• The Journal of Advanced Prosthodontics
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• v.11 no.2
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• pp.95-104
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• 2019

PURPOSE. To evaluate the effect of surface treatments and repair materials on the shear bond strength and to measure the fracture toughness of CAD/CAM provisional restoration materials. MATERIALS AND METHODS. Four CAD/CAM (3D printing: Nextdent C&B and ZMD-1000B Temporary, CAD/CAM resin block: Yamahachi PMMA disk and Huge PMMA block) and four conventional (monometacrylate: Jet and Alike, dimetacrylate: Luxatemp and Protemp 4) materials were selected to fabricate disk-shaped specimens and divided into six groups according to surface treatment (n=10). CAD/CAM materials were repaired with Jet or Luxatemp, while conventional materials were repaired with their own materials. The shear bond strength was measured by using universal testing machine. Ten rectangular column-shaped specimens for each material were fabricated to measure the fracture toughness by single edge v notched beam technique. Statistical analysis was performed by one-way ANOVA. RESULTS. The highest shear bond strength of CAD/CAM materials was achieved by SiC paper + sandblasting. It was also accomplished when repairing 3D printing materials with Luxatemp, and repairing CAD/CAM resin blocks with Jet. Yamahachi PMMA disk showed the highest fracture toughness. Nextdent C&B showed the lowest fracture toughness value but no statistically significant difference from Alike and Luxatemp (P>.05). CONCLUSION. In order to successfully repair the CAD/CAM provisional restoration, mechanical surface treatment and appropriate repair material according to the CAD/CAM material type should be selected. The CAD/CAM provisional materials have proper mechanical properties for clinical use as compared to conventional materials.

• Journal of the Korean Society of Safety
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• v.21 no.4 s.76
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• pp.33-41
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• 2006

Material degradation should be considered to assess integrity and residual life of high temperature equipments. However, the property data reflecting degradation are not sufficient for practical use. In this study measuring properties for 1Cr-1Mo-0.25V forging steel generally used for turbine rotor was carried out. Degradation was simulated by isothermal ageing. heat treatment and variation of microstructure was observed. Mechanical properties such as tensile strength, impact energy, hardness and fracture toughness were measured. Assuming a semi-elliptical surface crack at the bore hole in a turbine rotor, material risk was estimated by using the aged material property data obtained in this study. Safety margin was decreased and life of the rotor was exhausted. This procedure can be used in assessing the residual life of a turbine rotor due to material degradation.

• Journal of Dental Rehabilitation and Applied Science
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• v.17 no.3
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• pp.199-204
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• 2001

This study was to investigate the reused possibility of zirconia reinforced glass-ceramic(IPS Empress Cosmo ceramic) with sprue button in the flexure strength and fracture toughness. 40 disk-shaped ceramic specimens (20 specimens: as-pressed material; 20 specimens: reused material) with approximately 1.7 mm thickness and 15 mm diameter were prepared by "lost wax" technique. The remnants(sprue buttons) were used for repressing. The surface treatments for the discs were gradually abraded with 320, 800, 1200, and 2000 grit SiC sandpaper. The specimens were evaluated their flexure strength with the biaxial flexure jig(ball-on-three balls) and their fracture toughness with Vickers Indentation-microfracture test. The Weibull moduli were calculated for biaxial flexural strength. The mean flexure strength and fracture toughness of each group were $122.2{\pm}18.3MPa$, $1.00{\pm}0.09MPa{\cdot}m^{0.5}$ (as-pressed ceramics), and $122.2{\pm}20.3MPa$, $1.01{\pm}0.10MPa{\cdot}m^{0.5}$ (reused ceramics). There were no significant differences in the strength and the fracture toughness between the as-pressed and the reused IPS Empress Cosmo ceramic (P>0.05). This implied zirconia reinforced glass-ceramic(IPS Empress Cosmo ceramic) could be used one more time by reusing of sprue button in the flexure strength and fracture toughness.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1999.05a
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• pp.291-294
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• 1999

The effect of AI$_2$O$_3$+Y$_2$O$_3$additives on fracture toughness of $\beta$-SiC-ZrB$_2$composites by hot-pressed sintering were Investigated. The $\beta$-SiC-ZrB$_2$ ceramic composites were hot-presse sintered and annealed by adding 1, 2, 3wt% AI$_2$O$_3$+Y$_2$O$_3$(6:4wt%) powder as a liquid forming additives at 195$0^{\circ}C$ for 4h. In this microstructures, no reactions were observed between $\beta$-SiC and ZrB$_2$, and the relative density Is over 90.79% of the theoretical density and the porosity decreased with increasing AI$_2$O$_3$+Y$_2$O$_3$ contents. Owing to crack deflection and crack bridging of fracture toughness mechanism, the fracture toughness showed the highest of 5.5328MPa . m$^{1}$2/ for composites added with 2wt% AI$_2$O$_3$+Y$_2$O$_3$ additives at room temperature. But the standard deviation of fracture toughness of specimens decreased with increasing AI$_2$O$_3$+Y$_2$O$_3$ contents and showed the highest of 0.8624 for composite tilth 1wt%, AI$_2$O$_3$+Y$_2$O$_3$additives.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.16 no.6
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• pp.4192-4200
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• 2015

In this paper, dispersibility of steel fiber is improved mixing with form for material development of protection and blast resistant structure sprayed concrete. And it is developed a high toughness cellular sprayed concrete material using steel fiber. Oversupply form for dispersibility improvement of steel fiber is mostly fade away through sprayed, finally it is satisfied with the proper mixing ratio under 3 % ~ 6 %. This is considered for compressive strength and flexural toughness. Test results of compressive strength showed superior strength capability in 28, 56 days, also flexural strength and flexural toughness is great. Then oversupply form is enhanced for dispersibility of steel fiber and I think that it did not cause decreasing of strength. But analysis results of pore structure through image analysis failed for a great spacing factor and specific surface area. This is largely measured in spacing factor because air content have a grate evaporation effect for sprayed.

