• Journal of Conservation Science
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• v.37 no.5
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• pp.525-535
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• 2021

This study identified material properties through scientific analysis on Jikgeumdan(satin with gold threads) from Donggungbi-Wonsam and the gold threads used in the embroidery. The Donggungbi-Wonsam's base of gold threads were estimated to have used mulberry fiber's Korean paper(Hanji) because non-wood-based fibers were observed. The X-ray spectrometer showed that the Tongsuseulan of Donggungbi-Wonsam was a flat gold thread of pure gold and Jikgeumdan of flat silver thread of its Saekdong and Hansam. High sulfur levels were detected in the flat silver thread, which appeared to have formed silver sulfide by either manufacturing process using sulfur or conservation environment. he dragon insignia's embroidery is also described as two types twisted gold threads; pure gold and alloying-gold and silver. while dragon insignia's border line is decorated with a twisted gold thread of pure gold. In particular, it was investigated that adhesives such as an animal glue, a protein-based compound by gas chromatography mass spectrometry. Additionally, XRF and Raman spectroscopy analysis on the mixture substances between the metal surface and the base paper of gold threads identified talc and quartz in the gold threads and Seokganju(hematite) in the flat silver threads.

• Atmosphere
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• v.31 no.3
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• pp.267-282
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• 2021

Characteristics of carbonaceous components and organic compounds in PM_2.5 over the atmosphere of the Yellow Sea were investigated. PM_2.5 samples were collected onboard the meteorological research vessel, GISANG 1, over the Yellow Sea during the YES-AQ campaign in 2018 and 2019, respectively. The average concentrations of carbonaceous components in this region were 2.59 ± 1.59 ㎍ m^-3 for the OC, 0.24 ± 0.10 ㎍ m^-3 for the EC, 2.14 ± 1.30 ㎍ m^-3 for the WSOC and 1.17 ± 0.94 ㎍ m^-3 for the HULIS-C, respectively. The total concentration of 56 organic compounds (ΣOCs) accounts for 10% of OC. The main group among organic compounds were dicarboxylic acids which account for 57% of ΣOCs, followed by n-alkanoic acids accounting for 34% of ΣOCs. In n-alkanoic acid distribution, hexanoic (C_6:0) and octanoic (C_8:0) acids which are low molecular weight n-alkanoic acids and known as emitted from marine biogenic activities were dominant in this region. Furthermore, non-HULIS-C fraction increased when the air mass originated from the marine region rather than the continental region. When the Asian dust episode was observed, the WISOC concentrations along with the levoglucosan were increased, while the haze episodes caused the increase of WSOC, HULIC-S and DCAs. In this study, we found that the components of carbonaceous and organic aerosols in PM_2.5 over the Yellow Sea were changed with the specific air pollution episodes. It indicates that the physicochemical properties of PM_2.5 can be changed by the air pollution episodes in this region.

• Korean Journal of Materials Research
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• v.28 no.12
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• pp.732-737
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• 2018

We develop a purification process of $Hg_2Br_2$ raw powders using a physical vapor transport(PVT) process, which is essential for the fabrication of a high performance acousto-optic tunable filter(AOTF) module. Specifically, we characterize and compare three $Hg_2Br_2$ powders: $Hg_2Br_2$ raw powder, $Hg_2Br_2$ powder purified under pumping conditions, and $Hg_2Br_2$ powder purified under vacuum sealing. Before and after purification, we characterize the powder samples through X-ray diffraction and X-ray photoelectron spectroscopy. The corresponding results indicate that physical properties of the $Hg_2Br_2$ compound are not damaged even after the purification process. The impurities and concentration in the purified $Hg_2Br_2$ powder are evaluated by inductively coupled plasma-mass spectroscopy. Notably, compared to the sample purified under pumping conditions, the purification process under vacuum sealing results in a higher purity $Hg_2Br_2$ (99.999 %). In addition, when the second vacuum sealing purification process is performed, the remaining impurities are almost removed, giving rise to $Hg_2Br_2$ with ultra-high purity. This high purification process might be possible due to independent control of impurities and $Hg_2Br_2$ materials under the optimized vacuum sealing. Preparation of such a highly purified $Hg_2Br_2$ materials will pave a promising way toward a high-quality $Hg_2Br_2$ single crystal and then high performance AOTF modules.

