• Title/Summary/Keyword: Material mixing method

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Syntheses of(Ti, Al)N Powder by the Direct Nitridation (1) (직접질화법에 의한(Ti, Al)N계 복합질화물의 합성(I))

  • Sohn, Yong-Un;Lee, Young-Ki;Hwang, Yeon;Cho, Young-Soo;Kim, Suk-Yoon
    • Journal of the Korean Society for Heat Treatment
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    • v.8 no.3
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    • pp.187-196
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    • 1995
  • TiN and AlN are ceramic materials with mechanical and chemical properties for use in structural applications at elevated temperature. The purpose of this research is to develop the technology for the synthesis of (Ti, Al)N power, which shows simultancously the excellent properties of TiN and AlN, from the mixed powder($Ti_{0.25}Al_{0.75}$, $Ti_{0.5}Al_{0.5}$ and $Ti_{0.75}Al_{0.25}$) by the direct nitriding method. The effects of variables such as temperature, mixing ratio of Al to Ti in raw material were investigated. The(Ti, Al)N powder can be easily synthesized from the mixed powder by the direct nitriding method. Among the mixed powdres, the nitriding behavior decreased with increasing the ratio of Al to Ti. This behavior is well explained by the nitriding mechanism presented in this research.

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Grain Orientation and Electrical Properties of $Sr_2Nb_2O_7$ Ceramics and Thin Films (다결정 및 박막형 $Sr_2Nb_2O_7$의 입자배향과 전기적특성)

  • 손창헌;전상재;남효덕;이희영
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.11 no.4
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    • pp.274-280
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    • 1998
  • Polycrystalline $Sr_2Nb_2O_7$ ceramics with very high Curie temperature were sintered using the powder derived by the chemical coprecipitation method (CCP). The phase evolution and grain-orientation of sintered samples were examined by XRD, while sintering behavior, dielectric properties and polarization were studied by SEM and ferroelectric tester. Extremely high degree of grain-orientation was observed along the (0k0) direction, which resulted in anisotropic dielectric properties of the sintered samples, with the dielectric constant values approaching those for single crystal. Thin film fabrication of $Sr_2Nb_2O_7$ in the pyroniobate family was also attempted on $SiO_2$/Si(100), Pt/$SiO_2$/Si(100), Pt/Ti/$SiO_2$/Si(100) and Pt/$ZrO_2/SiO_2/Si_2(100)$ substrates, using metalorganic decomposition (MOD) process. Neodecanoate precursor solution was prepared by mixing strontium neodecanoate with niobium neodecanoate synthesized from niobium ethoxide. It was found that $Sr_2Nb_2O_7$ single phase appeared in XRD patterns the samples annealed above $950^{\circ}C$. The effect of substrate type on film microstructure and dielectric properties was observed.

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Application study of C.S.G method by the test construction and field test (시험시공 및 현장시험을 통한 C.S.G 공법의 적용성 검토)

  • Kim, Ki-Young;Park, Han-Gyu;Cho, Sung-Eun;Jeon, Je-Sung
    • Proceedings of the Korean Geotechical Society Conference
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    • 2006.03a
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    • pp.61-68
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    • 2006
  • Cemented Sand and Gravel(CSG) is a material made by simple mixing of rock-based raw materials such as excavated soil and riverbed gravel together with cement and water. The use of CSG methodl for cofferdam and large dam is gradually increasing in Japan because a quarry and aggregate plants can be diminished. Also, the CSG method can reduce dam construction cost, construction duration and destruction of environment. In this paper, field test and test construction of CSG method was conducted on Hwabuk Dam. The mechanical properties of CSG, such as compressive strength, extention strength and field permeability test were investigated. From the results of the experimental study, application study of CSG method was discussed.

