• Title/Summary/Keyword: Low-Shrinkage

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A NEW METHOD TO MEASURE THE LINEAR POLYMERIZATION SHRINKAGE OF COMPOSITES USING A PARTICLE TRACKING METHOD WITH COMPUTER VISION (컴퓨터 시각과 입자 추적 방법을 이용한 복합레진의 선형중합수축 측정의 새로운 방법)

  • Lee, In-Bog;Min, Sun-Hong;Seo, Deog-Gyu;Kim, Sun-Young;Kwon, Young-Chul
    • Restorative Dentistry and Endodontics
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    • v.35 no.3
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    • pp.180-187
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    • 2010
  • Since the introduction of restorative dental composites, their physical properties have been significantly improved. However, polymerization shrinkage is still a major drawback. Many efforts have been made to develop a low shrinking composite, and silorane-based composites have recently been introduced into the market. In addition, many different methods have been developed to measure the polymerization shrinkage. In this study, we developed a new method to measure the linear polymerization shrinkage of composites without direct contact to a specimen using a particle tracking method with computer vision. The shrinkage kinetics of a commercial silorane-based composite (P90) and two conventional methacrylate-based composites (Z250 and Z350) were investigated and compared. The results were as follows: 1. The linear shrinkage of composites was 0.33-1.41%. Shrinkage was lowest for the silorane-based (P90) composite, and highest for the flowable Z350 composite. 2. The new instrument was able to measure the true linear shrinkage of composites in real time without sensitivity to the specimen preparation and geometry.

Autogenous Shrinkage of High-Performance Concrete Containing Mineral Admixture (광물질 혼화재를 함유한 고성능 콘크리트의 자기수축)

  • Lee, Chang-Soo;Park, Jong-Hyok;Kim, Yong-Hyok;Kim, Young-Ook
    • Journal of the Korean Society of Hazard Mitigation
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    • v.7 no.3
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    • pp.19-31
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    • 2007
  • Humidity and strain were estimated for understanding the relation between humidity change by self-desiccation and shrinkage in high-performance concrete with low water binder ratio and containing fly ash and blast furnace slag. Internal humidity change and shrinkage strain were about 10%, 10%, 7%, 11%, 11% and $320{\times}10^{-6}$, $270{\times}10^{-6}$, $231{\times}10^{-6}$, $371{\times}10^{-6}$, $350{\times}10^{-6}$ respectively on OPC30, O30F10, O30F20, O30G40, O30G50 and from the results, fly ash made humidity change and strain decrease but slag increase comparing with ordinary portland cement. Considering only relation internal humidity and shrinkage by self-desiccation, humidity change and shrinkage represented the strong linear relation regardless of mineral admixture. For specifying the relation on internal humidity change and autogenous shrinkage strain, shrinkage model was established which is driven by capillary pressure in pore water and surface energy in hydrates on the assumption of a single network and extended meniscus in pore system of concrete. This model and experimental results had a similar tendency so it would be concluded that the internal humidity change by self-desiccation in HPC originated in small pores less than 20nm, therefore controlling plan on autogenous shrinkage might be focused on surface tension of water and degree of saturation in small pore.

A Study on The Thickness Shrinkage of Injection Molded Parts with The Variation of Injection Mold Core and Molding Materials (사출금형코어 및 성형수지 변화에 따른 두께 방향 수축률에 관한 연구)

  • Shin, Sung-Hyun;Jeong, Eui-Chul;Kim, Mi-Ae;Chae, Bo-Hye;Son, Jung-Eon;Kim, Sang-Yoon;Yoon, Kyung-Hwan;Lee, Sung-Hee
    • Design & Manufacturing
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    • v.13 no.2
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    • pp.17-21
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    • 2019
  • In this study, selective laser sintered 3D printing mold core and metal core were used to investigate the difference of the thickness shrinkage from the gate of the injection molded part at a constant interval. SLS 3D printing mold core was made of nylon-based PA2200 powder and the metal core was manufactured by conventional machining method. As the PA2200 powder material has low strength, thermal conductivity and high specific heat characteristics compared with metal, molding conditions were set with the consideration of molten temperature and injection pressure. Crystalline resin(PP) and amorphous resin(PS) with low melting temperature and viscosity were selected for the injection molding experiment. Cooling time for processing condition was selected by checking the temperature change of the cores with a cavity temperature sensor. The cooling time of the 3D printing core was required a longer time than that of the metal core. The thickness shrinkage of the molded part compared to the core depth was measured from the gate by a constant interval. It was shown that the thickness shrinkage of the 3D printing core was 2.02 ~ 4.34% larger than that of metal core. In additions, in the case of metal core, thickness shrinkage was increased with distance from the gate, on the contrary, in the case of polymer core showed reversed aspect.

