• Title/Summary/Keyword: M&C

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The effect of aging on the Microstructure and Hardness of Stellite 12 alloy overlayer by PTA process (PTA법에 의한 스텔라이트 12합금 육성층의 미세조직 및 경도에 미치는 시효처리의 영향)

  • 정병호;김무길;이성열
    • Journal of Advanced Marine Engineering and Technology
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    • v.26 no.1
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    • pp.68-75
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    • 2002
  • Stellite 12 alloy-powders were overlaid on 410 stainless steel valve seat by plasma transferred arc(PTA)process. Variation of microstructure and hardness of overlaid deposit with aging time at $750^{\circ}C$ was investigated. The deposit showed hypoeutectic microstructure, which was consisting of primary cobalt dendrite and networked $M_{7}C_{3}$type eutectic carbides. After aging new M_{23}C_{6}$ carbide was formed by the partial decomposition of $M_7C_3$ type eutectic carbides and finely dispersed $M_{23}C_6$ type carbides were also precipitated in the matrix. Hardness of the deposit was increased with increase of aging time at $750^{\circ}C$ and showed maximum value at 35hours. After showing maximum value, it was fallen down again at 70hours because of overaging. The increase of hardness in aging is ascribed to the formation of new stable $M_{23}C_6$ type carbide by the partial decomposition of $M_7C_3$ type eutectic carbides and also precipitation of finely dispersed $M_{23}C_6$ carbides in matrix.

Characteristics of Carbon Circulation for Ascidian Farm in Jindong Bay in Summer and Winter (진동만 미더덕 양식장의 하계 및 동계 탄소 순환 특성)

  • Park, Jihye;Cho, Yoonsik;Lee, Won-Chan;Hong, Sokjin;Kim, Hyung-Chul;Kim, Jeong-Bae;Park, Junghyun
    • Journal of Wetlands Research
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    • v.14 no.2
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    • pp.211-221
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    • 2012
  • The ascidian Styela clava has been one of the favorite seafood in Korea. Suspended culture of Styela clava was initiated in 2001 and the annual production reached 15,084 M/T, but declined to 2,655 M/T in 2011. In order to solve this problem, it is necessary to estimate the material balance according to the farm-environment. Vertical particulate fluxes and release fluxes were estimated at 2 stations, an ascidian farm (AF) and a non-cultivated area (control) in Jindong Bay. An in-situ benthic chamber(BelcI) was used in summer and winter season. The sedimentation fluxes of organic carbon were 72 mmol C $m^{-2}\;d^{-1}$, 93 mmol C $m^{-2}\;d^{-1}$, 34 mmol C $m^{-2}\;d^{-1}$ in Jul. AF, Feb. AF, Feb. control. The organic carbon oxidation rates were 13 mmol C $m^{-2}\;d^{-1}$, 81 mmol C $m^{-2}\;d^{-1}$, 31 mmol C $m^{-2}\;d^{-1}$, in each. The release fluxes of nutrients followed the general pattern, well. Consequently, the ratio of the organic carbon burial fluxes were 20:4:1, in each. By the estimation of the carbon circulation, it could be a scientific basis to analyze the reason of production decline for cultivated organism.

Biological Characteristics and Growth of the Korean Freshwater Rotifer, Brachionus calyciflorus at Various Temperatures (한국 담수산 윤층 Brachionus calyciflorus의 생물학적 특징과 온도별 성장)

  • 강언종;이배익;김응오
    • Journal of Aquaculture
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    • v.10 no.4
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    • pp.449-456
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    • 1997
  • This study was concuted to determine the optimal conditions for raising the freshwater rotifer, Brachinus calyciflorus. The authors presented some biological informatin obtained from incubation experiment under the various controlled temperatures. Lorica size of the rotifer was divided into two groups : the length and the width for the S-type was $141.0\pm16.7\mu m$($110.1-182.5\;\mu m, n=44$)and $107.0\pm20.3\mu m\;(75.3-152.3\mu m, n=44)$, and those for the L-type was $262.8\pm15.2\mu m\;(234.4-288.6\mu m,\;n=20)\;and\;182.6\pm13.4\mu m (159.8-207.0\mu m,\;n=20$), respectively. The number of eggs being attached on the female varied from 1 to 11 at various culture conditions. Egg type was divided into two groups, large and small. Large and small egg was measured in its major axis as 85a.7-107.8$\mu$m and 55.1-65.2$\mu$m for S-type, and 104.9-121.8 $\mu$m and 62.8-89.1$\mu$m for L-type respectively. The maximum density was reached at 4th day after incubation. The density was 583.9 rotifers/$m\ell$ for $25^{\circ}C$-experimental. group and 421.3 rotifers/$m\ell$ for $22^{\circ}C$-experimental. group respectively. In the case of $28^{\circ}C$-experimental. group, it suddenly decreased into 4.7 rotifers/$m\ell$ at 1st day after incubations and did not recover to its initial density. The maximum rate of increase of populatin per day was reached 0.802 for $22^{\circ}C$-experimental. group at day 2 and fluctuated thereafter. For $25^{\circ}C$-experimental. group it increased to 0.964 at day 3 of incubation and then declined. And the egg ratio of female was reached the maximum of 0.614 for 22$^{\circ}C$- at 3rd day and 0.772 for $25^{\circ}C$-experimental. group at 4th day of incubation.

