• 제목/요약/키워드: Mass standards

검색결과 467건 처리시간 0.024초

자율주행 자동차 임시운행 허가를 위한 안전 성능 평가 시나리오 (An evaluation scenario of safety performance for extraordinary service permission of autonomous vehicle)

  • 정용환;이경수;최인성;민경찬
    • 자동차안전학회지
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    • 제7권2호
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    • pp.44-49
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    • 2015
  • This paper presents an evaluation scenario of safety performance for extraordinary service permission of autonomous vehicle driving on a motorway. Based on advanced driver assistance system (ADAS) which is already mass-production, an autonomous vehicle driving on motorway is tested on the public roads and also getting close to mass-production. Before the autonomous vehicle tested, the safety of autonomous driving system should be evaluated based on a proper test scenario. Prior to develop the test scenario, this paper reviews the licensing standards for an autonomous vehicle in California and Nevada, and the international regulations of each ADAS. To develop the scenario, the driving conditions of motorway are categorized into five modes and fundamental evaluation requirements of elements of autonomous driving system are derived. An evaluation scenario, which represents the real driving conditions, has been developed to assess the safety of autonomous vehicle. This scenario has validated by computer simulation using model predictive control (MPC) based autonomous driving algorithm.

유도결합 플라스마 질량분석법에 의한 모발의 다원소 분석 (Multi - elemental Analysis of Hair by Inductively Coupled Plasma/Mass Spectrometry)

  • 차명진;강준모;박창준
    • 분석과학
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    • 제15권4호
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    • pp.335-340
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    • 2002
  • 유도결합 플라스마 질량분석법 (ICP-MS)을 이용하여 모발 중 다원소 동시 정량법을 확립하였다. 0.05 g의 모발 시료에 내부표준물질인 In을 가하고 질산 1.5 mL와 함께 테플론 가압분해 용기에 넣어 마이크로파를 이용하여 분해하는 시료전처리법을 사용하였다. 측정값의 정확도 및 신뢰도를 확인하기 위하여 모발 인증표준물질인 GBW 09101을 반복 분석하였는데 측정값은 인증값과 불확도 범위 내에서 잘 일치하는 결과를 얻었다.

Determination of Li by Isotope Dilution Inductively Coupled Plasma Mass Spectrometry

  • Park, Chang J.;Chung, Bag S.
    • 분석과학
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    • 제8권4호
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    • pp.427-434
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    • 1995
  • Inductively coupled plasma mass spectrometry combined with the isotope dilution method is used for the determination of lithium. The isotope dilution method is based on the addition of a known amount of enriched isotope (spike) to a sample. The analyte concentration is obtained by measuring the altered isotope ratio. The spike solution is calibrated through so called reverse isotope dilution with a primary standard. The spike calibration is an important step to minimize error in the determined concentration. It has been found essential to add spike to a sample and the primary standard so that the two isotope ratios should be as dose as possible. Since lithium is neither corrosive nor toxic, lithium is used as a chemical tracer in the nuclear power plants to measure feedwater flow rate. 99.9% $^7Li$ was injected into a feedwater line of an experimental system and sample were taken downstream to be spiked with 95% $^6Li$ for the isotope dilution measurements. Effects of uncertainties in the spike enrichment and isotope ratio measurement error at various spike-to-sample ratios are presented together with the flow rate measurement results in comparison with a vortex flow meter.

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Accuracy of Body Mass Index-defined Obesity Status in US Firefighters

  • Jitnarin, Nattinee;Poston, Walker S.C.;Haddock, Christopher K.;Jahnke, Sara A.;Day, Rena S.
    • Safety and Health at Work
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    • 제5권3호
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    • pp.161-164
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    • 2014
  • Obesity is a significant problem affecting United States (US) firefighters. While body mass index (BMI) is widely used to diagnose obesity, its use for this occupational group has raised concerns about validity. We examined rates and types of misclassification of BMI-based obesity status compared to body fat percentage (BF%) and waist circumference (WC). Male career firefighters (N = 994) from 20 US departments completed all three body composition assessments. Mean BMI, BF%, and WC were $29kg/m^2$, 23%, and 97 cm, respectively. Approximately 33% and 15% of BF%- and WC-defined obese participants were misclassified as non-obese (false negatives) using BMI, while 8% and 9% of non-obese participants defined by BF% and WC standards were identified as obese (false positives) using BMI. When stratified by race/ethnicity, Pacific Islanders showed high rates of false positive misclassification. Precision in obesity classification would be improved by using WC along with BMI to determine firefighters' weight status.