The Characteristics of Compressive Strength in Mortar with Internal Curing According to Curing Condition (내부양생을 적용한 모르타르의 양생조건에 따른 압축강도 특성)

  • Kim, Joo-Hyung;Cho, Young-Keun;Lee, Kwang-Myong
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.6 no.2
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    • pp.87-93
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    • 2018
  • The use of high-strength concrete in construction have been increasing steadily. However, high-strength concrete has a low water-binder ratio, and the problems such as cracks due to hydration heat and shrinkage during the hydration process at the early age. Recently, as a method to reduce the shrinkage of concrete, study of internal curing has carried out according to increasing about interest about it. In this study, the effect of compressive strength on the curing condition(drying, moist, water) was investigated by using artificial lightweight aggregate(LWA) in high strength and high volume mortar. As a result of autogenous shrinkage, the effect of shrinkage reduction was enhanced depending on the increasing of LWA replacement. According to the curing condition, the results of compressive strength showed the different trend. The compressive strength has increased on the drying and moisture condition and decreased on the water condition.

Effect of Fe, Mn Content on the Castability in Al-9wt%Si-Mg System Alloys for High Elongation (고신율 금형주조용 Al-9wt%Si-Mg계 합금의 주조특성에 미치는 Fe, Mn함량의 영향)

  • Kim, Heon-Joo;Jeong, Chang-Yeol
    • Journal of Korea Foundry Society
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    • v.33 no.6
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    • pp.233-241
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    • 2013
  • Effect of Fe and Mn contents on the castability of Al-9wt%Si-xMg-yFe-zMn alloy has been studied. The alloy was composed of ${\alpha}$-Al phase, Al+eutectic Si phase, ${\beta}$-Al5FeSi compound and chinese script ${\alpha}$-$Al_{15}(Mn,Fe)_3Si_2$ compound. ${\beta}$-$Al_5FeSi$ and ${\alpha}$-$Al_{15}(Mn,Fe)_3Si_2$ compounds assumed to effect the fluidity and shrinkage behaviors of the alloy during solidification due to the crystallization of ${\alpha}$-$Al_{15}(Fe,Mn)_3Si_2$ and ${\beta}$-$Al_5FeSi$ compounds above eutectic temperature. As Fe and Mn contents of Al-9wt%Si-0.3wt%Mg system alloy increased from 0.15wt% to 0.6wt% and from 0.3wt% to 0.7wt%, fluidity of the alloy decreased by 5.7% and 3.3%, respectively. And as Mg content of Al-9wt%Si-0.45wt%Fe-0.5wt%Mn system alloy increased from 0.3wt% to 0.4wt%, fluidity of the alloy decreased by 8.6%. When Fe content of the alloy increased from 0.15wt% to 0.6wt%, macro shrinkage ratio decreased from 6.1% to 4.1%, and micro shrinkage ratio increased from 0.04% to 0.24%. Similarly, Mn content of the alloy increased from 0.3wt% to 0.7wt%, macro shrinkage ratio decreased from 6.0% to 4.5% and micro shrinkage ratio increased from 0.12% to 0.18%. Judging from the castability of the alloy, Al-9wt%Si-0.3wt%Mg alloy with low content of Fe and Mn, 0.1wt% Fe and 0.3wt% Mn, is recommendable.

Investigation of Shrinkage around Small Box of Short Span Slab (단경간 슬래브 중앙 소형박스(개구부)주변의 건조수축 거동 조사 연구)

  • Kim, Sang-Yeon
    • Land and Housing Review
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    • v.7 no.4
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    • pp.323-328
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    • 2016
  • There are small box opening for inserting of electric lamp box in the slab of apartment. Around this box opening, we normally use the detailing of WWF or plastic ring strengthening to protect cracks induced by shrinkage. The shrinkage amount of slab box around was measured and analysed in order to consider validity of these strengthening methods and to find out economical alternative. Alternative of strengthening methods are normally used strengthening methods in construction companies, which are WWF strengthening, plastic ring strengthening and no strengthening methods. The shrinkage amount was measured using contact guage at the spot of tip attached around the box on slab of small area unit apartment which have small exclusive area below $59m^2$. Measured data shows that there are no big differences between all the 3 strengthening methods and Measure data range is $-264{\mu}{\varepsilon}{\sim}+216{\mu}{\varepsilon}$. Measured shrinkage is on trend slightly increase till 3~5weeks after removal of forms and then decrease. But amount of shrinkage are very low for all the slabs and there are no probabilities of concrete crack by shrinkage.

