• Title/Summary/Keyword: Material property test

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The Effect of Hydrogen on Mechanical Properties of Gas Pipeline Material: I Tensile property (가스배관 재료의 기계적특성에 미치는 수소의 영향: I 인장특성)

  • Kim, Woo-Sik;Jang, Jae-Il
    • Journal of the Korean Institute of Gas
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    • v.15 no.3
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    • pp.67-73
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    • 2011
  • One of the important topics to prepare the up-coming era of so-called ‘hydrogen economy’ is hydrogen transmission. Pipeline is conceivably the most economic way to consistently and safely transport a large amount of hydrogen over a long distance, which may be strongly requested in hydrogen economy era. As a good starting point for the purpose, one might wonder whether conventional API pipeline steels as designed for natural gas transmission can be used as the hydrogen pipeline materials or not. To answer the question, here we performed a series of micro-/nano-indentations together with tensile tests on the hydrogen-charged API X65, X70 and X100 steels having different strength level. In this paper, from the results of tensile tests, the hydrogen effects on the mechanical behavior in the API steels are systematically evaluated.

Shaking table test of wooden building models for structural identification

  • Altunisik, Ahmet C.
    • Earthquakes and Structures
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    • v.12 no.1
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    • pp.67-77
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    • 2017
  • In this paper, it is aimed to present a comparative study about the structural behavior of tall buildings consisting of different type of materials such as concrete, steel or timber using finite element analyses and experimental measurements on shaking table. For this purpose, two 1/60 scaled 28 and 30-stories wooden building models with $40{\times}40cm$ and $35{\times}35cm$ ground/floor area and 1.45 m-1.55 m total height are built in laboratory condition. Considering the frequency range, mode shapes, maximum displacements and relative story drifts for structural models as well as acceleration, displacement and weight limits for shaking table, to obtain the typical building response as soon as possible, balsa is selected as a material property, and additional masses are bonded to some floors. Finite element models of the building models are constituted in SAP2000 program. According to the main purposes of earthquake resistant design, three different earthquake records are used to simulate the weak, medium and strong ground motions. The displacement and acceleration time-histories are obtained for all earthquake records at the top of building models. To validate the numerical results, shaking table tests are performed. The selected earthquake records are applied to first mode (lateral) direction, and the responses are recorded by sensitive accelerometers. Comparisons between the numerical and experimental results show that shaking table tests are enough to identify the structural response of wooden buildings. Considering 20%, 10% and 5% damping rations, differences are obtained within the range 4.03-26.16%, 3.91-65.51% and 6.31-66.49% for acceleration, velocity and displacements in Model-1, respectively. Also, these differences are obtained as 0.49-31.15%, 6.03-6.66% and 16.97-66.41% for Model-2, respectively. It is thought that these differences are caused by anisotropic structural characteristic of the material due to changes in directions parallel and perpendicular to fibers, and should be minimized using the model updating procedure.

Evaluation of Applicability on a High-rise Building for the Effective Usage of High Performance Steel for Building Structures (건축구조용 고성능 강재 HSA800의 효율적 사용을 위한 초고층 건물의 적용성 평가)

  • Kim, Do Hwan;Kim, Joo Woo;Lee, Dong Woo;Yang, Jae Guen;Lee, Myung Jae
    • Journal of Korean Society of Steel Construction
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    • v.26 no.5
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    • pp.463-471
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    • 2014
  • As building height and span is getting taller and longer, the researches to increase material's strength and serviceability are continuously performed. This study evaluated mechanical and chemical properties of newly developed high-strength steel (HSS) for building structures, namely HSA800 and verified cost-effectiveness and applicability of HSS for a tall building by comparing the analysis results of normal strength steel (SM490) model. HSA800 was manufactured by TMCP to have a good weldability in spite of HSS and satisfied Korean Industrial Standards (KS). The analysis results for evaluating cost-effectiveness show that total steel quantity could be saved approximately 30% when using HSS compared to SM490. It is expected that HSA800 will contribute to enhance constructability of building.

Structural and Corrosive Properties of ZrO2 Thin Films using N2O as a Reactive Gas by RF Reactive Magnetron Sputtering (N2O 반응 가스를 주입한 RF Reactive Magnetron Sputtering에 의한 ZrO2 박막의 구조 및 부식특성 연구)

