• Title/Summary/Keyword: Material Measurements

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Measurement of High Temperature Dielectric Property at Microwave Frequency Using Cavity Perturbation Method (Cavity Perturbation Method를 이용한 마이크로파 주파수대의 고온 유전특성 측정 연구)

  • Kim, Dong-Eun;Jung, Jin-Ho;Lee, Sung-Min;Kim, Hyung-Tae
    • Journal of Powder Materials
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    • v.13 no.6 s.59
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    • pp.455-461
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    • 2006
  • High temperature dielectric constants of the various ceramic materials have been measured using cavity perturbation method. The measurements were applied to refractory, traditional and fine ceramic powder compacts from room temperature to $1200^{\circ}C$. Calibration constant in the equation suggested by Hutcheon et al., was determined from the dielectric constants of reference specimen (teflon and alumina) at room temperature. From these results, informations on the refectory materials were obtained for the microwave kiln design and understanding of the microwave heating effects of ceramics have been improved.

Measurements of Temperature Rise and Temperature Distribution of Samples by Infrared Radiation (적외선 복사에 의한 시료의 온도상승과 온도분포 측정)

  • Han, Jong-Sung;Kim, Ki-Hoon;Kim, Hoon
    • Proceedings of the Korean Institute of IIIuminating and Electrical Installation Engineers Conference
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    • 2003.11a
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    • pp.133-137
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    • 2003
  • When a light is projected upon a material, part of its radiation energy is absorbed and the rest is reflected or transmitted according to the nature of the material. The molecules of the substance absorbing a light obtains the radiation energy to the wavelength of the light to make photochemical degradation by ultraviolet ray or thermal reactions like physical damage by infrared ray. The degree of damage by radiation energy varies to the substances of materials, the spectral power distribution of the light source and the duration of irradiation. Because the damage brings about a devaluation of material and once damaged, it is irretrievable, it is necessary to minimize the damage and conserve the native quality of a material by a protective lighting system. A measuring system was set up to measure the temperature rise of each sample by infrared radiation from light sources. And the temperature rise and temperature distribution by various infrared lamps were measured with varying time.

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Identifiability of Ludwik's law parameters depending on the sample geometry via inverse identification procedure

  • Zaplatic, Andrija;Tomicevic, Zvonimir;Cakmak, Damjan;Hild, Francois
    • Coupled systems mechanics
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    • v.11 no.2
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    • pp.133-149
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    • 2022
  • The accurate prediction of elastoplasticity under prescribed workloads is essential in the optimization of engineering structures. Mechanical experiments are carried out with the goal of obtaining reliable sets of material parameters for a chosen constitutive law via inverse identification. In this work, two sample geometries made of high strength steel plates were evaluated to determine the optimal configuration for the identification of Ludwik's nonlinear isotropic hardening law. Finite element model updating(FEMU) was used to calibrate the material parameters. FEMU computes the parameter changes based on the Hessian matrix, and the sensitivity fields that report changes of computed fields with respect to material parameter changes. A sensitivity analysis was performed to determine the influence of the sample geometry on parameter identifiability. It was concluded that the sample with thinned gauge region with a large curvature radius provided more reliable material parameters.

Experimental Study on the Ultimate Strength of Composite Cylinders under Hydrostatic Pressure (수압을 받는 복합재 원통의 최종강도 실험 연구)

  • Cho, Sang-Rai;Koo, Jeong-Bon;Cho, Jong-Rae;Kwon, Jin-Hwe;Choi, Jin-Ho;Kim, Hyun-Su
    • Journal of Ocean Engineering and Technology
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    • v.21 no.3 s.76
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    • pp.52-57
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    • 2007
  • Composite material is one of the strongest candidates for deep see pressure hulls. Research regarding composite cylinders, subjected to hydrostatic pressure, has been ongoing for a couple of decades, abroad, but domestic research is very new. Experimental investigations seem necessary, in order to understand their structural behavior not only up to the ultimate limit state, but in the post-ultimate regime. That experimental information will be very helpful in the development of any theoretical methods or to substantiate any commercial numerical packages for structural analyses. In this study, ultimate strength tests on seven composite cylinders subjected to hydrostatic pressure are reported, which includes the fabrication method of models, mechanical properties of the material, initial shape imperfection measurements, test procedure, and strain and axial shortening measurements during the tests. The ultimate strengths of the models were compared with predictions of numerical analyses. The numerical predictions are higher than the test results. It seems necessary to improve the accuracy of the numerical predictions by considering the initial shape and material imperfections.

Experimental Study on the Ultimate Strength of Composite Cylinder under Hydrostatic Pressure (수압을 받는 복합재 원통의 최종강도 실험 연구)

  • Cho, Sang-Rai;Kim, Hyun-Su;Koo, Jeong-Bon;Cho, Jong-Rae;Kwon, Jin-Hwe;Choi, Jin-Ho
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2006.11a
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    • pp.154-157
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    • 2006
  • Composite material is one of the strong candidates for deep see pressure hulls. Research regarding composite unstiffened or stiffened cylinders subjected to hydrostatic pressure has a couple of decades history abroad but domestic research is very new. Experimental investigations seem necessary to understand their structural behavior not only up to the ultimate limit state but in post-ultimate regime. Those experimental information will be very helpful to develop any theoretical methods or to substantiate any commercial numerical packages for structural analyses. In this study, ultimate strength tests on seven composite cylinders subjected to hydrostatic pressure are reported, which includes the fabrication method of models, material properties of the material, initial shape imperfection measurements, test procedure and strain and axial shortening measurements during the tests. The ultimate strengths of the models were compared with those of numerical analyses. The numerical predictions are higher than the test results. It is necessary to improve the accuracy of the numerical predictions.