• The Journal of Advanced Prosthodontics
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• v.14 no.5
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• pp.285-293
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• 2022

PURPOSE. This study evaluated the relationship among translucency, crystalline phase, grain size, and fracture toughness of zirconia. MATERIALS AND METHODS. Four commercial zirconia - Prettau^®Anterior^® (PA), Prettau^® (P), InCorisZI (ZI), and InCorisTZI (TZI)- were selected for this study. The bar specimens were prepared to determine fracture toughness by using chevron notched beam method with four-point bending test. The grain size was evaluated by a mean linear intercept method using a scanning electron microscope. X-ray diffraction and Rietveld refinement were performed to evaluate the amount of tetragonal and cubic phases of zirconia. Contrast ratio (CR) was measured to investigate the level of translucency. RESULTS. PA had the lowest fracture toughness among other groups (P < .05). In addition, the mean fracture toughness of P was significantly less than that of ZI, but there was no difference compared with TZI. Regarding grain size measurement, PA had the largest average grain size among the groups. P obtained larger grain size than ZI and TZI (P < .05). However, there was no significant difference between ZI and TZI. Moreover, PA had the lowest CR value compared with the other groups (P < .05). This means PA was the most translucent material in this study. Rietveld refinement found that PA presented the greatest percentage of cubic phase, followed by TZI, ZI, and P, respectively. CONCLUSION. The different approaches are used by manufacturers to fabricate various types of translucent zirconia with different levels of translucency and mechanical properties, which should be concerned for material selection for successful clinical outcome.

• Composites Research
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• v.21 no.4
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• pp.7-14
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• 2008

Prediction of the load-bearing capacity of an adhesive-bonded Joint is of practical importance for engineers. This paper introduces interface fracture mechanics approach to predict the load-bearing capacity of composite metal bonded joints. The adhesion strength of composite/steel bonding is evaluated in terms of the energy release rate of an interfacial crack and the fracture toughness of the interface. Virtual track closure technique (VCCT) is used to calculate energy release rates, and hi-material end-notched flexure (ENF) specimens are devised to measure the interfacial fracture toughness. Bi-material ENF specimens gave consistent mode II fracture toughness $(G_{IIc})$ values of the composite/steel interface regardless of the thickness of specimens. The critical energy release rates of double-lap joints showed a good agreement with the measured fracture toughness. Therefore. the energy-based interfacial fracture characterization can be a practical engineering tool for predicting the load-bearing capacity of bonded joints.

• Proceedings of the KIEE Conference
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• 1999.07d
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• pp.1864-1866
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• 1999

The magnetic nondestructive test can be applied to evaluate the magnetic material characteristics and the fracture properties through the internal defects of SA-508 used in the pressure vessels of the nuclear power plants as the direct and accurate in-situ testing methods. The fracture toughness, yield strength and the stress distribution around the defects in the surface and sub-surface of magnetic materials can be directly estimated by Bark-hausen noise(BN) methods as NDT. The testing process of SA-508 by Barkhausen noise method was advanced by controlling the austenizing peak temperature and the time of maintenance at a constant austenizing peak temperature, therefore causing the variation of fracture toughness. Through above process. we can evaluate the variations of effective grain size and the correlation of effective grain size and FATT at each situation. And the stress distribution around the defects can be quantified nondestructively through Barkhausen method.

• Transactions of the Korean Society of Mechanical Engineers
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• v.19 no.6
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• pp.1460-1468
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• 1995

The objective of this paper is to evaluate the material properties of SA106 Gr. C carbon steel and its associated weld manufactured for main steam system of Yonggwang 3,4 nuclear generating stations. A total of 43 tensile and 35 fracture toughness tests were performed and the effects of various parameters such as pipe size, crack plane orientation, test temperature, welding on material properties were discussed. Test results show that the effects of crack plane orientation, test temperature, and welding on fracture toughness were significant while the effects of pipe size, specimen orientation and test temperature on tensile properties were negligible. Especially the dependence of J-R curves on the crack plane orientation appears to be the characteristics of carbon steel.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1992.11a
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• pp.97-101
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• 1992

Cordierite glass ceramic has become an electronic substrate material for electronic circuits and the use of whiskers for improving strength and toughness is evident. Green sheets of mixtures containing 15% silicon nitride were sintered to greater than 99 % density. The microstructure was analysed using optical microscopy, scanning electron microscopy (SEM), and X-ray diffraction (XRD). The toughness and hardness were improved with increasing the whisker vol. % and sintering temperature. Especially, it is assumed that toughening increasing at the more high sintering temperature relevants to the glass phase increasing, as showned in the roughness of the fracture surfaces. It was directionally dependent of whisker direction during processing.