가스크로마토그래피-이온트랩질량분석법을 이용한 하수슬러지 중 다핵방향족탄화수소(PAHs) 함량 분석 (The Quantitative Analysis of Polycyclic Aromatic Hydrocarbons(PAHs) in Sewage Sludge by Gas Chromatography-Ion Trap Mass Spectrometry)

  • 남재작;소규호;박우균;조남준;이상학
    • 한국환경과학회지
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    • 제11권4호
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    • pp.367-373
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    • 2002
  • The polycyclic aromatic hydrocarbons(PAHs) content in sewage sludge was determined by gas chromatography linked to ion trap mass spectrometry(GC/ITMS) with five deuterated PAHs as internal standards. The minimum detection limit was from 1.66 to 7.14 pg for individual PAH by GC/ITMS. For determining total PAHs(∑PAH) in sewage sludge 84 samples from 74 waste water treatment plants in whole country were analyzed. The average content of ∑PAH far whole samples was 3,289$\pm$3,098 $\mu\textrm{g}$/kg, and ranged from 142 to maximum 20,102 $\mu\textrm{g}$/kg. According to the number of population of the city, the areas were classified as five regions, ie. big, large, middle, small, and rural area in which the waste water treated plants were grown. The contents of PAHs were 4,689$\pm$5,503, 5,839$\pm$6,401, 3,725$\pm$2,053, 2,237$\pm$2,069, and 2,475$\pm$1,489 $\mu\textrm{g}$/kg, in big, large, middle, small, and rural area, respectively.

Fragmentations and Proton Transfer Reactions of Product Ions Formed from Mono-, Di-, and Triethanolamines

  • Choi, Sung-Seen;So, Hun-Young
    • Bulletin of the Korean Chemical Society
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    • 제25권10호
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    • pp.1538-1544
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    • 2004
  • Fragmentations and proton transfer reactions of mono-, di-, and triethanolamines were studied using FTMS. It was found that the most abundant fragment ion was $[M-CH_2OH]^+$. The $[M-CH_2OH-H_2O]^+$ was observed in the mass spectra of diethanolamine and triethanolamine. By increasing the ion trapping time in the ICR cell, the $[M+H]^+$ and $[M+H-H_2O]^+$ ions were notably increased for all the samples while the $[M+H-2H_2O]^+$ was observed in the mass spectra of diethanolamine and triethanolamine. The proton transfer reactions between the fragment ions and neutral molecules occurred predominantly by increasing the ion trapping time. The rate constants for the proton transfer reactions were calculated from experimental results. The proton transfer reaction of $CHO^+$ was the fastest one, which is consistent with the heats of reaction. The rate constants for proton transfer reactions of triethanolamine were much slower than those of ethanolamine and diethanolamine because of the steric hindered structure of triethanolamine. The plausible structures of observed ions and heats of reaction for proton transfer were calculated with AM1 semiempirical method.

도로터널 굴착공사의 적정공기 판단기준 (Optimum Construction Duration for Road Tunnel Excavation Works)

  • 김하나;김대영;김대영;정성춘;허영기
    • 대한건축학회논문집:구조계
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    • 제34권4호
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    • pp.59-64
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    • 2018
  • Construction schedule acceleration due to unreasonable construction planning frequently leads to construction accidents. In order to avoid such inevitable acceleration and to ensure safety in construction sites, there is a need for objective standards to determine appropriate construction duration for each construction process earlier in the process. In order to achieve the goal, intensive experts interviews were firstly conducted to identify candidate drivers affecting construction schedule of road tunnel excavation works. Then, a total of 34 field data was collected from on-going sites to analyze. It was found that actual excavation length per one day on site is varied mostly by Rock Mass Rating(RMR) types from various statistical analyses. Therefore an one-way table of excavation length per a day by RMR types were presented in a form of percentile. The results will help industry experts determine the most appropriate construction schedule for the works, which eventually lead to a zero accident site in many ways.

Optimization of Ceramide Analysis Method Using LC-MS in Cosmetics

  • Su-Jin Park;Hee-Jin Yoo;Duck-Hyun Kim;Ji-Won Park;Eunji Jeon;Abhik Mojumdar;Kun Cho
    • Mass Spectrometry Letters
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    • 제15권1호
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    • pp.49-53
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    • 2024
  • Ceramide is a lipid in which sphingoid bases and fatty acids are linked by amide bonds. As a marker of skin disease in the human stratum corneum, its disease-causing and therapeutic effects have been partially confirmed, and it is therefore an important element in commercially available cosmetic formulations. However, structural diversity caused by differences in the chain length, number, and location of hydroxyl groups makes quality control difficult. In this study, a method was established to separate different ceramide species using reversed-phase LC-MS/MS and thus enable qualitative evaluation. Separation of four standards was achieved within a short retention time, and the accuracy and sensitivity of the method were demonstrated by the low limit of detection (LOD) calculated based on the calibration curve showing linearity, with R2 > 0.994. After verification of reproducibility and reliability through intra- and inter-day analyses, the efficiency of the method was confirmed through analysis of commercial cosmetic raw materials.

