• Title/Summary/Keyword: Magnetization Technique

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Development of High-Sensitivity Cantilever-Detected ESR Measurement Using a Fiber-Optic Interferometer

  • Tokuda, Yuki;Tsubokura, Daichi;Ohmichi, Eiji;Ohta, Hitoshi
    • Journal of Magnetics
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    • v.18 no.2
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    • pp.173-177
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    • 2013
  • Cantilever-detected high-frequency electron spin resonance (ESR) is a powerful method of sub-terahertz and terahertz ESR spectroscopy for a tiny magnetic sample at low temperature. In this technique, a small magnetization change associated with ESR transition is detected as deflection of a sample-mounted cantilever. So far, we have succeeded in ESR detection at 370 GHz using a commercial piezoresistive microcantilever. The spin sensitivity was estimated to ${\sim}10^{12}$ spins/gauss. In order to further increase the sensitivity, we adopt a fiber-optic-based detection system using a Fabry-Perot interferometer in place of piezoresistive system. Fabry-Perot cavity is formed between an optical-fiber end and microcantilever surface, and a change in the interference signal, corresponding to the cantilever deflection, is sensitively detected. This system is suitable for low-temperature and high-magnetic-field experiments because of its compact setup and less heat dissipation. In this study, performance of Fabry-Perot interferometer is evaluated, and its application to cantilever-detected ESR measurement is described.

SWR as Tool for Determination of the Surface Magnetic Anisotropy Energy Constant

  • Maksymowicz, L.J.;Lubecka, M.;Jablonski, R.
    • Journal of Magnetics
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    • v.3 no.4
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    • pp.105-111
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    • 1998
  • The low energy excitations of spin waves (SWR) in thin films can be used for determination of the surface anisotropy constant and the nonhomogeneities of magnetization in the close-to-surface layer. The dispersion relation in SWR is sensitive on the geometry of experiment. We report on temperature dependence of surface magnetic anisotropy energy constant in magnetic semiconductor thin films of$ CdCr_{2-2x}In_{2x}Se_4$ at spin glass state. Samples were deposited by rf sputtering technique on Corning glass substrate in controlled temperature conditions. Coexistence of the infinite ferromagnetic network (IFN) and finite spin slusters (FSC) in spin glass state (SG) is know phenomena. Some behavior typical for long range magnetic ordering is expected in samples at SG state. The spin wave resonance experiment (microwave spectrometer at X-band) with excited surface modes was applied to describe the energy state of surface spins. We determined the surface magnetic anisotropy energy constant versus temperature using the surface inhomogeneities model of magnetic thin films. It was found that two components contribute to the surface magnetic anisotropy energy. One originates from the exchange interaction term due to the lack of translation symmetry for surface spin as well as from the originates from the exchange interaction term due to the lack of translation symmetry for surface spin as well as from the stray field of the surface roughness. The second one comes from the demagnetizing field of close-to surface layer with grad M. Both term linearly decrease when temperature is increased from 5 to 123 K, but dominant contribution is from the first component.

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Design of Self Magnetization MsS Sensor Using Crossed Coils (Crossed-Coils를 이용한 자기자화 MsS센서의 설계)

  • Kim, Yi-Gon;Park, Kyung-Jo;Moon, Hong-Sik;Kim, Jae-Hyun;Ahn, Hyun-Jin;Kang, Woo-Seok;Oh, Un-Kyung
    • Journal of the Korean Institute of Intelligent Systems
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    • v.18 no.6
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    • pp.856-862
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    • 2008
  • This paper propose a advanced technique for exciting and receiving the guided torsional wave to detect flaws in pipe systems. There are some difficulties in selecting and exciting of modes by using the nickel strip attached on pipe systems, such as qualification of residual magnetic field and multi-exciting of the unwanted modes etc. In order to there difficulties we propose the new sensor, so called Crossed-coils sensor. We will prove that it is possible to select the modes to be excited and to find a optimal excitation condition for torsional mode by using the proposed sensor.

