials (I) -Proposal of New Velocity Field for Upper Bound Analysis of Backward Extrusion- (반용융 재료의 물성치 평가에 관한 연구(I) -후방압출의 상계해석을 위한 동적 가용 속도장의 제안-)

  • 이주영;김낙수
    • Transactions of Materials Processing
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    • v.8 no.4
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    • pp.364-373
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    • 1999
  • For material characterization of semi-solid materials, backward extrusion process, which has been used in forming of hollow-sectioned products, was analyzed by the upper bound analysis in the current study. The existing kinematically admissible velocity field was applied to steady state at which there was no change in the assumed regions of velocity field. For unsteady state, new velocity field, as a function of dead zone angle, was proposed. Through the whole analysis, fiction between die and workpiece was also considered. It has been studied how the process variables, such as friction factor and punch velocity, and material parameters, such as strength coefficient, strain rate sensitivity could affect on analysis results. Finally, by the comparison with the finite element analysis, the reliability and efficiency of the proposed velocity field were discussed.

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Electron Microscopy for the Morphological Characterization of Nanocellulose Materials (전자현미경을 이용한 나노셀룰로오스 물질의 형태학적 특성 분석 연구)

  • Kwon, Ohkyung;Shin, Soo-Jeong
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.48 no.1
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    • pp.5-18
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    • 2016
  • Electron microscopy is an important investigation and analytical method for the morphological characterization of various cellulosic materials, such as micro-crystalline cellulose (MCC), microfibrillated cellulose (MFC), nanofibrillated cellulose (NFC), and cellulose nanocrystals (CNC). However, more accurate morphological analysis requires high-quality micrographs acquired from the proper use of an electron microscope and associated sample preparation methods. Understanding the interaction of electron and matter as well as the importance of sample preparation methods, including drying and staining methods, enables the production of high quality images with adequate information on the nanocellulosic materials. This paper provides a brief overview of the micro and nano structural analysis of cellulose, as investigated using transmission and scanning electron microscopy.

Electrospray Deposition and Characterization of Single-Walled Carbon Nanotube Thin Films

  • Sundharam, Sridharan;Choi, Kyung-Hyun
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2011.05a
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    • pp.40.1-40.1
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    • 2011
  • Single-walled carbon nanotubes are one among the most promising carbonaceous materials to be used as the electrodes in the devices like micro batteries, supercapacitors, etc. In this study, single-walled carbon nanotube thin films have been fabricated through electrospray deposition technique which is one of the attractive direct printing methods in the field of printed electronics. Single-walled carbon nanotube ink (water dispersed, 3wt %) has been used to fabricate thin films through electrospray deposition technique. The as-deposited SWCNT thin films have been characterized using the appropriate characterization techniques and the results are presented.

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Facile Synthesis, Characterization and Photocatalytic Activity of MWCNT-Supported Metal Sulfide Composites under Visible Light Irradiation

  • Zhu, Lei;Meng, Ze-Da;Oh, Won-Chun
    • Journal of the Korean Ceramic Society
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    • v.49 no.2
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    • pp.155-160
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    • 2012
  • This paper reported a simple deposition-precipitation method, introducing the metal (Ni, Ag and Sn) and $Na_2S{\cdot}5H_2O$ to preparedispersion metal sulfide nanoparticles on the surface of the Multi-walled carbon nanotube for synthesis of CNT-$M_xS_y$ ($NiS_2$, $Ag_2S$, SnS) composite photocatalysts. The characterization of the prepared CNT-$M_xS_y$ ($NiS_2$, $Ag_2S$, SnS) composites was performed by X-ray diffraction, scanning electron microscopy with energy dispersive X-ray analysis and BET analysis. Furthermore, the MB degradation rate constant for CNT-SnS composite was $5.68{\times}10^{-3}$ under visible light irradiation, which was much higher than the corresponding values for other samples. The detailed formation and photocatalytic mechanism are also provided here.

Studies on Borassus fruit fiber and its composites with Polypropylene

  • Sudhakara, P.;Obi Reddy, K.;Prasad, C. Venkata;Jagadeesh, Dani.;Kim, H.S.;Kim, B.S.;Bae, S.I.;Song, J.I.
    • Composites Research
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    • v.26 no.1
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    • pp.48-53
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    • 2013
  • This paper summarizes the structural characterization of borassus fruit fibers by means of various characterization techniques, optimization of alkali treatment of borassus fruit fine fibers (BFF) with a 5% concentration sodium hydroxide solution for different time intervals (1, 4, 8 and 12 h) and the changes occurring in borassus fibers. This paper also discusses the manufacturing of BFF/PP compotes using MAPP as a compatibilizer in addition to alkali treatment. Composites were evaluated for their mechanical and morphological properties. The tensile strength and modulus, flexural strength and modulus and impact strength were increased for alkali treated/MAPP composites by 4.5%, 17%, 17.2 %, 9% and 10% respectively.