• Journal of the Korea institute for structural maintenance and inspection
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• v.23 no.4
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• pp.113-119
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• 2019

Many researches on alternative materials as construction materials is continuing by recycling industrial byproducts due to shortage of sitereclamation and natural aggregates. In this paper, engineering properties in early-aged OPC (Ordinary Portland Cement) and GGBFS (Ground Granulated Blast Furnace Slag) concrete are evaluated with EOS aggregate replacement. The related experiments were carried out with 0.6 of water to binder ratio, three levels of EOS replacement ratios (0%, 30% and 50%) for fine aggregate, and two levels of cement replacement with GGBFS (0% and 40%). Several tests such as slump air content, and unit mass measurement are performed for fresh concrete, and compressive strength and diffusion coefficient referred to NT BUILD 492 method are measured for hardened concrete. Through the tests, it was evaluated that the compressive strength in concrete with EOS aggregate increased to 3 days and 7 days but slightly decreased at the age of 28 days. In the accelerated chloride penetration test, GGBFS concrete showed reduced diffusion coefficients by 60 - 67% compared with OPC concrete. The lowest chloride diffusion coefficient was evaluated in the 50% replacement with EOS aggregate, which showed an applicability of EOS aggregate to concrete production.

• The Journal of Engineering Geology
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• v.29 no.2
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• pp.123-136
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• 2019

This study examines the effect of collector well installed to reduce groundwater level in the regions with the occurrence of landcreep, a soil mass movement triggered by instability on slopes. Slopes are prone to failure as a result of instability caused by its internal, topographic and geological properties as well as due to external factors such as rainfall and earthquake. In Korea during the rain season, rainfall infiltration affects the groundwater level in soil, building up porewater pressure and load, and finally drives slopes to collapse. Slope failure caused by rainfall infiltration has been leading to a drastic forest degradation. The studied slope is located adjacent to a valley, its terrain corresponds to piedmont gentle slope, while the upper part of the failure surface is steep. After reinforcing the terrain where landcreep had occurred and installing collector well on the slope, we measured the changes in the groundwater level. In order to analyze the relationship between the well and the slope, we calculated the ratio of groundwater level to rainfall before and after the installation of the collector well. As a result, it is confirmed that the ratio increases after the installation of the well, which in turn reduces the groundwater level. Analysis of the change in groundwater level after 3, 7, 15 days antecedent rainfall showed that the higher the overall groundwater level, the less the value ($r_p$) of groundwater level-rainfall ratio is, while the value becomes relatively greater when the groundwater level is low. In particular, if a slope has a large catchment basin as is in the case of the studied site, antecedent rainfall affects groundwater level in the order of 3 < 7 < 15 days.

• Korean Journal of Heritage: History & Science
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• v.48 no.1
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• pp.148-165
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• 2015

Iron was one of the most influential factors for formation and development of ancient countries. The diffusion of ironware had increased agricultural productivity and brought about military technical revolution. Needless to say, the rise and fall of the countries depended on the possession of stable iron production. Raw materials and fuels are the key factors for mass production of iron and a transportation route is essential to supply the goods. Jungwon area satisfies the three factors. There are many iron manufacture sites such as Jincheon Seokjang-ri Gusan-ri, and Chunju Chilgeum-dong Tangeumdae earthen ramparts in the Jungwon area. In order to study the ancient iron manufacture technique, reconstitution experiment was carried out using restored furnace which was made based on the Jincheon Seokjang-ri B-23 furnace. Some notable results were identified with the experiment as in the followings. Firstly, a roasting process has a connection with the decrease of hardness of the iron ore. Secondly, melting of the blast pipe as well as the formation of product within the furnace had a crucial effect on the cessation of the experiment. Thirdly, reduced iron in various locations within the furnace prove that there was enough reducing environment during the working. Not only melting point but also properties of iron can vary depending on the carbon contents. For the reason, formation of approximate environment in which iron can react to the chalcoal is the most important factor in terms of iron manufacture.