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Identification of Lignan Compounds in Fruits of Schisandra chinensis BAILLON by Gas Chromatography/Mass Spectrometry (GC/MS에 의한 오미자 Lignan성분의 동정)

  • Sohn, Hyun-Joo;Bock, Jin-Young
    • Applied Biological Chemistry
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    • v.32 no.4
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    • pp.344-349
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    • 1989
  • Eleven lignan compounds in fruits of Schisandra chinensis BAILLON were identified by gas chromatography/mass spectrometry(GC/MS). The GC/MS conditions were as followed: the GC column used was SPB-1 fused silica capillary $(0.25mm\;id{\times}30m,Supelco)$ and the column oven temperature was programmed from $200^{\circ}C$ to $300^{\circ}C$ at the rate of $4^{\circ}C$ per minute; the MS ionization voltage was 70eV (EI mode). The compounds identified were gomisin J $(M^+;\;388)$, deoxyschizandrin$(M^+;\;416)$, gomisin N $(M^+;\;400)$, schizandrin$(M^+;\;432)$, wuweizisu C $(M^+;\;384)$, gomisin A $(M^+;\;416)$, angeloylgomisin H $(M^+;\;500)$, tigloylgomisin H $(M^+;\;500)$, angeloylgomisin Q $(M^+;\;530)$, gomisin B $(M^+;\;514)$ and benzoylgomisin H $(M^+;\;522)$, peaks of which were separated well on the GC chromatogram.

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Anisotropic Wet-Etching Process of Si Substrate for Formation of Thermal Vias in High-Power LED Packages (고출력 LED 패키지의 Thermal Via 형성을 위한 Si 기판의 이방성 습식식각 공정)

  • Yu, B.K.;Kim, M.Y.;Oh, T.S.
    • Journal of the Microelectronics and Packaging Society
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    • v.19 no.4
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    • pp.51-56
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    • 2012
  • In order to fabricate through-Si-vias for thermal vias by using wet etching process, anisotropic etching behavior of Si substrate was investigated as functions of concentration and temperature of TMAH solution in this study. The etching rate of 5 wt%, 10 wt%, and 25 wt% TMAH solutions, of which temperature was maintained at $80^{\circ}C$, was $0.76{\mu}m/min$, $0.75{\mu}m/min$, and $0.30{\mu}m/min$, respectively. With changing the temperature of 10 wt% TMAH solution to $20^{\circ}C$ and $50^{\circ}C$, the etching rate was reduced to $0.067{\mu}m/min$ and $0.233{\mu}m/min$, respectively. Through-Si-vias of $500{\mu}m$-depth could be fabricated by etching a Si substrate for 5 hours in 10 wt% TMAH solution at $80^{\circ}C$ after forming same via-pattern on each side of the Si substrate.

Effect of vitamin C on hepatic drug metabolism in hypoxia/reoxygenation

  • Lee, Hae-;Jung, Ju-Yeon;Han, Suck-Hee;Cho, Tai-Soon;Lee, Sun-Mee
    • Proceedings of the Korean Society of Applied Pharmacology
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    • 1998.11a
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    • pp.191-191
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    • 1998
  • It has been hypothesized that formation of oxygen-derived free radicals may play an important part in ischemically induced tissue injury. In this study, the effects of vitamin C treatment on hepatic reperfusion model were investigated. Livers isolated from 18 hrs fasted rats were subjected to low flow hypoxia (1 $m\ell$/g liver/min, for 45min) followed by reoxygenation (for 30min). The perfusion medium used was Krebs-Henseleit bicarbonate buffer (KHBB, pH 7.4) and vitamin C (0.25, 0.5, 1.0 and 2.0 mM) was added to perfusate. 7-Ethoxycoumarin was used as substrate of phase and metbolism. After hypoxia oxygen consumption significantly dropped but vitamin C 0.25, 0.5 and 1.0 mM treatments restored oxygen consumption to the level of control group. LDH and lipid peroxidation were not changed in all experimental groups. Oxidation, phase metabolism, significantly decreased following hypoxia but improved during reoxygenation. Vitamin C 0.25 mM treatment significantly improved the oxidation of 7-ethoxycoumarin during hypoxia and reoxygenation, but the oxidation significantly decreased by vitamin C 2.0 mM treatment. Similarly, sulfate conjugation decreased in hypoxic group, but this decrease was inhibited by vitamin C 0.25, 0.5 and 1.0 mM treatments. Our findings suggest that hypoxia/reoxygenation diminishes hepatic drug metabolizing function, vitamin C at concentration of 0.25-1.0 mM ameliorates but at higher concentration aggravates these hypoxia/reoxygenation-induced changes.