  • Jee, Seung-Hyun;Lee, Seok-Hee;Baek, Jong-Hyuk;Kim, Jun-Hwan;Yoon, Young-Soo
    • Journal of the Korean Ceramic Society
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    • v.48 no.1
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    • pp.69-73
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    • 2011
  • A $ZrO_2$ thin film as a corrosion protective layer was deposited on Zircaloy-4 (Z-4) clad material using $N_2O$ as a reactive gas by RF reactive magnetron sputtering at room temperature. The Z-4 substrate was located in plasma or out of plasma during the $ZrO_2$ deposition process to investigate mechanical and corrosive properties for the plasma immersion. Tetragonal and monoclinic phases were existed in $ZrO_2$ thin film immersed in plasma. We observed that a grain size of the $ZrO_2$ thin film immersed in plasma state is larger than that of the $ZrO_2$ thin film out of plasma state. In addition, the corrosive property of the $ZrO_2$ thin films in the plasma was characterized using the weight gains of Z-4 after the corrosion test. Compared with the $ZrO_2$ thin film immersed out of plasma, the weight gains of $ZrO_2$ thin film immersed in plasma were larger. These results indicate that the $ZrO_2$ film with the tetragonal phase in the $ZrO_2$ can protect the Z-4 from corrosive phenomena.

Study on operating characteristics of Ferrite cores for Flat TR in high frequency (Flat TR용 페라이트 코아의 고주파 동작 특성)

  • Han, Se-Won;Cho, Han-Goo;Ryu, Dong-Uk;Choi, Kwang-Bo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07b
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    • pp.1168-1171
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    • 2003
  • In contrast to a conventional transformer, the flat transformer is made using a number of small ferrite cores. Two cores for transformer and one core for inductor, which composed one module. Many modules can be connected together to form a flat matrix transformer. This structural arrangement eliminates the single hot spot problem in conventional transformers and permits high current density pertains at high frequency. In this study, the ferrite magnetic cores of Mn-Zn system for the Flat transformer were manufactured and the electrical and magnetic characteristics of its tested. The power loss of sample FO2(Mn-Zn ferrite) sintered at $1350^{\circ}C$ was $350kW/m^3$ in test conditions of 250kHz, 200mT and $100^{\circ}C$, which showed the good power loss property in high frequency. The power loss of FO2 samples has been studied as a function of magnetic flux density and frequency. Steinmetz exponent was 2.82 at 250kHz and 2.73 at 500kHz. These results illustrated the switching of power loss mechanism in ferrite core from hysteresis losses to eddy current losses or others.

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Design and Fabrication of Full-Scale Regenerative Cooling Combustion Chamber (${\varepsilon}$=12) of Liquid Rocket Engine for Ground Hot Firing Tests (지상연소시험용 실물형 재생냉각 연소기(확대비 12)의 설계 및 제작)

  • Kim, Jong-Gyu;Han, Yeoung-Min;Seo, Seong-Hyeon;Lee, Kwang-Jin;Choi, Hwan-Seok
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2007.11a
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    • pp.114-118
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    • 2007
  • Design and fabrication of a 30-tonf-class full-scale regenerative cooling combustion chamber of a liquid rocket engine for a ground hot firing test are described. It has chamber pressure of 60 bar and nozzle expansion ration of 12 and manufactured to have a single welded structure of· the mixing head and the chamber. The material of the mixing head is STS316L which has excellent mechanical property in cryogenic condition. The chamber comprise of the cylinder, nozzle throat, and 1st/2nd nozzle parts. The material of the inner jacket is copper alloy/STS329J1/STS316L and that of the outer jacket is STS329J1. The components of· the combustor were manufactured by mechanical processing including lathing, milling, MCT, rolling and pressing. The machined components were integrated to a single body by means of general welding, electron beam welding(EBW), and brazing.

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Prediction of the Equivalent Elastic Properties of Fiber Reinforced Composite Materials and Structural Analysis of Composite Satellite Panel (섬유강화 복합재료 등가탄성계수 예측과 복합재료 위성패널의 구조해석)

  • You, Won-Young;Lim, Jae Hyuk;Sohn, Dongwoo;Kim, Sun-Won;Kim, Sung-Hoon
    • Aerospace Engineering and Technology
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    • v.12 no.2
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    • pp.48-56
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    • 2013
  • In this paper, the equivalent elastic properties of fiber reinforced plastic laminar are investigated using various homogenization schemes. Although there are several methods for predicting the equivalent elastic properties such as analytical formula or semi-empirical formula, most of them have some limitations or are not much accurate when handling new composite material consisting of various fiber, matrix and fiber-volume fraction ratio. To resolve the issues, computational homogenization scheme is adopted with a representative volume element (RVE) comprised of a set of finite elements. Finally, the equivalent elastic properties are obtained by applying periodic boundary conditions. The obtained results are compared with those by the existing methods and test results. Also its effect on structural analysis results of the composite satellite panel is investigated.

