• Title/Summary/Keyword: Mass spectroscopy

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Volatile Compounds Characterizing the Flavor of Korean Horseradish Roots (한국산(韓國産) Horseradish 뿌리의 휘발성 풍미 성분)

  • Kim, In-Sook;Kimlee, Mie-Soon
    • Journal of Nutrition and Health
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    • v.18 no.4
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    • pp.293-300
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    • 1985
  • Volatile components of Korean horseradish roots harvested at different dates were prepared by steam distillation. Samples were examined by gas chromatography (GC) and combined gas chromatography-mass spectrometry (GC-MS). The major pungent constituent, allyl isothiocyanate was confirmed add tended to increase with delayed harvest time. Pungent principles also included allyl thiocyanate, 2-phenethyl, 2-butyl, 4- pentenyl, benzyl and 3-methylthiopropyl isothiocyanates. Infrared (IR) spectroscopy study showed that allyl isothiocyanate - thiocyanate interconversion did not occur under the condition of this study.

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Study on Electrical Activation of As Ion Implanted Si(100) (As 이온이 주입된 단결정 실리콘(100)의 전기적 활성화 연구)

  • 이동건;문영희;손정식;손정식;김동렬;배인호;김말문;한병국;정광화
    • Journal of the Korean Vacuum Society
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    • v.4 no.1
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    • pp.104-108
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    • 1995
  • Hall 효과 측정을 이용하여 As+이 주입된 다결정 실리콘의 열처리 조건에 따른 활성화 과정을 연구하였다. 주입된 이온의 농도 분포는 SIMS(Secondary Ion Mass Spectroscopy)와 SUPREMIV 모의 실험으로 조사하였다. 열처리 온도가 증가함에 따라 활성층의 전자 면 농도 증가가 뚜렷이 나타났으며, Hall 이동도의 온도 의존성 측정으로 주입된 도우즈에 따라 이온 주입층의 활성화에 필요한 열처리 온도가 달라져야함을 알 수 있었다. 그리고, 접합 손실전류의 감소는 $800^{\circ}C$(30분)의 열처리에서 현저하게 나타났다.

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One Pot Synthesis of Bioactive Novel Cyanopyridones

  • Khokhani, Kamlesh;Khatri, Taslimahemad;Patel, Praful
    • Journal of the Korean Chemical Society
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    • v.57 no.4
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    • pp.476-482
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    • 2013
  • Cyanopyridone was prepared by the condensation of cyanoacetamide, substituted arylaldehydes and malononitrile in presence of pipyridine. The structure of the synthesized compound CP 1-20 was assigned on the basis of elemental analysis, IR, $^1H$-NMR and mass spectroscopy. These compounds were also screened for antimicrobial activity. The Minimum Inhibitory Concentration (MIC) of all the synthesized compounds was compared with standard drugs.

Fermi Velocity Renormalization in Graphene

  • Hwang, Choongyu;Siegel, David A.;Lanzara, Alessandra
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.163.1-163.1
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    • 2014
  • Electron-electron interactions bear important information on fundamental electronic properties such as electron effective mass, conductivity, and charge mobility. By using angle-resolved photoemission spectroscopy, here we address unusual electron self-energy in graphene induced by the electron-electron interactions, which are distinguished from those of an ordinary Fermi liquid. Our findings provide a new route for two-dimensional electron systems toward device applications.

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1-D and 2-D Metal Oxide Nanostructures

  • Son, Yeong-Gu
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.87-88
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    • 2012
  • Metal oxide nanostructures have been applied to various fields such as energy, catalysts and electronics. We have freely designed one and two-dimensional (1 and 2-D) metal (transition metals and lanthanides) oxide nanostructures, characterized them using various techniques including scanning electron microscopy, transmission electron microscopy, X-ray diffraction crystallography, thermogravimetric analysis, FT-IR, UV-visible-NIR absorption, Raman, photoluminescence, X-ray photoelectron spectroscopy, and temperature-programmed thermal desorption (reaction) mass spectrometry. In addition, Ag- and Au-doped metal oxides will be discussed in this talk.

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Characteristics of Products in the Reaction 40 MeV/nucleon $^{14}N+Ag$

  • Chung, Yong-Hee;Porile, N. T.
    • Bulletin of the Korean Chemical Society
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    • v.15 no.11
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    • pp.971-975
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    • 1994
  • Cross sections and recoil properties have been measured for the fragments produced in the interaction of silver with 40 MeV/nucleon $^{14}N$ ions using off-line ${\gamma}$-ray spectroscopy. The data were used to obtain the isobaric-yield distribution, the mass yield distribution, and the fractional momentum transfer. The values of forward-to-backward ratios were measured to be very large, indicating that substantial momentum transfer occurs at this energy regime. The results are compared with other studies of the interaction of silver with intermediate-energy heavy ions.

A New Guaiane type Sesquiterpene from Torilis japonica

  • Ryu, Jae-Ha;Jeong, Yeon-Su
    • Archives of Pharmacal Research
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    • v.24 no.6
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    • pp.532-535
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    • 2001
  • A new guaiane type sesquiterpene was isolated from the fruit of Torilis japonica (Umbelliferae). Based on NMR, IR and mass spectroscopy its structure was confirmed as deangeloyloxy torilin, $1{\beta},{\;}7{\alpha},{\;}10{\alpha}$H-11-acetoxy-guaia-4-en-3-one (1). This is the first report showing that this compound can be isolated from Torilis japonica.

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