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Inverse model for pullout determination of steel fibers

  • Kozar, Ivica;Malic, Neira Toric;Rukavina, Tea
    • Coupled systems mechanics
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    • v.7 no.2
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    • pp.197-209
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    • 2018
  • Fiber-reinforced concrete (FRC) is a material with increasing application in civil engineering. Here it is assumed that the material consists of a great number of rather small fibers embedded into the concrete matrix. It would be advantageous to predict the mechanical properties of FRC using nondestructive testing; unfortunately, many testing methods for concrete are not applicable to FRC. In addition, design methods for FRC are either inaccurate or complicated. In three-point bending tests of FRC prisms, it has been observed that fiber reinforcement does not break but simply pulls out during specimen failure. Following that observation, this work is based on an assumption that the main components of a simple and rather accurate FRC model are mechanical properties of the concrete matrix and fiber pullout force. Properties of the concrete matrix could be determined from measurements on samples taken during concrete production, and fiber pullout force could be measured on samples with individual fibers embedded into concrete. However, there is no clear relationship between measurements on individual samples of concrete matrix with a single fiber and properties of the produced FRC. This work presents an inverse model for FRC that establishes a relation between parameters measured on individual material samples and properties of a structure made of the composite material. However, a deterministic relationship is clearly not possible since only a single beam specimen of 60 cm could easily contain over 100000 fibers. Our inverse model assumes that the probability density function of individual fiber properties is known, and that the global sample load-displacement curve is obtained from the experiment. Thus, each fiber is stochastically characterized and accordingly parameterized. A relationship between fiber parameters and global load-displacement response, the so-called forward model, is established. From the forward model, based on Levenberg-Marquardt procedure, the inverse model is formulated and successfully applied.

Synthesis of Polyamine Grafted Chitosan Copolymer and Evaluation of Its Corrosion Inhibition Performance

  • Li, Heping;Li, Hui;Liu, Yi;Huang, Xiaohua
    • Journal of the Korean Chemical Society
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    • v.59 no.2
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    • pp.142-147
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    • 2015
  • Two new chitosan derivatives, polyamine grafted chitosan copolymers have been synthesized for corrosion protection of carbon steel in acidic medium. First, methyl acrylate graft chitosan copolymer (CS-MAA) was prepared by the reaction of chitosan (CS) and methyl acrylate (MAA) via the Michael addition reaction. Then, CS-MAA was reacted with ethylene diamine (EN) and triethylene tetramine (TN) respectively to synthesize ethylene diamine grafted chitosan copolymer (CS-MAA-EN) and triethylene tetramine grafted chitosan copolymer (CS-MAA-TN), and the structures were characterized by Fourier-transform infrared spectroscopy (FT-IR). At last, the corrosion inhibition activities on Q235 carbon steel were investigated by using gravimetric measurements, metallographic microscope, potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) measurements. The compounds CS-MAA-EN and CS-MAA-TN show an appreciable corrosion inhibition property against corrosion of Q235 carbon steel in 5% HCl solution at $25^{\circ}C$. It has been observed that CS-MAA-EN shows greater corrosion inhibition efficiency than CS-MAA-TN. The inhibition efficiency of CS-MAA-EN was close to 90% when the mass fraction concentration was 0.2%~0.3%; the inhibition efficiency of CS-MAA-TN was close to 85% when the mass fraction concentration was 0.02%. The present work provided very promising results in the preparation of green corrosion inhibitors.

Accuracy and reliability of stitched cone-beam computed tomography images

  • Egbert, Nicholas;Cagna, David R.;Ahuja, Swati;Wicks, Russell A.
    • Imaging Science in Dentistry
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    • v.45 no.1
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    • pp.41-47
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    • 2015
  • Purpose: This study was performed to evaluate the linear distance accuracy and reliability of stitched small field of view (FOV) cone-beam computed tomography (CBCT) reconstructed images for the fabrication of implant surgical guides. Material and Methods: Three gutta percha points were fixed on the inferior border of a cadaveric mandible to serve as control reference points. Ten additional gutta percha points, representing fiduciary markers, were scattered on the buccal and lingual cortices at the level of the proposed complete denture flange. A digital caliper was used to measure the distance between the reference points and fiduciary markers, which represented the anatomic linear dimension. The mandible was scanned using small FOV CBCT, and the images were then reconstructed and stitched using the manufacturer's imaging software. The same measurements were then taken with the CBCT software. Results: The anatomic linear dimension measurements and stitched small FOV CBCT measurements were statistically evaluated for linear accuracy. The mean difference between the anatomic linear dimension measurements and the stitched small FOV CBCT measurements was found to be 0.34 mm with a 95% confidence interval of +0.24 - +0.44 mm and a mean standard deviation of 0.30 mm. The difference between the control and the stitched small FOV CBCT measurements was insignificant within the parameters defined by this study. Conclusion: The proven accuracy of stitched small FOV CBCT data sets may allow image-guided fabrication of implant surgical stents from such data sets.