Relation between Autogenous Shrinkage of Concrete and Relative Humidity, Capillary Pressure, Surface Energy in Pore (공극 내 상대습도, 모세관압력, 표면에너지 변화에 따른 콘크리트 자기수축)

  • Lee, Chang-Soo;Park, Jong-Hyok
    • Journal of the Korea Concrete Institute
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    • v.20 no.2
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    • pp.131-138
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    • 2008
  • Humidity and strain were estimated for understanding the relation between humidity change by self-desiccation and shrinkage in high-performance concrete with low water binder ratio. Internal humidity change and shrinkage strain were about 10%, 4% and $320\times10^{-6}$, $120\times10^{-6}$ respectively on concrete with water binder ratio 0.3, 0.4 and from the results, humidity change and shrinkage represented the strong linear relation regardless of mixture. For specifying the relation on internal humidity change and autogenous shrinkage strain, shrinkage model was established which is driven by capillary pressure in pore water and surface energy in hydrates on the assumption of a single network and extended meniscus in pore system of concrete. This model and experimental results had a similar tendency so it would be concluded that the internal humidity change by self-desiccation in HPC originated in small pores less than 20 nm, therefore controlling plan on autogenous shrinkage might be focused on surface tension of water and degree of saturation in small pore.

Physicochemical Properties of Non-Formaldehyde Resin Finished Rayon Fabric and Their Optimal Treatment Condition (비포름알데하이드계 수지 가공제 처리한 레이온직물의 물리화학적 특성 변화와 최적 처리 조건에 관한 연구)

  • Kim, Han-Gi;Yoon, Nam-Sik;Huh, Man-Woo;Jeon, Sung-Ki
    • Textile Coloration and Finishing
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    • v.24 no.3
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    • pp.221-231
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    • 2012
  • Rayon fabrics were treated with some commercial non-formaldehyde and low-formaldehyde resins, and then their effect on the physicochemical properties of fabrics, including formaldehyde release, tear strength, shrinkage, and wrinkle recovery, were investigated respectively. Rayons treated with non-formaldehyde resin, little formaldehyde release was observed. Considering other factors, the optimal concentration of non-formaldehyde resin was shown to be 11-13%, and curing temperature was $170{\sim}175^{\circ}C$. In case of low-formaldehyde type, 9-11% resin concentration and curing temperature of $170{\sim}180^{\circ}C$ were recommended for optimal finishing condition. The choice and combination of resins and catalysts were also important factors, and preliminary considerations before resin-finishing of rayon are also important to get much better results.

Physicochemical Properties of Non-Formaldehyde Resin Finished Cotton Fabric and their Optimal Treatment Condition (비포름알데하이드계 수지 가공제 처리한 면직물의 물리화학적 특성 변화와 최적 처리 조건에 관한 연구)

  • Kim, Han-Gi;Yoon, Nam-Sik;Huh, Man-Woo;Kim, Ick-Soo
    • Textile Coloration and Finishing
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    • v.24 no.2
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    • pp.121-130
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    • 2012
  • Cotton fabrics were treated with some commercial non-formaldehyde and low-formaldehyde resins, and then their effect on the physicochemical properties were respectively investigated including formaldehyde release, tear strength, shrinkage, and wrinkle recovery. Formaldehyde release less than 10ppm was obtained only by non-formaldehyde resin. Considering other factors, the optimal concentration of non-formaldehyde resin was shown to be 9-11%. In case of low-formaldehyde type, 5-7% resin concentration and curing temperature of $160{\sim}170^{\circ}C$ were recommended for optimal finishing condition. The choice and combination of resins and catalysts were also important factors, and preliminary considerations before treating cotton fabrics with resins used in this study are also important to get much better results.

Effect of low-calcium fly ash on sulfate resistance of cement paste under different exposure conditions

  • Zhang, Wuman;Zhang, Yingchen;Gao, Longxin
    • Advances in concrete construction
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    • v.7 no.3
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    • pp.175-181
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    • 2019
  • Low-calcium fly ash (LCFA) were used to prepare cement/LCFA specimens in this study. The basic physical properties including water demand, fluidity, setting time, soundness and drying shrinkage of cement/LCFA paste were investigated. The effects of curing time, immersion time and wet-dry cycles in 3% $Na_2SO_4$ solution on the compressive strength and the microstructures of specimens were also discussed. The results show that LCFA increases the water demand, setting time, soundness of cement paste samples. 50% and 60% LCFA replacement ratio decrease the drying shrinkage of hardened cement paste. The compressive strength of plain cement specimens decreases at the later immersion stage in 3% $Na_2SO_4$ solution. The addition of LCFA can decrease this strength reduction of cement specimens. For all specimens with LCFA, the compressive strength increases with increasing immersion time. During the wet-dry cycles, the compressive strength of plain cement specimens decreases with increasing wet-dry cycles. However, the pores in the specimens with 30% and 40% LCFA at early ages could be large enough for the crystal of sodium sulfate, which leads to the compressive strength increase with the increase of wet-dry cycles in 3% $Na_2SO_4$ solution. The microstructures of cement/LCFA specimens are in good agreement with the compressive strength.