Effect of Boron Additions on Glass Formation and Magnetic Properties of Fe-Co-Ti-Zr-B Amorphous Ribbons

  • Kim, Sumin;Han, Bo Kyeong;Choi-Yim, Haein
    • Journal of Magnetics
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    • v.21 no.2
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    • pp.164-167
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    • 2016
  • The effect of the B additions on glass formation and magnetic properties is reported for the $Fe_{(87-x-y)}Co_yTi_7Zr_6B_x$ (x = 2, 4, 6 and y = 35, 40) alloy system. The ribbon samples with the width of 2 mm for each composition were prepared by the melt spinning technique; furthermore, their phase information was obtained from X-ray diffraction. Glass formation and magnetic properties were measured using differential scanning calorimetry and vibrating sample magnetometer respectively. The $Fe_{45}Co_{40}Ti_7Zr_6B_2$ (x = 2 and y = 40) system has the nanocrystalline phase identified as ${\alpha}-Fe$, as well as the amorphous phase, whereas all other alloys are fully amorphous. It is associated with the role of B on the glass formation. The widest supercooled liquid region is obtained as 71 K at x = 4 (both y = 35 and 40). The saturation magnetization decreases with the increase of the amount of the B addition, and the highest value is 1.59 T as x = 2 and y = 35 for this alloy system.

High Frequency Properties of Patterned Fe-Al-O Thin Films

  • N.D. Ha;Park, B.C.;B.K. Min;Kim, C.G.;Kim, C.O.
    • Proceedings of the Korean Magnestics Society Conference
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    • 2003.06a
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    • pp.194-194
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    • 2003
  • As a result of the recent miniaturization an enhancement in the performance of thin film inductors and thin film transformers, there are increased demands for the thin films with high magnetic permeability in the high frequency range, high saturation magnetization, in high electrical resistivity, and low coercive force. In order to improve high frequency properties, we will investigate anisotropy field by shape and size of pattern. The Fe-Al-O thin films of 16mm and 1 $\mu\textrm{m}$ thickness were deposited on Si wafer, using RF magnetron reactive sputtering technique with the mixture of argon and oxygen gases. The fabricating conditions are obtained in the working partial pressure of 2mTorr, O$_2$ partial pressure of 5%, input power of 400W, and Al pellets on an Fe disk with purity of 99,9%. Magnetic properties of the continuous films as followed: the 4$\pi$M$\_$s/ of 19.4kG, H$\_$c/ of 0.6Oe, H$\_$k/ of 6.0Oe and effective permeability of 2500 up to 100㎒ were obtained. In this work, we expect to enhance effect of magnetic anisotropy on patterned of Fe-Al-O thin films.

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Imaging Magnetic Flux Leakage based Steel Plate Damage for Steel Structure Diagnosis (강구조물 진단을 위한 누설자속 기반 강판 손상의 이미지화)

  • Kim, Hansun;Kim, Ju-Won;Yu, Byoungjoon;Kim, Wonkyu;Park, Seunghee
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.23 no.7
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    • pp.129-136
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    • 2019
  • In this study, the magnetic flux leakage technique was applied to diagnose steel plate damage, imaging technique was applied through those signals. Steel plate specimens with different thicknesses were prepared for the imaging the magnetic flux leakage signal, and 6 different depths of damage were artificially processed at the same locations on each specimen. The sensor head consist hall sensor and magnetization yoke was fabricated to magnetize the steel plate specimen and measure the magnetic flux leakage signal. In order to remove the noise and increase the resolution of the image in the signal collected from the hall sensor, various of signal processing was performed. P-P value was analyzed for each channel to analyze the magnetic flux leakage signals measured from each damaged part. Based on the above processed signals and analysis, it was converted into heatmap image. Through this, it was possible to identify the damage on the steel plate at glance by imaging magnetic flux leakage signal.

Alternating Acquisition Technique for Quantification of in vitro Hyperpolarized [1-13C] Pyruvate Metabolism

  • Yang, Seungwook;Lee, Joonsung;Joe, Eunhae;Lee, Hansol;Song, Ho-Taek;Kim, Dong-Hyun
    • Investigative Magnetic Resonance Imaging
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    • v.20 no.1
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    • pp.53-60
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    • 2016
  • Purpose: To develop a technique for quantifying the $^{13}C$-metabolites by performing frequency-selective hyperpolarized $^{13}C$ magnetic resonance spectroscopy (MRS) in vitro which combines simple spectrally-selective excitation with spectrally interleaved acquisition. Methods: Numerical simulations were performed with varying noise level and $K_p$ values to compare the quantification accuracies of the proposed and the conventional methods. For in vitro experiments, a spectrally-selective excitation scheme was enabled by narrow-band radiofrequency (RF) excitation pulse implemented into a free-induction decay chemical shift imaging (FIDCSI) sequence. Experiments with LDH / NADH enzyme mixture were performed to validate the effectiveness of the proposed acquisition method. Also, a modified two-site exchange model was formulated for metabolism kinetics quantification with the proposed method. Results: From the simulation results, significant increase of the lactate peak signal to noise ratio (PSNR) was observed. Also, the quantified $K_p$ value from the dynamic curves were more accurate in the case of the proposed acquisition method compared to the conventional non-selective excitation scheme. In vitro experiment results were in good agreement with the simulation results, also displaying increased PSNR for lactate. Fitting results using the modified two-site exchange model also showed expected results in agreement with the simulations. Conclusion: A method for accurate quantification of hyperpolarized pyruvate and the downstream product focused on in vitro experiment was described. By using a narrow-band RF excitation pulse with alternating acquisition, different resonances were selectively excited with a different flip angle for increased PSNR while the hyperpolarized magnetization of the substrate can be minimally perturbed with a low flip angle. Baseline signals from neighboring resonances can be effectively suppressed to accurately quantify the metabolism kinetics.