Plasma etching behavior of RE-Si-Al-O glass (RE: Y, La, Gd)

  • Lee, Jeong-Gi;Hwang, Seong-Jin;Lee, Seong-Min;Kim, Hyeong-Sun
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2010.05a
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    • pp.49.1-49.1
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    • 2010
  • The particle generation during the plasma enhanced process is highly considered as serious problem in the semiconductor manufacturing industry. The material for the plasma processing chamber requires the plasma etching characteristics which are homogeneously etched surface and low plasma etching depth for preventing particulate contamination and high durability. We found that the materials without grain boundaries can prevent the particle generation. Therefore, the amorphous material with the low plasma etching rate may be the best candidate for the plasma processing chamber instead of the polycrystalline materials such as yttria and alumina. Three glasses based on $SiO_2$ and $Al_2O_3$ were prepared with various rare-earth elements (Gd, Y and La) which are same content in the glass. The glasses were plasma etched in the same condition and their plasma etching rate was compared including reference materials such as Si-wafer, quartz, yttria and alumina. The mechanical and thermal properties of the glasses were highly related with cationic field strength (CFS) of the rare-earth elements. We assumed that the plasma etching resistance may highly contributed by the thermal properties of the fluorine byproducts generated during the plasma exposure and it is expected that the Gd containing glass may have the highest plasma etching resistance due to the highest sublimation temperature of $GdF_3$ among three rare-earth elements (Gd, Y and La). However, it is found that the plasma etching results is highly related with the mechanical property of the glasses which indicates the cationic field strength. From the result, we conclude that the glass structure should be analyzed and the plasma etching test should be conducted with different condition in the future to understand the plasma etching behavior of the glasses perfectly.

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Synthesis of Multi-component Olivine by a Novel Mixed Transition Metal Oxalate Coprecipitation Method and Electrochemical Characterization

  • Park, Yeong-Uk;Kim, Jong-Sun;Gwon, Hyeok-Jo;Seo, Dong-Hwa;Kim, Seong-Uk;Hong, Ji-Hyeon;Gang, Gi-Seok
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2010.05a
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    • pp.37.1-37.1
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    • 2010
  • The multi-component olivine cathode material, $LiMn_{1/3}Fe_{1/3}Co_{1/3}PO_4$, was prepared via a novel coprecipitation method of the mixed transition metal oxalate, $Mn_{1/3}Fe_{1/3}Co_{1/3}(C_2O_4){\cdot}2H_2O$. The stoichiometric ratio and distribution of transition metals in the oxalate, therefore, in the olivine product, was affected sensitively by the environments in the coprecipitation process, while they are the important factors in determining the electrochemical property of electrode materials with multiple transition metals. The effect of the pH, atmosphere, temperature, and aging time was investigated thoroughly with respect to the atomic ratio of transition metals, phase purity, and morphology of the mixed transition metal oxalate. The electrochemical activity of each transition metal in the olivine synthesized through this method clearly was enhanced as indicated in the cyclic voltammetry (CV) and galvanostatic charge/discharge measurement. Three distinctive contributions from Mn, Fe, and Co redox couples were detected reversibly in multiple charge and discharge processes. The first discharge capacity at the C/5 rate was $140.5\;mAh\;g^{-1}$ with good cycle retention. The rate capability test showed that the high capacity still is retained even at the 4C and 6C rates with 102 and $81\;mAh\;g^{-1}$, respectively.

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A study on the SEI film formation as organic solvent decomposition of lithium ion batteries and its electrochemical behavior (리튬이온전지의 유기용매분해에 따른 SEI film 형성과 전기화학적 거동에 관한 연구)

  • Kim, Min-Seong;Gu, Hal-Bon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11b
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    • pp.545-549
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    • 2001
  • We have produced electrolyte solution out of 1.15M $LiPF_6$ EC/EMC/DEC/PC(30/55/10/5 by vol%) as a reference, and at the same time, performed basic physical property test using a single solvent of 1.15M $LiPF_6$ DEC, DMC, EMC and a 2 component electrolyte solution of 1.15M $LiPF_6$ EC/DEC(1/2 by vol%) and PC/DEC(1/2 by vol%). Cyclic Voltammetry Analysis showed that, compared to existing carbonate organic solvent, the addition of DEC,DMC and EMC brought the de-decomposition peak of salt anion of $PF_6$ and the solvent at lower oxidization potential of 2.3V, 0.7V and 2.1V(vs. $Li/Li^+$). In addition, a kinetics current peak, in which intercalation of Lt is proceeded at 750mV, 450mV(vs. $Li/Li^+$), was confirmed. These findings suggest that the DEC solvent decomposition occurred at an electric potential lower than that of oxidization of existing carbonate organic solvent. Through the impedance analysis, we checked electric charge transfer resistance($R_{ct}$) according to the electric potential of $Li^+$ intercalation at 750mV(vs. $Li/Li^+$), which was the same as the resistance ($R_f$) and cyclic voltammetry of SEI film that was formed at Reference. By doing so, we found that the significant decrease of polarization resistance($R_p$) when Reference was played a part in the formation of compact SEI layer at the initial decomposition reaction.

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