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Charateristics of Soft Paving Materials used Eco-friendly (친환경 소프트 포장재의 공학적 특성에 관한 연구)

  • Jeon, Du-Jun;Park, Sung-Jin
    • Journal of the Society of Disaster Information
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    • v.15 no.2
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    • pp.206-213
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    • 2019
  • Purpose: This study aims to develop eco - friendly paving materials using Sawdust and EPDM chips. Method: Materials are eco-friendly materials and have no environmental problems. By using EPDM chip, the walking feeling can be increased. Results: In this study, the optimum mixing ratio was calculated through mixing design test. Based on the blending ratio, the surface layer of the sidewalk is made of fine sawdust and EPDM chips. We used only sawdust of grain - 107 -size to make the base layer of the sidewalks and the surface layer of the bicycle road with the permeability and the anti - resilience, and suggested the application method through the test construction. Conclusion: This study the expected that the recent efforts of the government to reduce the elastic paving material, which is the environmentally harmful problem with the complete eco-friendly paving material, are expected to revive.

In Case of Treatment of PEC4 Hydroseeding Measures for Revegetation of Rock Cut-Slopes (암비탈면 녹화용 환경친화적 PEC4 공법의 시공)

  • Kim, Kyung-Hoon;Kim, Hak-Young;Hwang, Ae-Min;Lee, Seung-Eun
    • Journal of the Korean Society of Environmental Restoration Technology
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    • v.2 no.4
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    • pp.64-73
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    • 1999
  • This study was conducted to find out the effects of hydroseeding material and seed mixture on the revegetation of rock cut-slopes by PEC4 (Polymer-Ecology-Control) Hydroseeding Measures. PEC4 hydroseeding material was applied to four cut-slopes using hydroseeding measures from April to August, 1999, and the field survey was carried out by monthly. PEC4 material consisted of bark compost and organic soil amendments. This material has high content of organic matter and high level of water holding capacity. PEC4 hydroseeding material shows low level of soil hardness, so it gives to good condition for seed germinating and plant growing in early stage. PEC4 material attached at rock cut-slopes by two types of adhesive agent was not eroded by rainfall. The plant coverage and number of plant species were affected by mixing ratio of seeds and seeding timing. From the viewpoint of plant establishment, the optimal hydroseeding timing of mixed seeds for plant growth seems to be in May. Most of the plant seeds were germinated well and they covered rock cut-slopes so quickly and effectively. Plant importance value of Silene armeria and Platycodon grandiflorum. were higher than any other seeded-native species in the competition between native species and exotic species, so they have enough possibility to be used for slope revegetation works. Thus it leads to conclusion that the revegetation method used in this experiment was a very effective method for plant establishment on rock cut-slopes.

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Evaluation of 2 Part Curtainwall Structural Silicone Sealant (커튼월용 2액형 구조용 실란트 혼합비별 물성 평가 연구)

  • Kim, Sung Hyun;Jung, Jin-young;Ahn, Myung-Su;Seo, YeonWon;Bae, Keesun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2014.11a
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    • pp.78-80
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    • 2014
  • Silicone structural glazing (SSG) is a method utilizing a silicone adhesive to attach glass, metal, or other panel material to the structure of a building. Windload and other impact loads on the facade are transferred from the glass or panel through the silicone structural sealant to the systems' framework. Silicone structural glazing systems are currently a very common method of glazing throughout the world. Locally, structural silicone glazing has become very common to achieve aesthetically pleasing and high utilization of small land for both residential and commercial building. Although structural silicone glazing has been utilized for approximately thirty years in Korea, the understanding of its technology was low and limited. Consequently, Korean projects experienced many quality issues during assembly and construction, even in very recently finished buildings. Adhesion loss and water infiltration occurred on more than one project, and the time and cost to repair these issues were substantial. In general, there are two kinds of structural silicones depending on fabrication methods. 1part structural silicone is for site glazing system and 2part structural silicone is for unitized factory glazing system. In this paper, 2part structural silicone which is very common for factory fabricating curtainwall systems was evaluated with regards to various mixing ratio. Since the structural performance of 2part sealant can be affected by mixing ratios, some extra ranges of recommended mixing ratio were evaluated to see any performance differences. Besides on cure profile, comparative evaluations for mechanical properties and adhesion develop on common building substrates were conducted.