다변량 판별분석을 통한 터널 설계시의 암반분류 연구 (A study on rock mass classification in the design of tunnel using multivariate discriminant analysis)

  • 이송;안태훈;유오식
    • 한국터널지하공간학회 논문집
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    • 제6권3호
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    • pp.237-245
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    • 2004
  • 터널의 설계에 있어서 RMR 분류방법은 암반을 분류하고 암반등급에 따른 지보패턴을 결정하기 위하여 널리 사용하여 왔다. 하지만 이러한 RMR 분류방법은 현장상태를 고려하여야만 구할 수 있는 변수들을 사용하고 암반을 분류하는 기술자의 경험적 판단에 의존될 수 밖에 없다. RMR 암반분류 방법을 설계단계에서 활용할 때 RMR의 평가요소들을 모두 고려하는 것은 실무적으로 불가능하다. 따라서 설계시 정량적인 요소만을 사용하여 RMR 분류 가능성을 확인하기 위하여 판별분석을 수행하였다. 정량적 데이터인 암석강도 혹은 RQD는 RMR 값과의 상관계수가 높으며, 기존 암반분류기준을 살펴볼 때 암석강도와 RQD는 암반분류를 위한 중요한 요소이다. 기존의 RMR 암반분류 방법을 통한 암반분류와 두 가지 변수만을 고려한 판별분석을 수행한 암반분류 결과 암석강도를 독립변수로 사용한 판별분석시 74.8%, RQD를 독립변수로 사용한 판별분석시 74.3%의 정확도로 RMR 암반분류가 가능하였다. 암석강도와 RQD를 함께 고려한 판별분석을 하였을 때 82.5%의 정확도로 RMR 암반분류가 가능하였다. 기존의 사례분석에서 RMR 전체 요소를 통하여 수행된 설계단계의 전체 적중률은 40.3% 정도 수준임을 감안할 때 설계단계에서는 암석강도와 RQD 만으로도 충분한 RMR 암반분류가 가능할 것이다.

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소아 핵의학 검사 시 사용되는 방사성의약품의 양 산출 기준 조사 (A Research of Standards for Radiopharmaceutical Doses in Pediatric Nuclear Medicine)

  • 도용호;김계환;이홍재;김진의;김현주
    • 핵의학기술
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    • 제13권1호
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    • pp.47-50
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    • 2009
  • 목적 : 현재 소아 핵의학 검사 시 사용되는 방사성의약품 선량 산출 기준은 확립되어있지 않다. 그리하여 병원들은 몸무게 기준 산출 공식(mCi/kg), 체표면적 시준 산출 공식(mCi/$m^2$) 또는 미국, 유럽, IAEA의 선량 산출 공식 등 다양한 선량 기준을 따르고 있다. 그러나 이러한 선량 산출 공식들은 1세 이하의 영아나 50 kg 이상의 어린이들에 대한 정확한 선량을 산출하는데 어려움을 격고 있으므로 국내의 선량기준을 조사하여 이를 미국, 유럽, IAEA의 기준에 비교하고 각 기준의 문제점을 비교여 적절한 선량 기준의 확립을 권고 하고자 본 논문을 시행하게 되었다. 실험재료 및 방법: 객관적인 정보의 획득을 위하여 소아핵의학 검사를 가장 많이 시행하는 국내 4개 대학병원을 선정하여 설문을 실시하였으며 이에 대한 답변을 기초로 각 몸무게 당 사용되는 방사성의약품의 양을 multiplier로 변환하여 이를 미국, 유럽, IAEA의 multiplier와 비교하였다. 결과: 국민 대부분의 병원들은 몸무게 기준 산출 공식을 이용하여 소아 핵의학 검사 시 사용되는 방사성의약품의 양을 산출하고 있었으며 1세 이하의 영아와 50 kg 이상 어린이에 대한 과소량, 과잉량 투여 문제는 고려되고 있지 않은 것으로 나타났다. 결론 및 고찰: 본 논문을 통하여 대한민국의 기준을 비롯한 여러 기준들은 소아 핵의학 검사 시 적정한 선량 산출에 어려움을 겪고 있는 것으로 나타났다. 그러므로 성공적인 검사가 가능한 최소의 선량으로 방사선 피폭을 최소화 하는 세계적으로 인정된 선량 체계를 확립하여야 할 것이다. 또한 보다 우수한 영상 재구성 프로그램의 개발을 통하여 검사 시간을 단축함과 동시에 보다 나은 영상 구현을 실현하여야 할 것이다.

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