• Korean Chemical Engineering Research
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• v.57 no.5
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• pp.611-619
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• 2019

This study was carried out to investigate fuel decomposition characteristics and coke formation according to types of endothermic fuels and methods of catalyst molding. Methylcyclohexane (MCH), n-dodecane, and exo-tetrahydrodipentadiene (exo-THDCP) were used as the endothermic fuels. As a catalyst, USY720 supported with platinum was used. It was manufactured by only using pressure to disk-type, or pelletized with a binder and a silica solution. The characteristics of the catalysts according to the molding method were analyzed by X-ray diffraction analysis, scanning electron microscopy, nitrogen adsorption-desorption isotherm, and ammonia temperature programmed desorption analysis. The reaction was carried out under conditions of high temperature and high pressure ($500^{\circ}C$, 50 bar) in which the fuel could exist in a supercritical state. The product was analyzed by gas chromatograph/mass spectrometer and the coke produced by the catalyst was analyzed by thermogravimetric analyzer. After the reaction, the composition of the products varied greatly depending on the structure of the fuel. In addition, the crystallinity and surface properties of the catalysts were not changed by the method of catalyst molding, but the changes of the acid sites and the pore characteristics were observed, which resulted in changes in the amount and composition of products and coke.

• Journal of Korean Tunnelling and Underground Space Association
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• v.21 no.3
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• pp.347-362
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• 2019

Underground excavation using TBM machines has been increasing to reduce complaints caused by noise, vibration, and traffic congestion resulted from the urban underground construction in Korea. However, TBM excavation design and construction still need improvement because those are based on standards of the technologically advanced countries (e.g., Japan, Germany) that do not consider geological environment in Korea at all. Above all, although TBM performance is a main factor determining the TBM machine type, duration and cost of the construction, it is estimated by only using UCS (uniaxial compressive strength) as the ground parameters and it often does not match the actual field conditions. This study was carried out as part of efforts to predict penetration rate suitable for Korean ground conditions. The effective parameters were defined through the correlation analysis between the penetration rate and the geotechnical parameters or TBM performance parameters. The effective parameters were then used as variables of the multiple regression analysis to derive a regression model for predicting TBM penetration rate. As a result, the regression model was estimated by UCS and joint spacing and showed a good agreement with field penetration rate measured during TBM excavation. However, when this model was applied to another site in Korea, the prediction accuracy was slightly reduced. Therefore, in order to overcome the limitation of the regression model, further studies are required to obtain a generalized prediction model which is not restricted by the field conditions.

• Journal of Adhesion and Interface
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• v.22 no.2
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• pp.63-68
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• 2021

Unsaturated Polyester Resin (UPR) is in general used as a resin to prepare for composite materials with reinforcing materials such as glass fibers. UPR, a thermosetting resin, is used in industry to prepare for sheet molding compound (SMC) molding prepreg that has excellent productivity and is advantageous for mass production among various molding methods of composite materials. The fiber-reinforced composite material using UPR as a matrix material is light and has the advantage of excellent physical properties, but it is weak against impact and is fragile. Four types of polyurethane were synthesized and added to UPR resin to overcome the shortcomings.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.22 no.1
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• pp.372-378
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• 2021

A body armor vest is a form of munition related directly to the safety and life of combatants. Therefore, it must meet the requirements for ballistic resistance. The ROK demands the performance of body armor vest meet the Level IIIA specified by the NIJ STD-0101.06 published by the US National Institute of Justice. This study performed acceptance tests on body armor vests. The factors for evaluating the ballistic resistance evaluated were not only whether it penetrates when shooting but also whether the BFS (Backface Signature) depth does not exceed 44 mm when it does not penetrate. The factors were assessed to determine if they were consistent or not. The BFS depth is affected by various test factors, such as the physical properties of the backing material and the changes in the amount of impact with the bullet velocity. In this study, an analysis of the bulletproof performance was performed by extracting the data with the same conditions using ANOVA to remove the influence of these external factors. The analysis revealed a correlation between the BFS depth, bullet velocity, vest conditions, and protection area. The mass production process was analyzed by estimating the Interval of BFS on each lot. Through this, a new methodology for ballistic resistance evaluation and paradigm for future quality assurance is suggested.