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Electrical Characteristic of Blend with LLDPE and EVA Due to Mixing Ratio (혼합비에 따른 선형저밀도 폴리에틸렌과 에틸렌비닐아세테이트 블랜드의 전기적 특성)

  • 신종열;이충호;홍진웅
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.14 no.6
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    • pp.525-532
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    • 2001
  • In this paper, physical properties and electrical characteristics of linear low density polyethylene(LLDPE) films blended with ethylene vinyl acetate(EVA), containing polar groups within it, were investigated to improve defects of polyethylene(PE) such like space charge accumulation and tree growth. Blending method changes super-structure of LLDPE, having a great influence on electrical characteristics. For analysis of physical properties, FTIR, XRD and DSC methods were executed, and for electrical characteristics, volume resistivity and dielectric strength were measured with the varying temperature. From the results, it is confirmed that bled specimens tend to be safe to varying temperature, and specially of 70:30 and 50:50 have a good performance.

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The Myths and Facts of MTA (MTA의 Myths & Facts)

  • Ko, Hyun-Jung
    • The Journal of the Korean dental association
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    • v.48 no.11
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    • pp.813-818
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    • 2010
  • Since MTA has many beneficial properties such as biocompatibility, great sealing capacity, antibacterial effects, low cytotoxicity, and stimulation of formation of mineralized tissue, it has been widely used as the material of choice in root-end filling, apexification, pulpotomy, perforation repair and so on. However, despite its favorable characteristics, MTA presents working properties which are less than ideal. The resulting cement from the mixing of powder and water is difficult to manipulate, and its setting time has been reported to be 2 h 45 min whereas the working time is <4 minutes. Additional moisture is also required to activate the setting of the cement. Moreover, according to recent studies, the physical properties of MT A may be hampered by acidic environment or blood contamination. Therefore, practitioners may have surprisingly worse results than they expected when they are not fully acquainted with the characteristics and manipulation method of MTA.

A study on the Etching and Dielectric Properties of PZT Thin Films with Excess Pb Contents (Pb 함량에 따른 PZT 박막의 식각 및 유전특성에 관한 연구)

  • Kim, Kyoung-Tae;Lee, Sung-Gap;Kim, Chang-Il;Lee, Young-Hie
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.04b
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    • pp.56-59
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    • 2000
  • In this study, Ferroelectric $Pb(Zr_x,Ti_{1-x})O_3$(x=0.53) thin films were fabricated by the spin-coating on the Pt/Ti/$SiO_2$/Si substrate using the PZT metal alkoxide solutions with various excess Pb contents. Etching of PZT film was performed using planar inductively coupled Ar(20)$/Cl_2/BCl_3$ plasma. The etch rate of PZT film was 2450 ${\AA}/min$ at Ar(20)$/BCl_3$(80) gas mixing ratio and substrate temperature of $80^{\circ}C$. The leakage current densities of before etching and after etching PZT thin film were $6.25\times10^{-8}A/cm^2$, $8.74\times10^{-7}A/cm^2$ with electric field of 0.07MV/em, respectively.

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Properties of EMNC and EMNSC for Insulation New Material as Apply to High Voltage Heavy Electric Machine (고압중전기기용 절연신소재 EMNC와 EMNSC의 특성연구)

  • Park, Jae-Jun
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.61 no.10
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    • pp.1454-1460
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    • 2012
  • In order to develop an new electric insulation material for heavy electric equipments, epoxy/micro/nano composite (EMNC) was prepared by mixing micro-silica with nano layered silicate, where the nano layered silicate was synthesized by our electric field dispersion method, EMNSC was prepared by treating the EMNC with a silane coupling agent. Thermal properties such as glass transition temperature (Tg) and thermal expansion coefficient, and DMA characteristics were studied, and mechanicla properties such as tensile and flexural tests were performed. AC electrical insulation strength was also tested. All properties of EMNSC were modified by treating EMNC with silane coupling agent and it was confirmed that our new developed composites could be used in the heavy electric equipments.