Verification of Optimum Degaussing Technique through the Mock-up Test of a Ship (축소 함정을 이용한 최적 소자기법 검증)

  • Kim, Dong-Wook;Choi, Nak-Sun;Kim, Dong-Hun;Yang, Chang-Seob;Chung, Hyun-Ju
    • Journal of the Korean Magnetics Society
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    • v.24 no.4
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    • pp.107-113
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    • 2014
  • In this paper, a optimum degaussing technique, which can minimize an underwater magnetic field anomaly generated by the ferromagnetic hull, was verified through the mock-up test of a ship. To predict degaussing field signals due to the degaussing coils installed in a ship, individual coil effects were measured. Exploiting the linearity of coil effects and analytical sensitivity formula, optimum degaussing current values fed to individual coils were decided. To identify degaussing performance of the proposed method, the obtained degaussing currents were applied to the coils. Then the field anomaly signals were measured and analyzed before and after degaussing. Experimental results show the magnitude of the field signal after degaussing is reduced up to 95% of that before degaussing.

Fabrication of Ni Nanodot Structure Using Porous Alumina Mask (다공성 알루미나 마스크를 이용한 니켈 나노점 구조 제작)

  • Lim, Suhwan;Kim, Chul Sung;Kouh, Taejoon
    • Journal of the Korean Magnetics Society
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    • v.23 no.4
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    • pp.126-129
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    • 2013
  • We have fabricated an ordered Ni nanodot structure using an alumina mask prepared via 2-step anodization technique under phosphoric acid. We have formed a porous structure with average pore size of 279 nm on $2{\mu}m$ thick alumina film and the thermal deposition of thin Ni film though the mask led to the formation of ordered Ni nanodot structure with an average dot size of 293 nm, following the pore structure on the mask. We further investigated the magnetic properties of the nanodot structure by measuring the hysteresis curve at room temperature. When compared to the magnetic properties of a continuous Ni film, we observed the decrease in the squareness and the increase in coercivity along the magnetization easy axis, due to the isolated nanodot structure. Our study suggests that the ordered nanodot structure can be easiy fabricated with thin film deposition technique using anodized alumina mask as a mask.

The Variation of Tagging Contrast-to-Noise Radio (CNR) of SPAMM Image by Modulation of Tagline Spacing (Tagline 간격의 조절을 통한 SPAMM 영상에서의 Tagging 대조도 대 잡음비의 변화)

  • 강원석;최병욱;최규옥;이상호;홍순일;정해조;김희중
    • Progress in Medical Physics
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    • v.13 no.4
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    • pp.224-228
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    • 2002
  • Myocardial tagging technique such as spatial modulation of magnetization (SPAMM) allows the study of myocardial motion with high accuracy. However, the accuracy of the estimation of tag intersection can be affected by tagline spacing. The aim of this study was to investigate the relationship between tagline spacing of SPAMM image and tagging contrast-to-noise ratio (CNR) in in-vivo study. Two healthy volunteers were undergone electrocardiographically triggered MR imaging with SPAMM-based tagging pulse sequence at a 1.5T MR scanner. Horizontally modulated stripe patterns were imposed with a range from 3.6 to 9.6 mm of tagline spacing. Images of the left ventricle(LV) wall were acquired at the mid-ventricle level during cardiac cycle with FE-EPI (TR/TE = 5.8/2.2 msec, FA= 10$^{\circ}$. Tagging CNR for each image was calculated with a software which developed in our group. During contraction, tagging CNR was more rapidly decreased in case of narrow tagline spacing than in case of wide tagline spacing. In the same heart phase, CNR was increased corresponding with tagline spacing. Especially, at the fully contracted heart phase, CNR was more rapidly increased than the other heart phases as a function of tagline spacing. The results indicated that the optimization of tagline spacing provides better tagging CNR in order to analyze the myocardial motion more accurately.

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