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Fabrication of Polycrystalline SiC Doubly Clamped Beam Micro Resonators and Their Characteristics (양단이 고정된 빔형 다결정 3C-SiC 마이크로 공진기의 제작과 그 특성)

  • Chung, Gwiy-Sang;Lee, Tae-Won
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.22 no.4
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    • pp.303-306
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    • 2009
  • This paper describes the characteristics of polycrystalline 3C-SiC doubly clamped beam micro resonators. The polycrystalline 3C-SiC doubly clamped beam resonators with $60{\sim}100{\mu}m$ lengths, $10{\mu}m$ width, and $0.4{\mu}m$ thickness were fabricated using a surface micromachining technique. Polycrystalline 3C-SiC micro resonators were actuated by piezoelectric element and their fundamental resonant frequency was measured by a laser vibrometer in vacuum at room temperature. For the $60{\sim}100{\mu}m$ long cantilevers, the fundamental frequency appeared at $373.4{\sim}908.1\;kHz$. The resonant frequencies of doubly clamped beam with lengths were higher than simulated results because of tensile stress. Therefore, polycrystalline 3C-SiC doubly clamped beam micro resonators are suitable for RF MEMS devices and bio/chemical sensor applications.

Fabrication and characterization of polycrystalline 3C-SiC mocro-resonators (다결정 3C-SiC 마이크로 공진기 제작과 그 특성)

  • Lee, Tae-Won;Chung, Gwiy-Sang
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.250-250
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    • 2008
  • This paper describes the resonant characteristics of polycrystalline SiC micro resonators. The $1{\mu}m$ thick polycrystalline 3C-SiC cantilevers with different lengths were fabricated using a surface micromachining technique. Polycrystalline 3C-SiC micro resonators were actuated by piezoelectric element and their fundamental resonance was measured by a laser vibrometer in vacuum at room temperature. For the 100 ~ $40{\mu}m$ long cantilevers, the fundamental frequency appeared at 147.2 kHz - 856.3 kHz. The $100{\mu}m$ and $80{\mu}m$ long cantilevers have second mode resonant frequency at 857.5 kHz and 1.14 MHz. Therefore, polycrystalline 3C-SiC micro resonators are suitable for RF MEMS devices and bio/chemical sensor applications.

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Facile [11C]PIB Synthesis Using an On-cartridge Methylation and Purification Showed Higher Specific Activity than Conventional Method Using Loop and High Performance Liquid Chromatography Purification (Loop와 HPLC Purification 방법보다 더 높은 비방사능을 보여주는 카트리지 Methylation과 Purification을 이용한 손쉬운 [ 11C]PIB 합성)

  • Lee, Yong-Seok;Cho, Yong-Hyun;Lee, Hong-Jae;Lee, Yun-Sang;Jeong, Jae Min
    • The Korean Journal of Nuclear Medicine Technology
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    • v.22 no.2
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    • pp.67-73
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    • 2018
  • $[^{11}C]PIB$ synthesis has been performed by a loop-methylation and HPLC purification in our lab. However, this method is time-consuming and requires complicated systems. Thus, we developed an on-cartridge method which simplified the synthetic procedure and reduced time greatly by removing HPLC purification step. We compared 6 different cartridges and evaluated the $[^{11}C]PIB$ production yields and specific activities. $[^{11}C]MeOTf$ was synthesized by using TRACERlab FXC Pro and was transferred into the cartridge by blowing with helium gas for 3 min. To remove byproducts and impurities, cartridges were washed out by 20 mL of 30% EtOH in 0.5 M $NaH_2PO_4$ solution (pH 5.1) and 10 mL of distilled water. And then, $[^{11}C]PIB$ was eluted by 5 mL of 30% EtOH in 0.5 M $NaH_2PO_4$ into the collecting vial containing 10 mL saline. Among the 6 cartridges, only tC18 environmental cartridge could remove impurities and byproducts from $[^{11}C]PIB$ completely and showed higher specific activity than traditional HPLC purification method. This method took only 8 ~ 9 min from methylation to formulation. For the tC18 environmental cartridge and conventional HPLC loop methods, the radiochemical yields were $12.3{\pm}2.2%$ and $13.9{\pm}4.4%$, respectively, and the molar activities were $420.6{\pm}20.4GBq/{\mu}mol$ (n=3) and $78.7{\pm}39.7GBq/{\mu}mol$ (n=41), respectively. We successfully developed a facile on-cartridge methylation method for $[^{11}C]PIB$ synthesis which enabled the procedure more simple and rapid, and showed higher molar radio-activity than HPLC purification method.

On characterizations of real hypersurfaces of type B in a complex hyperbolic space

  • Ahn, Seong-Soo;Suh, Young-Jin
    • Journal of the Korean Mathematical Society
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    • v.32 no.3
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    • pp.471-482
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    • 1995
  • A complex n-dimensional Kaehlerian manifold of constant holomorphic sectional curvature c is called a comples space form, which is denoted by $M_n(c)$. A complete and simply connected complex space form consists of a complex projective space $P_nC$, a complex Euclidean space $C^n$ or a complex hyperbolic space $H_nC$, according as c > 0, c = 0 or c < 0. The induced almost contact metric structure of a real hypersurface M of $M_n(c)$ is denoted by $(\phi, \zeta, \eta, g)$.

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